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21. 发明授权

US5639706A Hydrogenation catalyst based on a platinum metal partially poisoned with finely divided sulfur 失效
标题翻译：基于铂金属的氢化催化剂部分中和细分硫
公开(公告)号：US5639706A
公开(公告)日：1997-06-17
申请号：US511736
申请日：1995-08-07
申请人： Franz-Josef Weiss , Hugo Fuchs , Gerald Neubauer , Heinz-Walter Schneider
发明人： Franz-Josef Weiss , Hugo Fuchs , Gerald Neubauer , Heinz-Walter Schneider
IPC分类号： B01J23/40 , B01J23/42 , B01J27/02 , B01J37/18 , B01J37/20 , C01B21/14
CPC分类号： B01J23/40 , B01J23/42 , B01J27/02 , B01J37/18 , B01J37/20 , C01B21/1418
摘要： A hydrogenation catalyst, obtainable by carrying out essentially the following steps:(a) treatment of a platinum metal salt with finely divided sulfur followed by(b) reduction of the platinum metal salt to metallic platinum metal.
摘要翻译：一种氢化催化剂，可通过基本上进行以下步骤得到：（a）用细碎的硫处理铂金属盐，然后（b）将铂金属盐还原为金属铂金属。

22. 发明授权

US4804473A Removal of water-immiscible solvents from offgases containing same 失效
标题翻译：从含有它们的废气中除去与水不混溶的溶剂
公开(公告)号：US4804473A
公开(公告)日：1989-02-14
申请号：US136418
申请日：1987-12-22
申请人： Uwe Brand , Emile DeDecker , Ernst Deuker , Hugo Fuchs , Klaus Kartte , Gerald Neubauer , Jozef Oostvogels
发明人： Uwe Brand , Emile DeDecker , Ernst Deuker , Hugo Fuchs , Klaus Kartte , Gerald Neubauer , Jozef Oostvogels
IPC分类号： B01D53/44 , B01D53/14 , B01D53/34 , B01D53/72 , B01D53/77 , C07D201/16 , B01D11/04
CPC分类号： B01D53/1487 , B01D53/1493 , C07D201/16
摘要： Water-immiscible solvents are removed from offgases containing same by washing with water-containing caprolactam.
摘要翻译：通过用含水己内酰胺洗涤除去与水相混溶的溶剂。

23. 发明授权

US5350847A Purification of caprolactam 失效
标题翻译：己内酰胺的纯化
公开(公告)号：US5350847A
公开(公告)日：1994-09-27
申请号：US113081
申请日：1993-08-30
申请人： Hugo Fuchs , Gerald Neubauer , Claus-Ulrich Priester
发明人： Hugo Fuchs , Gerald Neubauer , Claus-Ulrich Priester
IPC分类号： C07B63/02 , C07D201/16 , C07D201/12
CPC分类号： C07D201/16
摘要： Caprolactam is purified by oxidative treatment in which mixtures which essentially contain the caprolactam to be purified and unsaturated lactams are treated with oxygen or an oxygen-containing gas mixture in an alkaline medium.
摘要翻译：己内酰胺通过氧化处理纯化，其中基本上含有待纯化的己内酰胺和不饱和内酰胺的混合物在碱性介质中用氧或含氧气体混合物处理。

24. 发明授权

US5637700A Purification of caprolactam 失效
标题翻译：己内酰胺的纯化
公开(公告)号：US5637700A
公开(公告)日：1997-06-10
申请号：US297719
申请日：1994-08-30
申请人： Hugo Fuchs , Gerald Neubauer , Claus-Ulrich Priester
发明人： Hugo Fuchs , Gerald Neubauer , Claus-Ulrich Priester
IPC分类号： C07B63/02 , C07D201/16 , C07D201/12
CPC分类号： C07D201/16
摘要： Caprolactam is purified by oxidative treatment in which mixtures which essentially contain the caprolactam to be purified and unsaturated lactams are treated with oxygen or an oxygen-containing gas mixture in an alkaline medium.
摘要翻译：通过氧化处理纯化己内酰胺，其中基本上含有要纯化的己内酰胺和不饱和内酰胺的混合物在碱性介质中用氧或含氧气体混合物处理。

25. 发明授权

US5496789A Hydrogenation catalyst based on a platinum metal partially poisoned with finely divided sulfur 失效
标题翻译：基于铂金属的氢化催化剂部分中和细分硫
公开(公告)号：US5496789A
公开(公告)日：1996-03-05
申请号：US224677
申请日：1994-04-07
申请人： Franz-Josef Weiss , Hugo Fuchs , Gerald Neubauer , Heinz-Walter Schneider
发明人： Franz-Josef Weiss , Hugo Fuchs , Gerald Neubauer , Heinz-Walter Schneider
IPC分类号： B01J23/40 , B01J23/42 , B01J27/02 , B01J37/18 , B01J37/20 , C01B21/14
CPC分类号： B01J23/40 , B01J23/42 , B01J27/02 , B01J37/18 , B01J37/20 , C01B21/1418
摘要： A hydrogenation catalyst, obtainable by carrying out essentially the following steps:(a) treatment of a platinum metal salt with finely divided sulfur followed by(b) reduction of the platinum metal salt to metallic platinum metal.
摘要翻译：一种氢化催化剂，可通过基本上进行以下步骤得到：（a）用细碎的硫处理铂金属盐，然后（b）将铂金属盐还原为金属铂金属。

26. 发明授权

US4138472A Process for obtaining coarsely crystalline pure ammonium sulfate 失效
标题翻译：获得粗结晶纯硫酸铵的方法
公开(公告)号：US4138472A
公开(公告)日：1979-02-06
申请号：US844647
申请日：1977-10-25
申请人： Gerald Neubauer , Gerard Van Wauwe , Josef Beullens , Uwe Brand , Hugo Fuchs , Klaus Kartte
发明人： Gerald Neubauer , Gerard Van Wauwe , Josef Beullens , Uwe Brand , Hugo Fuchs , Klaus Kartte
IPC分类号： C01C1/242 , C01C1/248
CPC分类号： C01C1/242 , C01C1/248
摘要： A process for obtaining coarsely crystalline pure ammonium sulfate from reaction mixtures which have been obtained by Beckmann rearrangement of cyclohexanone-oxime with sulfuric acid or oleum, by neutralizing the mixtures with ammonia at an elevated temperature, with the addition of recycled ammonium sulfate mother liquor, the concentration being so chosen that during the neutralization no solid ammonium sulfate precipitates, separating the crude caprolactam from the ammonium sulfate solution, crystallizing ammonium sulfate by evaporating the ammonium sulfate solution under reduced pressure, separating off the crystallized ammonium sulfate and recycling the mother liquor to the neutralization stage. The neutralization is carried out at from 80.degree. to 115.degree. C. under autogenous pressure and the ammonium sulfate solution obtained after separating off the crude lactam is evaporated under a pressure of from 200 to 600 mm Hg while cooling to from 72.degree. to 101.degree. C.
摘要翻译：从反应混合物中获得粗结晶纯硫酸铵的方法，其通过用硫酸或发烟硫酸重整环己酮 - 肟，通过在升高的温度下用氨中和混合物，再加入回收的硫酸铵母液，浓度如此选择，使得在中和期间没有固体硫酸铵沉淀，将粗己内酰胺与硫酸铵溶液分离，通过在减压下蒸发硫酸铵溶液使硫酸铵结晶，分离结晶的硫酸铵并将母液再循环至中和阶段。中和在自生压力下在80〜115℃进行，分离出内酰胺后得到的硫酸铵溶液在200〜600mmHg的压力下蒸发，同时冷却至72〜101℃。 C。

27. 发明授权

US4837362A Preparation of pure hydroxylammonium salts of fatty acids of 1 to 4 carbon atoms 失效
标题翻译：制备1至4个碳原子的脂肪酸的纯羟基铵盐
公开(公告)号：US4837362A
公开(公告)日：1989-06-06
申请号：US3658
申请日：1987-01-15
申请人： Hugo Fuchs , Franz-Josef Weiss
发明人： Hugo Fuchs , Franz-Josef Weiss
IPC分类号： C07C53/08 , C07C51/00 , C07C51/41 , C07C51/43 , C07C53/122 , C07C67/00
CPC分类号： C07C51/412
摘要： Pure hydroxylammonium salts of fatty acids of 1 to 4 carbon atoms are prepared by reacting hydroxylammonium sulfate and alkali metal salts of fatty acids with 1 to 4 carbon atoms in solution at elevated temperatures and separating off the hydroxylammonium salts of fatty acids of 1 to 4 carbon atoms by(a) reacting hydroxylammonium sulfate and alkali metal salts of fatty acids of 1 to 4 carbon atoms in solution in water or alkanols of 1 to 3 carbon atoms or mixtures thereof at 20.degree.-70.degree. C.,(b) evaporating the solvent out of the reaction mixture to obtain a dry residue,(c) isolating the hydroxlammonium salts of fatty acids of 1 to 4 carbon atoms from the dry residue thus obtained by sublimation under reduced pressure.
摘要翻译： 1〜4个碳原子的脂肪酸的纯羟基铵盐是通过羟基硫酸铵与脂肪酸的碱金属盐在溶液中在高温下反应而制成的，分离出1至4个碳原子的脂肪酸的羟基铵盐原子通过（a）使羟基硫酸铵和1至4个碳原子的脂肪酸的碱金属盐在1至3个碳原子的水或链烷醇或其混合物的溶液中在20℃-70℃下反应，（b）将溶剂从反应混合物中得到干燥残余物，（c）从减压升华得到的干燥残余物中分离出1至4个碳原子的脂肪酸的羟基铵盐。

28. 发明授权

US4795571A Purification of frozen crystal layers 失效
标题翻译：冷冻晶体层的净化
公开(公告)号：US4795571A
公开(公告)日：1989-01-03
申请号：US154227
申请日：1988-02-10
申请人： Bernhard Holzknecht , Hugo Fuchs , Eckhard Hetzel , Klaus Wintermantel , Peter Thoma
发明人： Bernhard Holzknecht , Hugo Fuchs , Eckhard Hetzel , Klaus Wintermantel , Peter Thoma
IPC分类号： B01D9/00 , B01D9/02 , B01D9/04 , C07B63/00 , C07C67/00 , C07C241/00 , C07C265/14 , C07D201/16
CPC分类号： C07D201/16 , B01D9/0013
摘要： Frozen crystal layers are purified by a process in which these crystal layers, after they have been frozen out from a melt or solution on a cooling surface, are brought into contact with a purifying liquid and thus purified over their entire thickness, after which the said layers are separated from the purifying liquid and then melted, wherein the temperature of the crystal layers and of the purifying liquid is close to the melting point or solubility temperature, mass transfer at the phase boundary is intensified by forced convection, and this purification is carried out in the course of from 1 to 60 minutes on layers having a thickness of from 0.2 to 10 mm.
摘要翻译：冷冻的晶体层通过这些方法纯化，其中这些晶体层在从冷却表面上的熔体或溶液中冷冻出来之后，与净化液体接触并由此在其整个厚度上净化，之后所述将层与净化液分离，然后熔融，其中晶体层和净化液的温度接近熔点或溶解温度，通过强制对流加强相边界处的质量传递，并进行该纯化在厚度为0.2至10mm的层上为1至60分钟的过程。

29. 发明授权

US4268440A Preparation of caprolactam 失效
标题翻译：己内酰胺的制备
公开(公告)号：US4268440A
公开(公告)日：1981-05-19
申请号：US129827
申请日：1980-03-13
申请人： Joachim Werther , Hugo Fuchs , Uwe Brand , Friedrich R. Faulhaber
发明人： Joachim Werther , Hugo Fuchs , Uwe Brand , Friedrich R. Faulhaber
IPC分类号： C07B61/00 , C07D201/04
CPC分类号： C07D201/04
摘要： A process for the preparation of caprolactam wherein, in a first stage, cyclohexanone-oxime is vaporized, in the presence of inert gases, by bringing it into contact with a fluidized bed of inert solid particles at from 150.degree. to 250.degree. C., and the mixture of cyclohexanone-oxime vapor and inert gases is passed into a second stage, where the cyclohexanone-oxime is rearranged to caprolactam at from 230.degree. to 450.degree. C. over a supported catalyst, containing boron trioxide, in a fluidized bed.
摘要翻译：一种制备己内酰胺的方法，其中在惰性气体存在下，在第一阶段将环己酮 - 肟气化，使其与150℃至250℃的惰性固体颗粒流化床接触，并将环己酮 - 肟蒸气和惰性气体的混合物进入第二阶段，其中环己酮 - 肟在230℃至450℃下在含有三氧化硼的负载催化剂上在流化床中重排为己内酰胺。

30. 再颁专利

USRE33073E Obtaining caprolactam by cleaving oligomers of caprolactam 失效
标题翻译：通过裂解己内酰胺的低聚物来获得己内酰胺
公开(公告)号：USRE33073E
公开(公告)日：1989-09-26
申请号：US171414
申请日：1988-03-21
申请人： Hugo Fuchs , Uwe Brand , Helmut Buchaeckert
发明人： Hugo Fuchs , Uwe Brand , Helmut Buchaeckert
IPC分类号： C07D201/12
CPC分类号： C07D201/12
摘要： Caprolactam is obtained by cleaving oligomers of caprolactam by a process in which the oligomers, in a liquid or solid state, are introduced into a fluidized alumina bed and cleaved at from 290.degree. to 400.degree. C. in the presence of steam, and, in addition to the amount of inert gas required to fluidize the alumina bed, from 0.1 to 3 times this amount of inert gas is introduced above the fluidized bed.

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