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21. 发明授权

US4189542A Process for the production of foam moldings having an impervious outer skin using semi-prepolymer prepared from isocyanates such as isophorone diisocyanate 失效
标题翻译：使用由异氰酸酯如异佛尔酮二异氰酸酯制备的半预聚物生产具有不透水外皮的泡沫塑料制品的方法
公开(公告)号：US4189542A
公开(公告)日：1980-02-19
申请号：US930303
申请日：1978-08-02
申请人： Helmut Kleimann , Holger Meyborg , Hans-Jurgen Lienert , Gerhard Grogler
发明人： Helmut Kleimann , Holger Meyborg , Hans-Jurgen Lienert , Gerhard Grogler
IPC分类号： C08J9/02 , C08G18/10 , C08G18/75 , C08G18/80 , C08G18/14
CPC分类号： C08G18/8058 , C08G18/10 , C08G18/75 , C08G18/8032
摘要： The instant invention is directed to a process for the production of weather-resistant rigid molded foams based on polyurethanes having a dimensional stability under heat according to DIN 53 432 of at least 70.degree. C. and a compact surface, a cellular core and an integral density distribution throughout the cross-section of the moldings, comprising foaming a foamable reaction mixture of polyisocyanates, polyhydroxyl compounds, blowing agents and, optionally, other isocyanate-reactive compounds, activators and other auxiliaries in a closed mold under the conditions of in-mold foaming, the improvement wherein the polyisocyanates used are reaction products containing isocyanate groups and urethane groups, said reaction products formed by reacting diisocyanates containing at least one cycloaliphatically bound isocyanate group and no more than one aliphatically bound isocyanate group with sub-stoichiometric quantities of organic polyhydroxyl compounds.
摘要翻译：本发明涉及一种用于生产基于聚氨酯的耐候刚性模塑泡沫的方法，所述聚氨酯在根据DIN 53 432的加热条件下具有至少70℃的尺寸稳定性，以及紧凑的表面，多孔芯和积分包括在模制品的整个横截面处的密度分布，包括在模内的条件下，在封闭模具中发泡多异氰酸酯，多羟基化合物，发泡剂和任选的其它异氰酸酯反应性化合物，活化剂和其它助剂的可发泡反应混合物发泡，其中使用的多异氰酸酯是含有异氰酸酯基团和氨基甲酸酯基团的反应产物的改进，所述反应产物是通过使含有至少一个环脂族连接的异氰酸酯基团的二异氰酸酯和不超过一个脂族结合的异氰酸酯基团与亚化学计量的有机多羟基化合物。

22. 发明授权

US4564645A Process for the production of dianhydrohexitol mixtures and the production of polymers from such mixtures 失效
标题翻译：用于制备二羟基己糖醇混合物的方法和由这些混合物生产聚合物
公开(公告)号：US4564645A
公开(公告)日：1986-01-14
申请号：US689357
申请日：1985-01-07
申请人： Herbert Salzburg , Manfred Hajek , Holger Meyborg
发明人： Herbert Salzburg , Manfred Hajek , Holger Meyborg
IPC分类号： C07D493/04 , C08G18/32 , C08G18/30
CPC分类号： C07D493/04 , C08G18/3218
摘要： Liquid dianhydrohexitol mixtures are prepared from diacylation products of hexitols and compounds such as organic carboxylic acids, carboxylic acid anhydrides, carboxylic acid halides, ketene and carbonic acid ester derivatives. More specifically, such diacylation products are simultaneously dehydrated and isomerized by subjecting them to a temperature of at least 130.degree. C. in the presence of a strong acid to yield diacylated dianhydro-hexitol isomer mixtures. These isomer mixtures are then converted to dianhydro-hexitol isomer mixtures by hydrolysis or transesterification. Suitable strong acids include proton acids, Lewis acids and heterogeneous acid catalysts (e.g., ion exchange resins). The mixtures of the present invention are characterized by a minimal tendency towards crystallization. These mixtures are particularly useful as chain extending agents in the production of polyurethanes.
摘要翻译：液体二脱水己糖醇混合物由己醇的二酰化产物和有机羧酸，羧酸酐，羧酸卤化物，乙烯酮和碳酸酯衍生物等化合物制备。更具体地说，这样的二酰化产物通过在强酸存在下使其至少130℃的温度同时进行脱水和异构化，得到二酰化二脱氢 - 己糖醇异构体混合物。然后通过水解或酯交换将这些异构体混合物转化为二脱氢己糖醇异构体混合物。合适的强酸包括质子酸，路易斯酸和多相酸催化剂（如离子交换树脂）。本发明的混合物的特征在于最小的结晶倾向。这些混合物特别可用作聚氨酯生产中的扩链剂。

23. 发明授权

US4506086A Process for the production of dianhydrohexitol mixtures and liquid mixture of dianhydrohexitols 失效
标题翻译：二脱水己醇混合物的生产方法和二脱水己醇的液体混合物
公开(公告)号：US4506086A
公开(公告)日：1985-03-19
申请号：US515411
申请日：1983-07-20
申请人： Herbert Salzburg , Manfred Hajek , Holger Meyborg
发明人： Herbert Salzburg , Manfred Hajek , Holger Meyborg
IPC分类号： C07D493/04 , C08G18/32
CPC分类号： C07D493/04 , C08G18/3218
摘要： Liquid dianhydrohexitol mixtures are prepared from diacylation products of hexitols and compounds such as organic carboxylic acids, carboxylic acid anhydrides, carboxylic acid halides, ketene and carbonic acid ester derivatives. More specifically, such diacylation products are simultaneously dehydrated and isomerized by subjecting them to a temperature of at least 130.degree. C. in the presence of a strong acid to yield diacylated dianhydrohexitol isomer mixtures. These isomer mixtures are then converted to dianhydrohexitol isomer mixtures by hydrolysis or transesterification. Suitable strong acids include proton acids, Lewis acids and heterogeneous acid catalysts (e.g., ion exchange resins). The mixtures of the present invention are characterized by a minimal tendency towards crystallization. These mixtures are particularly useful as chain extending agents in the production of polyurethanes.
摘要翻译：液体二脱水己糖醇混合物由己醇的二酰化产物和有机羧酸，羧酸酐，羧酸卤化物，乙烯酮和碳酸酯衍生物等化合物制备。更具体地说，这样的二酰化产物通过在强酸存在下经受至少130℃的温度同时进行脱水和异构化，得到二酰基二脱水己糖异构体混合物。然后通过水解或酯交换将这些异构体混合物转化成二羟基己糖异构体混合物。合适的强酸包括质子酸，路易斯酸和多相酸催化剂（如离子交换树脂）。本发明的混合物的特征在于最小的结晶倾向。这些混合物特别可用作聚氨酯生产中的扩链剂。

24. 发明授权

US4383051A Process for the preparation of polyurethane plastics using dianhydro-hexite diols 失效
标题翻译：使用二氢 - 己二醇二醇制备聚氨酯塑料的方法
公开(公告)号：US4383051A
公开(公告)日：1983-05-10
申请号：US357118
申请日：1982-03-11
申请人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
发明人： Holger Meyborg , Kuno Wagner , James M. Barnes , Herbert Salzburg
IPC分类号： C08L65/00 , C08G18/00 , C08G18/10 , C08G18/32 , C08G18/65 , C08L7/00 , C08L21/00 , C08L67/00 , C08L77/00 , C08G18/14
CPC分类号： C08G18/6511 , C08G18/10 , C08G18/3218
摘要： A process for the preparation of homogeneous and cellular polyurethane plastics by the reaction of(a) organic polyisocyanates;(b) compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having molecular weights of from 400 to 10,000;(c) chain extenders, and, optionally, additional(d) short-chained compounds containing at least 2 Zerewitinoff-active hydrogen atoms and having a molar mass of from 32 to 400, as well as, optionally,(e) catalysts, blowing agents and other known additives,is described, which is characterized in that 1,4-3,6-dianhydro-hexites, preferably 1,4-3,6-dianhydro-D-sorbitol and/or 1,4-3,6-dianhydro-D-mannitol, optionally mixed with lower molecular weight compounds, preferably with polyols having a molecular weight of from 62 to 400, particularly preferably butane diol-1,4 are used as the chain extenders. The new chain extenders produce high quality elastomers and foams.
摘要翻译：通过（a）有机多异氰酸酯的反应制备均匀和细胞聚氨酯塑料的方法; （b）含有至少2个Zerewitinoff-活性氢原子并且分子量为400至10,000的化合物; （c）扩链剂，以及任选地，含有至少2个Zerewitinoff-活性氢原子并且具有32-400摩尔质量的另外的（d）短链化合物，以及任选的（e）催化剂，吹制其特征在于1,4-3,6-二脱水 - 己酸，优选1,4-3,6-二脱氢-D-山梨糖醇和/或1,4-3,6 - 二水-D-甘露糖醇，任选地与较低分子量的化合物混合，优选使用分子量为62至400的多元醇，特别优选丁二醇-1,4作为扩链剂。新的增链剂生产高品质的弹性体和泡沫。

25. 发明授权

US4350781A Process for the preparation of polymer precursors containing oxazolin-2-one rings 失效
标题翻译：制备含恶唑啉-2-酮环的聚合物前体的方法
公开(公告)号：US4350781A
公开(公告)日：1982-09-21
申请号：US286419
申请日：1981-07-24
申请人： Werner Rasshofer , Gerhard Grogler , Holger Meyborg
发明人： Werner Rasshofer , Gerhard Grogler , Holger Meyborg
IPC分类号： C07D263/62 , C08G18/10 , C08G18/38 , C08G18/80 , C08G18/32
CPC分类号： C07D263/62 , C08G18/10 , C08G18/3844 , C08G18/80
摘要： A polymer precursor containing an oxazolin-2-one ring is made by reacting (a) an amino-reactive group containing compound having at least two groups capable of entering into an addition or condensation reaction with primary or secondary aromatically-bound amino groups with (b) an aromatic amine having at least one primary or secondary aromatically-bound amino group and at least one condensed oxazolin-2-one ring. The reactants are used in quantities such that for each aromatically bound primary or secondary amino group there are from 0.95 to 5 groups present in the amino-reactive group containing compound which are capable of reacting with the amino group. These polymer precursors may be used to produce high molecular weight polymers useful in the production of solid molded products, adhesives, foam plastics and coatings.
摘要翻译：含有恶唑啉-2-酮环的聚合物前体是通过使（a）具有至少两个能够与伯或仲芳族结合的氨基进行加成或缩合反应的基团的含氨基反应性基团的化合物与（ b）具有至少一个伯或仲芳族结合的氨基和至少一个稠合的恶唑啉-2-酮的芳族胺。反应物的用量使得对于每个芳香结合的伯或仲氨基，在含有氨基反应性基团的化合物中存在0.95至5个能够与氨基反应的基团。这些聚合物前体可用于生产用于生产固体模制产品，粘合剂，泡沫塑料和涂料的高分子量聚合物。

26. 发明授权

US4305991A Integral-skin polyurethane foams and process therefor 失效
标题翻译：整体皮肤聚氨酯泡沫及其工艺
公开(公告)号：US4305991A
公开(公告)日：1981-12-15
申请号：US135817
申请日：1980-03-31
申请人： Holger Meyborg , Werner Mormann , Hans-Walter Illger , Manfred Bock
发明人： Holger Meyborg , Werner Mormann , Hans-Walter Illger , Manfred Bock
IPC分类号： C08G18/32 , C08G18/38 , C08G18/66 , C08G18/14 , B32B5/14 , C08G18/16 , C08G18/30
CPC分类号： C08G18/3271 , C08G18/3831 , C08G18/6688 , Y10S264/14 , Y10T428/249989 , Y10T428/31554
摘要： The instant invention relates to a process for the production of polyurethane foams by reacting polyisocyanates with polyhydroxyl compounds of a specified molecular weight range in the presence of blowing agents and chain lengthening or cross-linking agents and optionally in the presence of catalysts, foam stabilizers and other additives generally known. The improvement resides in(a) the polyisocyanates used containing aliphatically and/or cycloaliphatically bound isocyanate groups;(b) the polyhydroxyl compounds used containing ether groups; and(c) the chain lengthening or cross-linking agents comprising at least in part a member selected from the group consisting of a monoalkoxylated hydrazine, a dialkoxylated hydrazine, a reaction product of a monoalkoxylated or dialkoxylated hydrazine with an aliphatic monoisocyanate in a molar ratio of 1:1. The reaction is carried out in the presence of additional chain lengthening agents having a specified molecular weight. The present invention also relates to polyurethane foams obtained by this process.
摘要翻译：本发明涉及通过使多异氰酸酯与特定分子量范围的多羟基化合物在发泡剂和链延长或交联剂的存在下以及任选地在催化剂，泡沫稳定剂和其他通常已知的添加剂。改进在于（a）含有脂族和/或环状结合的异氰酸酯基团的多异氰酸酯; （b）含有醚基的多羟基化合物; 链长度或交联剂至少包括选自单烷氧基化肼，二烷氧基化肼，单烷氧基化或二烷氧基化肼与脂族单异氰酸酯的反应产物的摩尔比为1：1。该反应在具有特定分子量的另外的链延长剂的存在下进行。本发明还涉及通过该方法获得的聚氨酯泡沫。

27. 发明授权

US4303773A Process for the production of polyurethane urea elastomers 失效
标题翻译：生产聚氨酯脲弹性体的方法
公开(公告)号：US4303773A
公开(公告)日：1981-12-01
申请号：US148109
申请日：1980-05-09
申请人： Otto Ganster , Hans J. Meiners , Willi Eifler , Holger Meyborg , Jurgen Schwindt
发明人： Otto Ganster , Hans J. Meiners , Willi Eifler , Holger Meyborg , Jurgen Schwindt
IPC分类号： C08G18/00 , C08G18/10 , C08G18/28 , C08G18/32 , C08G18/54 , C08G18/65 , C08G18/16 , C08G18/24
CPC分类号： C08G18/6529 , C08G18/10 , C08G18/2805 , C08G18/3243 , C08G2120/00 , Y10S528/906
摘要： This invention relates to a process for the production of non-cellular polyurethane ureas elastomers using a chain-extender mixture produced from asymmetrically alkyl-substituted anilines by condensation with formaldehyde. The chain-extending agents used in the instant invention show medium reactivity to compounds containing isocyanate groups. These chain-extending agents may be processed both in high-pressure and in low-pressure metering and mixing units because they are either liquid at room temperature or can be melted at relatively low temperatures (below 55.degree. C.). The homogeneous, i.e. non-cellular, polyurethane urea elastomers obtained in the instant invention are distinguished by having excellent mechanical properties.
摘要翻译：本发明涉及使用由不对称烷基取代的苯胺与甲醛缩合制备的扩链剂混合物生产非细胞聚氨酯脲醛弹性体的方法。用于本发明的增链剂显示出对含有异氰酸酯基团的化合物的介质反应性。这些增链剂可以在高压和低压计量和混合单元中进行加工，因为它们在室温下是液体的，或者可以在相对低的温度（低于55℃）下熔化。通过具有优异的机械性能来区分在本发明中获得的均匀的，即非细胞的聚氨酯脲弹性体。

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