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21. 发明授权

US07129323B2 Bimolecular nucleation methods for thermoplastics 有权
标题翻译：热塑性塑料的双分子成核方法
公开(公告)号：US07129323B2
公开(公告)日：2006-10-31
申请号：US10172338
申请日：2002-06-14
申请人： Darin L. Dotson , Nathan A. Mehl , Brian M. Burkhart , Jiannong Xu
发明人： Darin L. Dotson , Nathan A. Mehl , Brian M. Burkhart , Jiannong Xu
IPC分类号： C08K5/098 , C08K3/22
CPC分类号： C08K5/0083 , C08J3/201 , C08J2323/10 , C08K5/098
摘要： Specific methods of inducing high nucleation rates in thermoplastics, such as polyolefins, and particularly, though not necessarily, polypropylenes, through the introduction of two different compounds that are substantially soluble within the target molten thermoplastic resin (such as, as one non-limiting example, an added compound including at least one acid group and an added organic salt) are provided. Such introduced components react to form a nucleating agent in situ within such a target molten thermoplastic resin which is then allowed to cool. Preferably, one compound is an acid, preferably bicyclic (i.e., two cyclic systems sharing at least three carbon atoms) or monocycloaliphatic (i.e., a single, saturated ring system) in nature, such as, without limitation, bicyclo[2.2.1]heptane dicarboxylic acid or hexahydrophthalic acid, and the other compound is an organic salt, such as a carboxylate, sulfonate, phosphate, oxalate, and the like, and more preferably selected from the group consisting of metal C8–C22 esters. Such a production method thus provides a manner of generating in Situ the desired nucleating agent through reaction of such soluble compounds. Kits (e.g., masterbatch methods, for example) comprising such components for easy introduction within target molten polyolefin resins are also contemplated within this invention.
摘要翻译：通过引入基本上可溶于目标熔融热塑性树脂的两种不同的化合物（例如作为一个非限制性实例），在热塑性塑料如聚烯烃，特别是但不一定是聚丙烯中诱导高成核速率的具体方法，含有至少一个酸基和添加的有机盐的添加化合物）。这种引入的组分反应以在这样的目标熔融热塑性树脂中就地形成成核剂，然后使其冷却。优选地，一种化合物在本质上是酸，优选双环（即，共享至少三个碳原子的两个环状体系）或单环脂族（即单个饱和环系），例如但不限于双环[2.2.1] 庚烷二羧酸或六氢邻苯二甲酸，另一种化合物为有机盐，如羧酸盐，磺酸盐，磷酸盐，草酸盐等，更优选选自金属C 8 -C 22酯。因此，这种制备方法提供了通过这些可溶性化合物的反应原位产生所需成核剂的方式。在本发明中也考虑了包含这些组分以用于在目标熔融聚烯烃树脂内容易引入的组分（例如，母料方法）。

22. 发明申请

US20050249905A1 Polyolefin container having certain shrink characteristics and method of making such containers 审中-公开
标题翻译：具有一定收缩特性的聚烯烃容器和制造这种容器的方法
公开(公告)号：US20050249905A1
公开(公告)日：2005-11-10
申请号：US11137046
申请日：2005-05-25
申请人： Jiannong Xu , Bemard Vermeersch , W. Lambert
发明人： Jiannong Xu , Bemard Vermeersch , W. Lambert
IPC分类号： B29C35/08 , B29C49/00 , B29C49/06 , B29C49/12 , B65D1/00 , B65D1/02
CPC分类号： B29C49/0005 , B29B2911/1402 , B29B2911/14026 , B29B2911/14033 , B29B2911/1404 , B29B2911/14106 , B29B2911/14133 , B29B2911/14326 , B29B2911/14593 , B29B2911/14653 , B29B2911/14906 , B29C49/06 , B29C49/12 , B29C2035/0822 , B29K2023/12 , B29K2067/00 , B29K2623/12 , B29L2031/7158 , B65D1/0207 , Y10T428/1352
摘要： The two stage production of clear, low-haze, injection stretch blow molded polypropylene container articles with advantageous free shrink characteristics is disclosed. In the first processing stage, a preform article is manufactured on an injection molding machine. In a second and subsequent step, which may occur remotely from apparatus used in the first step, the preform article is heated and stretch blown into a container. The process may employ the selection of processing parameters to produce preform articles that facilitate stretch blow molding at relatively high rates of speed, while still maintaining an appropriate polypropylene polymer morphology that results in clear, low haze containers. Free shrink may be improved and measured. Furthermore, a haze, MFI, and wall thickness of containers subjected to a free shrinkage test following manufacture may be used to estimate or predict the processing parameters used to manufacture the container.
摘要翻译：公开了具有有利的自由收缩特性的透明，低雾，注射拉伸吹塑聚丙烯容器制品的两阶段生产。在第一加工阶段，在注射成型机上制造预成型制品。在可以从第一步骤中使用的装置远程发生的第二和随后的步骤中，将预成型制品加热并拉伸吹入容器。该方法可以采用加工参数的选择来生产预成型制品，以便以相当高的速度进行吹塑成型，同时仍保持导致澄清的低雾度容器的合适的聚丙烯聚合物形态。可以改善和测量自由收缩。此外，可以使用在制造之后进行自由收缩试验的容器的雾度，MFI和壁厚来估计或预测用于制造容器的加工参数。

23. 发明申请

US20110105664A1 THERMOPLASTIC POLYMER COMPOSITION 有权
标题翻译：热塑性聚合物组合物
公开(公告)号：US20110105664A1
公开(公告)日：2011-05-05
申请号：US12903686
申请日：2010-10-13
申请人： Darin L. Dotson , Robbie Willem Johan M. Hanssen , Jiannong Xu
发明人： Darin L. Dotson , Robbie Willem Johan M. Hanssen , Jiannong Xu
IPC分类号： C08K5/098
CPC分类号： C08K5/098 , C07C53/134 , C08K5/0083 , C08K5/0091 , C08L23/02 , Y10S521/908
摘要： A thermoplastic polymer composition comprises a thermoplastic polymer and a nucleating agent. The nucleating agent comprises a compound conforming to the structure of Formula (I) or Formula (II)
摘要翻译：热塑性聚合物组合物包含热塑性聚合物和成核剂。成核剂包括符合式（I）或式（II）的结构的化合物，

24. 发明授权

US08779045B2 Thermoplastic polymer composition 有权
标题翻译：热塑性聚合物组成
公开(公告)号：US08779045B2
公开(公告)日：2014-07-15
申请号：US12903686
申请日：2010-10-13
申请人： Darin L. Dotson , Robbie Willem Johan M. Hanssen , Jiannong Xu
发明人： Darin L. Dotson , Robbie Willem Johan M. Hanssen , Jiannong Xu
IPC分类号： C08K5/098 , C08K5/00 , C08L23/02 , C07C53/134
CPC分类号： C08K5/098 , C07C53/134 , C08K5/0083 , C08K5/0091 , C08L23/02 , Y10S521/908
摘要： A thermoplastic polymer composition comprises a thermoplastic polymer and a nucleating agent. The nucleating agent comprises a compound conforming to the structure of Formula (I) or Formula (II)
摘要翻译：热塑性聚合物组合物包含热塑性聚合物和成核剂。成核剂包括符合式（I）或式（II）的结构的化合物，

25. 发明申请

US20070080485A1 Film and methods of making film 审中-公开
标题翻译：电影和制作电影的方法
公开(公告)号：US20070080485A1
公开(公告)日：2007-04-12
申请号：US11496989
申请日：2006-08-01
申请人： Christopher Kerscher , Jiannong Xu
发明人： Christopher Kerscher , Jiannong Xu
IPC分类号： C08K5/09 , B29C55/28 , B29C55/06
CPC分类号： C08J5/18 , C08J2323/12 , C08K5/098 , C08K2201/014 , C08L23/12
摘要： Employment of cycloaliphatic salt nucleating agent additives in thermoplastics or polyolefins such as polypropylene may improve the properties of a manufactured film. Furthermore, co-additives used with the cycloaliphatic salts, such as fatty acid salts, also may improve the film properties in terms of physical properties and haze of the resulting film. Fatty acid salts may include stearates with metal ion salts, such as zinc, calcium, lithium, magnesium or sodium.
摘要翻译：在热塑性塑料或聚烯烃如聚丙烯中使用脂环族成核剂添加剂可以改善所制成膜的性能。此外，与脂环族盐例如脂肪酸盐一起使用的共添加剂也可以在所得膜的物理性能和雾度方面改善膜性质。脂肪酸盐可以包括具有金属离子盐的硬脂酸盐，例如锌，钙，锂，镁或钠。

26. 发明申请

US20050197435A1 Polymer additive compositions for bimolecular nucleation in thermoplastics 审中-公开
标题翻译：用于热塑性塑料中双分子成核的聚合物添加剂组合物
公开(公告)号：US20050197435A1
公开(公告)日：2005-09-08
申请号：US11103384
申请日：2005-04-11
申请人： Darin Dotson , Nathan Mehl , Brian Burkhart , Jiannong Xu
发明人： Darin Dotson , Nathan Mehl , Brian Burkhart , Jiannong Xu
IPC分类号： C08K5/04
CPC分类号： C08K5/0083 , C08K5/092 , C08K5/098
摘要： Specific methods of inducing high nucleation rates in thermoplastics, such as polyolefins, and particularly, though not necessarily, polypropylenes, through the introduction of two different compounds that are substantially soluble within the target molten thermoplastic resin (such as, as one non-limiting example, an added compound including at least one acid group and an added organic salt) are provided. Such introduced components react to form a nucleating agent in situ within such a target molten thermoplastic resin which is then allowed to cool. Preferably, one compound is an acid, preferably bicyclic (i.e., two cyclic systems sharing at least three carbon atoms) or monocycloaliphatic (i.e., a single, saturated ring system) in nature, such as, without limitation, bicyclo[2.2.1]heptane dicarboxylic acid or hexahydrophthalic acid, and the other compound is an organic salt, such as a carboxylate, sulfonate, phosphate, oxalate, and the like, and more preferably selected from the group consisting of metal C8-C22 esters. Such a production method thus provides a manner of generating in situ the desired nucleating agent through reaction of such soluble compounds. Kits (e.g., masterbatch methods, for example) comprising such components for easy introduction within target molten polyolefin resins are also contemplated within this invention.
摘要翻译：通过引入基本上可溶于目标熔融热塑性树脂的两种不同的化合物（例如作为一个非限制性实例），在热塑性塑料如聚烯烃，特别是但不一定是聚丙烯中诱导高成核速率的具体方法，含有至少一个酸基和添加的有机盐的添加化合物）。这种引入的组分反应以在这样的目标熔融热塑性树脂中就地形成成核剂，然后使其冷却。优选地，一种化合物在本质上是酸，优选双环（即，共享至少三个碳原子的两个环状体系）或单环脂族（即单个饱和环系），例如但不限于双环[2.2.1] 庚烷二羧酸或六氢邻苯二甲酸，另一种化合物为有机盐，如羧酸盐，磺酸盐，磷酸盐，草酸盐等，更优选选自金属C 8 -C 22酯。因此，这种制备方法提供了通过这些可溶性化合物的反应原位产生所需成核剂的方式。在本发明中也考虑了包含这些组分以用于在目标熔融聚烯烃树脂内容易引入的组分（例如，母料方法）。

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