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21. 发明授权

US4537595A Organopolysiloxanes with Bunte salt groups, their synthesis and use for the surface treatment of inorganic or organic materials 失效
标题翻译：具有Bunte盐基的有机聚硅氧烷，它们的合成和用于无机或有机材料的表面处理
公开(公告)号：US4537595A
公开(公告)日：1985-08-27
申请号：US625711
申请日：1984-06-28
申请人： Burghard Gruning , Ulrich Holtschmidt , Gotz Koerner
发明人： Burghard Gruning , Ulrich Holtschmidt , Gotz Koerner
IPC分类号： C08G77/28 , C08G77/392 , D06M15/647 , D21H17/59 , D06M3/06 , C07F7/08 , D06M13/26 , D21F11/14
CPC分类号： C08G77/392 , C08G77/28 , D06M15/647 , D21H17/59 , Y10T428/31663
摘要： Organopolysiloxanes with Bunte salt groups having the formula ##EQU1## the Bunte salt groups being linked to a silicon atom by way of a carbon atom and in whichR.sup.1 is methyl with the proviso that up to 10% of the R.sup.1 groups may be alkyl with up to 18 carbon atoms or vinyl phenyl, hydrogen or hydroxyl,R.sup.2 is the ##STR1## group or the ##STR2## group, in which one of the R.sup.3, R.sup.4 groups represents an OH group and the other an --S.sub.2 O.sub.3 Me group (Me=alkali or the optionally substituted ammonium group), whereby the R.sup.3 and R.sup.4 radicals can be hydroxyl or together the oxygen of an oxirane ring in an amount up to 50% of the R.sup.2 group,a has any value from 1 to 2.33 andb has any value from 0.02 to 1.The compounds can be synthesized from the corresponding organopolysiloxanes having epoxy groups by reaction with alkali or ammonium thiosulfate and used for the surface treatment of inorganic or organic materials, for example, textiles, paper or rock wool.
摘要翻译：具有下式的Bunte盐基的有机聚硅氧烷是Bunte盐基团通过碳原子连接到硅原子，其中R 1是甲基，条件是高达10％的R 1基团可以是烷基与最多18个碳原子或乙烯基苯基，氢或羟基，R2是基团或基团，其中R3，R4中的一个代表OH基团，另一个代表-S2O3Me基团（Me = 碱或任选取代的铵基），其中R 3和R 4基团可以是高达50％的R2基团的羟基或环氧乙烷环的氧，a具有1至2.33的任何值，b具有任何值为0.02至1.该化合物可以通过与硫代硫酸铵或硫代硫酸铵反应而由相应的具有环氧基的有机聚硅氧烷合成，并用于无机或有机材料如纺织品，纸或岩棉的表面处理。

22. 发明授权

US4281147A Process for the production of aqueous solutions of alkali organosiliconates 失效
标题翻译：生产碱有机硅酸盐水溶液的方法
公开(公告)号：US4281147A
公开(公告)日：1981-07-28
申请号：US126389
申请日：1980-03-03
申请人： Gotz Koerner , Vaclav Kropac , Harald Rau
发明人： Gotz Koerner , Vaclav Kropac , Harald Rau
IPC分类号： C07F7/18 , C08G77/398 , C07F7/04 , C07F7/08
CPC分类号： C07F7/1868 , C08G77/398
摘要： A process for the preparation of aqueous solutions of alkali organosiliconates in which organoalkoxypolysiloxanes of the formula ##EQU1## in which R.sup.1 is an alkyl residue with 1 to 3 carbon atoms, a vinyl residue and/or a phenyl residue,R.sup.2 is an alkyl residue with 1 to 4 carbon atoms,a is a number .ltoreq.2, andx is 1 to 1.25,are reacted with aqueous solutions of sodium hydroxide or potassium hydroxide having a concentration of 0.7 to 0.9 mole/100 g at temperatures .gtoreq.80.degree. C. The liberated alcohol R.sup.2 OH may be distilled and/or the concentration adjusted to the desired value by the addition of water. With the present invention, alkali chloride-free alkali organosiliconate solutions having high concentration can be obtained while avoiding a filtration step.
摘要翻译：一种制备碱有机硅酸盐的水溶液的方法，其中式为“IMAGE”的有机烷氧基聚硅氧烷，其中R 1为具有1至3个碳原子的烷基残基，乙烯基残基和/或苯基残基，R2为烷基残基， 1至4个碳原子，a为数2，x为1至1.25，在温度≥80℃下与浓度为0.7至0.9摩尔/ 100g的氢氧化钠或氢氧化钾的水溶液反应可以将释放的醇R2OH蒸馏和/或通过加入水将浓度调节至所需值。通过本发明，可以在避免过滤步骤的同时获得高浓度的无碱金属氯化物的有机硅酸盐溶液。

23. 发明授权

US4248590A Preparation for shrinkproofing wool 失效
标题翻译：羊毛防缩制备
公开(公告)号：US4248590A
公开(公告)日：1981-02-03
申请号：US20024
申请日：1979-03-13
申请人： Gotz Koerner , Gunter Schmidt , Friedhelm Nickel
发明人： Gotz Koerner , Gunter Schmidt , Friedhelm Nickel
IPC分类号： D06M13/02 , D06M13/51 , D06M13/513 , D06M15/643 , D06M101/00 , D06M101/02 , D06M101/10 , D06M101/12 , D06M15/66 , C08L83/08 , D06M3/00 , D06M13/26
CPC分类号： D06M15/6433 , Y10S8/01
摘要： A preparation for shrinkproofing wool composed of 1 to 50 weight percent of organopolysiloxanes composed of 90 to 99.8 mole % of units having the formula R.sub.n.sup.1 SiO.sub.(4-n)/2, and 0.2 to 10 mole % of units having the formula R.sup.2 SiO.sub.3/2 with the remainder being water and other conventional additives. These preparations provide emulsions which are stable over long periods of time, do not precipitate even in the presence of moisture, provide durable shrinkproof properties to wool, and have no adverse effect on the "hand" of the wool.
摘要翻译：一种由1〜50重量％的由90〜99.8摩尔％的具有式Rn1SiO（4-n）/ 2的单元组成的有机聚硅氧烷和0.2〜10摩尔％的具有式R 2 SiO 3/2的单元与其余为水和其他常规添加剂。这些制剂提供长时间稳定的乳液，即使在水分存在下也不会沉淀，对羊毛提供耐久的防缩性能，并且对羊毛的“手”没有不利影响。

24. 发明授权

US4137179A Process for the production of an aqueous preparation for shrink-proofing wool 失效
标题翻译：用于生产用于防皱羊毛的水性制剂的方法
公开(公告)号：US4137179A
公开(公告)日：1979-01-30
申请号：US814911
申请日：1977-07-12
申请人： Gotz Koerner , Hans-Jurgen Patzke
发明人： Gotz Koerner , Hans-Jurgen Patzke
IPC分类号： D06M15/643 , D06M101/00 , D06M101/02 , D06M101/10 , D06M13/10
CPC分类号： D06M15/6436 , Y10T428/31663
摘要： A new method for producing a stable, aqueous preparation of compounds which are organosiloxanes having amino groups attached to the silicon atoms which are used for the shrink-proofing of wool which preparations contain silanes which may be aminodi- or trialkoxysilanes is disclosed. Composition and the method of treatment of wool are also disclosed. Wool treated with the preparations exhibit excellent decreased shrinkage as well as an absence of felting.
摘要翻译：公开了一种用于制备稳定的含水制剂的化合物的新方法，其为具有连接到硅原子上的氨基的有机硅氧烷，其用于羊毛的防缩，该制剂含有可以是氨基或三烷氧基硅烷的硅烷。还公开了羊毛的组合物和处理方法。用该制剂处理的羊毛显示出优异的减少的收缩率和不存在毡化。

25. 发明授权

US5198207A Method for the preparation of active magnesium hydride-magnesium hydrogen storage systems, which reversibly absorb hydrogen 失效
标题翻译：制备活性镁氢镁储存系统的方法，其中可逆的氢吸收氢
公开(公告)号：US5198207A
公开(公告)日：1993-03-30
申请号：US785298
申请日：1991-10-30
申请人： Wilfried Knott , Klaus-Dieter Klein , Gotz Koerner
发明人： Wilfried Knott , Klaus-Dieter Klein , Gotz Koerner
IPC分类号： B01J31/12 , B01J23/02 , C01B3/00 , C01B6/04
CPC分类号： C01B3/0026 , Y02E60/327 , Y10S420/90 , Y10S502/526
摘要： A method is disclosed for the preparation of active magnesium hydride-magnesium-hydrogen storage systems, which reversibly absorb hydrogen, with addition of a catalyst for the absorption of hydrogen with the formation of hydride. Magnesium hydride particles.ltoreq.400 .mu.m in diameter are added in an amount of at least 1.2% by weight, based on the magnesium to be hydrogenated, as catalyst during the first hydrogenation to the finely divided magnesium to be hydrogenated. The hydrogenation is carried out at a temperature of .gtoreq.250.degree. C. and a pressure of 0.5 to 5 MPa. The method is carried out with intensive stirring of the material that is being reacted.
摘要翻译：公开了一种用于制备活性氢化镁 - 镁 - 氢储存系统的方法，其可逆地吸收氢气，加入催化剂以形成氢化物吸收氢气。加入直径为400μm的氢化镁颗粒，以加氢镁为至少1.2重量％，在第一次氢化期间作为催化剂加入被细化的被氢化的镁。氢化在≥250℃的温度和0.5-5MPa的压力下进行。该方法是在剧烈搅拌下进行反应的材料。

26. 发明授权

US5091002A Preparation for the water-repellent impregnation of porous mineral building materials 失效
标题翻译：多孔矿物建筑材料的水分蚀刻制备
公开(公告)号：US5091002A
公开(公告)日：1992-02-25
申请号：US492086
申请日：1990-03-12
申请人： Eckehard Schamberg , Gotz Koerner , Herwig Fritsch , Manfred Grasse , Roland Sucker
发明人： Eckehard Schamberg , Gotz Koerner , Herwig Fritsch , Manfred Grasse , Roland Sucker
IPC分类号： C04B41/49 , C04B41/64
CPC分类号： C04B41/009 , C04B41/4961 , C04B41/64
摘要： A composition is disclosed which is useful for the water-repellent impregnation of porous mineral building materials. The composition is based on organosilicon compounds which contain alkoxy groups and comprises an emulsion which contains 2.5 to 25% by weight of an alkoxysilane of the formulaR.sup.1 -Si(OR.sup.2).sub.3whereinR.sup.1 is an alkyl group with 3 to 12 carbon atoms andR.sup.2 is a methyl or ethyl group, 2 to 20% by weight of an alkoxysiloxane of the formula ##STR1## wherein R.sup.3 is an alkyl group with 1 to 6 carbon atomsa is 0.8 to 1.2 andb is 0.2 to 1.2,0.01 to 5% by weight of an emulsifier, 0.01 to 0.1% by weight of fillers with an effective surface area of at least 40 m.sup.2 /g and 49.9 to 95.48% by weight of water. The composition has a long shelf life and, due to its high penetration, a high water-repellent effect on the surface, as well as deep within, all mineral building materials.
摘要翻译：公开了一种可用于多孔矿物建筑材料的拒水浸渍的组合物。该组合物基于含有烷氧基的有机硅化合物，并且包含含有2.5至25重量％的式R 1 -Si（OR 2）3的烷氧基硅烷的乳液，其中R 1是具有3至12个碳原子的烷基和R 2 是甲基或乙基，2-20重量％的下式的烷氧基硅氧烷，其中R3是具有1-6个碳原子的烷基，a是0.8-1.2，b是0.2-1.2,0.01到5％的乳化剂，0.01至0.1重量％的有效表面积为至少40m 2 / g和49.9至95.48％（重量）的水的填料。该组合物具有长的保存期限，并且由于其高渗透性，对所有矿物建筑材料的表面以及内部均具有高的防水效果。

27. 发明授权

US4988806A Nitrogen-containing derivatives of carboxymethylcellulose, their synthesis and their use in cosmetic preparations 失效
标题翻译：羧甲基纤维素的含氮衍生物，其合成及其在化妆品制剂中的应用
公开(公告)号：US4988806A
公开(公告)日：1991-01-29
申请号：US365612
申请日：1989-06-13
申请人： Burghard Gruning , Klaus Hoffmann , Gotz Koerner , Hans-Joachim Kollmeier
发明人： Burghard Gruning , Klaus Hoffmann , Gotz Koerner , Hans-Joachim Kollmeier
IPC分类号： A61K8/73 , A61Q5/00 , A61Q5/02 , C08B11/14 , C08B11/20 , D21H17/26
CPC分类号： A61Q5/00 , A61K8/731 , A61Q5/02 , C08B11/14 , C08B11/20 , D21H17/26 , A61K2800/5426 , Y10S514/88
摘要： Derivatives of carboxymethylcellulose are disclosed in which all or a portion of the carboxymethyl groups are replaced by groups of the general formula ##STR1## in which R.sup.1 is a hydrogen or methyl group,R.sup.2 is a divalent aliphatic hydrocarbon group with 2 to 5 carbon atoms,R.sup.3, R.sup.4 are alkyl groups with 1 to 4 carbon atoms,R.sup.5 is an alkyl group with 1 to 4 carbon atoms or a benzyl group,X is a halogen or sulfate group or a sulfonic acid group,with the proviso that, on the average, at least 0.1 quaternary ammonium groups are contained per anhydroglucose unit of the polymeric molecule.The invention furthermore relates to derivatives of carboxymethylcellulose, in which all or a portion of the carboxymethyl groups are replaced by groups of the general formula ##STR2## in which the substituents R.sup.1, R.sup.2, R.sup.3 and R.sup.4 have the above meaning, with the proviso that, on the average, at least 0.1 tertiary amino groups are contained per anhydroglucose unit of the polymeric molecule, as intermediates for the synthesis of the aforementioned derivatives.The invention furthermore is directed to a method for the synthesis of the derivatives of carboxymethylcellulose and their use in cosmetic preparations, especially for the care of hair.
摘要翻译：公开了羧甲基纤维素的衍生物，其中全部或部分羧甲基被R 1为氢或甲基的通式为“IMAGE”的基团取代，R 2为具有2至5个碳原子的二价脂族烃基， R3，R4是具有1至4个碳原子的烷基，R5是具有1至4个碳原子的烷基或苄基，X是卤素或硫酸根或磺酸基，条件是平均，聚合物分子中每个脱水葡萄糖单元含有至少0.1个季铵基团。本发明还涉及羧甲基纤维素的衍生物，其中全部或部分羧甲基被由通式“IMAGE”的基团取代，其中取代基R 1，R 2，R 3和R 4具有上述含义，条件是平均来说，作为合成上述衍生物的中间体，聚合物分子中每个脱水葡萄糖单元含有至少0.1个叔氨基。此外，本发明涉及一种合成羧甲基纤维素衍生物的方法及其在化妆品制剂中的用途，特别是用于护理头发。

28. 发明授权

US4844980A Silica or silicic acid particles whose surface located hydroxyl groups are at least partially replaced by organic groups 失效
标题翻译：其表面位于羟基的二氧化硅或硅酸颗粒至少部分被有机基团取代
公开(公告)号：US4844980A
公开(公告)日：1989-07-04
申请号：US43100
申请日：1987-04-24
申请人： Burghard Gruning , Ulrich Holtschmidt , Gotz Koerner , Gerd Rossmy
发明人： Burghard Gruning , Ulrich Holtschmidt , Gotz Koerner , Gerd Rossmy
IPC分类号： B01D17/04 , B01D17/05 , B01D19/04 , C01B33/18 , C09C1/30 , C10G33/04
CPC分类号： C10G33/04 , B01D17/047 , B01D19/0409 , C01B33/181 , C09C1/3081 , C01P2006/80 , Y10T428/2995 , Y10T428/31663
摘要： Silicic acid or silica particles having initially surface-located hydroxyl groups are modified by replacing at least partially the hydroxyl groups by an organic group to impart the particles with emulsion-breaking and foam-destroying properties. Processes for preparing the modified particles are also disclosed.
摘要翻译：具有最初表面定位的羟基的硅酸或二氧化硅颗粒是通过用有机基团至少部分取代部分羟基进行改性的，以使颗粒具有破乳和泡沫破坏性能。还公开了制备改性颗粒的方法。

29. 发明授权

US4781950A Method for impregnating mineral building materials 失效
标题翻译：浸渍矿物建筑材料的方法
公开(公告)号：US4781950A
公开(公告)日：1988-11-01
申请号：US79652
申请日：1987-07-30
申请人： Herbert Giesing , Gotz Koerner , Eckehard Schamberg , Jakob Wassermeyer , Christian Weitemeyer
发明人： Herbert Giesing , Gotz Koerner , Eckehard Schamberg , Jakob Wassermeyer , Christian Weitemeyer
IPC分类号： B01J19/18 , C04B41/49 , B05D1/02
CPC分类号： C04B41/4966 , B01J19/18 , B01J2219/00164 , B01J2219/00182 , B01J2219/185
摘要： Method for impregnating mineral building materials, with aqueous solutions of silanols and/or siloxanols is disclosed. The solution is obtained by continuous hydrolysis of alkoxysilanes and/or alkoxysiloxanes, of the general formula ##EQU1## wherein R.sup.1 =alkyl with 1 to 8 carbon atoms, at least 90% of the R.sup.1 groups in the average molecule being alkyl groups with 1 to 4 carbon atoms,R.sup.2 =methyl or ethyl,a=0 to 1.5,b=1.0 to 4.0,a+b=2.0 to 4.0in an amount corresponding to the expected consumption. The solution obtained is applied on the mineral building material within 3 to 30 minutes after the reactants are mixed. Suitable hydrolysis apparatus is also disclosed.
摘要翻译：公开了用硅烷醇和/或硅氧烷醇水溶液浸渍矿物建筑材料的方法。该溶液通过连续水解通式为“IMAGE”的烷氧基硅烷和/或烷氧基硅氧烷获得，其中R1 =具有1-8个碳原子的烷基，平均分子中至少90％的R 1基团是烷基，其中1至 4个碳原子，R2 =甲基或乙基，a = 0至1.5，b = 1.0至4.0，a + b = 2.0至4.0，其数量对应于预期的消耗量。将所得溶液在反应物混合后3至30分钟内施用于矿物建筑材料上。还公开了合适的水解装置。

30. 发明授权

US4749764A Process for the preparation of heat-curable silicone 失效
标题翻译：制备可热固化硅酮的方法
公开(公告)号：US4749764A
公开(公告)日：1988-06-07
申请号：US51244
申请日：1987-05-13
申请人： Gotz Koerner , Vaclav Kropac
发明人： Gotz Koerner , Vaclav Kropac
IPC分类号： C08G77/00 , C08G77/18 , C08G77/22 , C08G77/38 , C08G77/50 , C08G77/06
CPC分类号： C08G77/38 , C08G77/18 , C08G77/50
摘要： A method for preparing heat-curable silicone resins by reacting siloxanes with low molecular, multifunctional alcohol and removing the alcohol from the reaction mixture such that each siloxane group corresponds to approximately one alcohol group and terminating the reaction at a degree of conversion of 25% to 80% by cooling the reaction mixture to a temperature of less than 100.degree. C. The silicone resins prepared according to this process have excellent storage stability in the uncured state, a high rate of curing and excellent pigment compatibility and the cured resins possess high thermal stability with good elasticity and good adhesion to metallic substrates.
摘要翻译：一种通过使硅氧烷与低分子量多官能醇反应并从反应混合物中除去醇而制备可热固化的有机硅树脂的方法，使得每个硅氧烷基团对应于大约一个醇基团，并以25％的转化率终止反应，通过将反应混合物冷却至低于100℃的温度，可以得到80％。根据该方法制备的有机硅树脂在未固化状态下具有优良的储存稳定性，高固化速度和优异的颜料相容性以及固化树脂具有高热稳定性好，弹性好，对金属基材的附着力好。

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