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21. 发明授权

US4400523A Process for the preparation of styryl-cyclopropanecarboxylic acid esters and new intermediate products for this process 失效
标题翻译：制备苯乙烯基 - 环丙烷羧酸酯的方法和该方法的新中间产物
公开(公告)号：US4400523A
公开(公告)日：1983-08-23
申请号：US319768
申请日：1981-11-09
申请人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
发明人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
IPC分类号： C07C313/00 , A01N53/00 , A01N53/08 , A01N53/10 , C07C59/64 , C07C67/00 , C07C69/757 , C07C319/20 , C07C323/62 , C07D307/33 , C07D307/04 , C07D307/12
CPC分类号： C07D307/33 , A01N53/00 , C07C59/64
摘要： A process for the preparation of a styryl-cyclopropane-carboxylic acid ester of the formula ##STR1## in which R is C.sub.1-4 -alkyl or an alcohol radical customary in pyrethroids,R.sup.1 is alkoxy or alkylthio, either of which may be optionally substituted by halogen,R.sup.2 is hydrogen or alkoxy, orR.sup.1 and R.sup.2 together are optionally halogen-substituted alkylenedioxy, andR.sup.3 is hydrogen or chlorine, comprising reacting a compound of the formula ##STR2## with, respectively, one, two or three equivalents of a base at a temperature below 60.degree. C. The products are insecticidally active when R is the residue of a pyrethroid-type alcohol. Various syntheses are given for the starting materials which are new.
摘要翻译：制备式IMAMA的苯乙烯基 - 环丙烷 - 羧酸酯的方法，其中R是C1-4烷基或拟除虫菊酯中通常的醇基，R 1是烷氧基或烷硫基，其中任一个可以任选被取代通过卤素，R 2是氢或烷氧基，或者R 1和R 2一起是卤素取代的亚烷基二氧基，并且R 3是氢或氯，包括分别将下式的化合物与其反应：一个，两个或三个当量的碱在温度低于60℃。当R是拟除虫菊酯型酒精的残留物时，产物具有杀虫活性。给出了新的起始材料的各种合成。

22. 发明授权

US4318783A Process for the preparation of optionally substituted benzaldehyde dialkyl acetals 失效
标题翻译：制备任选取代的苯甲醛二烷基缩醛的方法
公开(公告)号：US4318783A
公开(公告)日：1982-03-09
申请号：US94132
申请日：1979-11-14
申请人： Hans-Rolf Buhmann , Dieter Arlt , Manfred Jautelat
发明人： Hans-Rolf Buhmann , Dieter Arlt , Manfred Jautelat
IPC分类号： C25B3/02
CPC分类号： C25B3/02 , Y02P20/582
摘要： An electrochemical oxidation process of optionally substituted toluene dissolved in an alcohol in the presence of a conducting salt is described wherein the electrochemical oxidation is carried out at a current density of 0.1 to 50 A/dm.sup.2 using oxidation-resistant anodes. According to the disclosure, the reaction product can be distillatively worked up to obtain secondary products which can be recycled to electrochemical oxidation optionally after treatment of at least some of the secondary products with hydrogen in the presence of a catalyst.
摘要翻译：描述了在导电盐存在下溶解在醇中的任选取代的甲苯的电化学氧化方法，其中使用耐氧化阳极以0.1至50A / dm 2的电流密度进行电化学氧化。根据公开内容，可以蒸馏处理反应产物以获得可在催化剂存在下用氢气处理至少一些次级产物之后任意再循环至电化学氧化的二次产物。

23. 发明授权

US5110975A Isocyanatoalkyl sulphonates and a process for their preparation 失效
标题翻译：异硫氰酸钠及其制备方法
公开(公告)号：US5110975A
公开(公告)日：1992-05-05
申请号：US626493
申请日：1990-12-12
申请人： Georg Schroeder , Dieter Arlt , Manfred Jautelat
发明人： Georg Schroeder , Dieter Arlt , Manfred Jautelat
IPC分类号： C07C309/63 , C07C309/65
CPC分类号： C07C309/65 , C07C309/63
摘要： Isocyanatoalkyl sulphonates of the general formula ##STR1## wherein the substituent meanings are as given in the description are obtained by reacting the corresponding isocyanatoalkyl halides with sulphonic acid esters of the formula ##STR2## wherein R.sup.3 has the meanings given in the description. They are used as cross-linking agents in polyamines.
摘要翻译：通过使相应的异氰酸根合烷基卤化物与下式的磺酸酯反应，其中R 3具有说明书中给出的含义，得到通式为其中取代基含义如本说明书中给出的通式为其的异氰酸烷基磺酸盐。它们用作多胺中的交联剂。

24. 发明授权

US4384114A Styryl substituted .GAMMA.-lactone derivatives 失效
标题翻译：苯乙烯基取代的GAMMA-内酯衍生物
公开(公告)号：US4384114A
公开(公告)日：1983-05-17
申请号：US320622
申请日：1981-11-12
申请人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
发明人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
IPC分类号： A01N53/00 , A01N53/08 , A01N53/10 , B01J31/00 , C07C41/30 , C07C43/225 , C07C45/00 , C07C47/277 , C07C67/00 , C07C69/757 , C07C253/00 , C07C255/39 , C07C313/00 , C07C319/20 , C07C323/62 , C07D303/08 , C07D307/33 , C07D317/52 , C07D317/60 , C07D407/06 , C07F9/40 , C07D307/32
CPC分类号： C07D307/33 , C07C41/30 , C07C45/00 , C07C47/277 , C07D303/08 , C07D317/52 , C07D407/06 , C07F9/4056
摘要： A process for the preparation of a styryl-cyclopropane-1-carboxylic acid ester of the formula ##STR1## in which R is C.sub.1-4 -alkyl or an alcohol radical customary in pyrethroids,R.sup.1 is alkoxy or alkylthio, either of which may be optionally substituted by halogen,R.sup.2 is hydrogen or alkoxy, orR.sup.1 and R.sup.2 together are optionally halogen-substituted alkylenedioxy, andR.sup.3 is hydrogen or chlorine,comprising reacting an ester of the formula ##STR2## in which Hal is chlorine or bromine, with a base. The compounds are insecticidally active. Numerous syntheses of the starting materials, some involving new intermediates, are also shown.
摘要翻译：制备式“IMAGE”的苯乙烯基 - 环丙烷-1-羧酸酯的方法，其中R是C1-4烷基或拟除虫菊酯中通常的醇基，R1是烷氧基或烷硫基，其中任一个可以是任选地被卤素取代，R 2是氢或烷氧基，或者R 1和R 2一起是卤素取代的亚烷基二氧基，并且R 3是氢或氯，包括使其中Hal是氯或溴的式“IMAGE”的酯与基础。这些化合物具有杀虫活性。还显示了许多合成原料，一些涉及新的中间体。

25. 发明授权

US4327025A Preparation of styryl-cyclopropane-carboxylic acid esters and intermediate therefor 失效
标题翻译：苯乙烯基 - 环丙烷 - 羧酸酯的制备及其中间体
公开(公告)号：US4327025A
公开(公告)日：1982-04-27
申请号：US137685
申请日：1980-04-07
申请人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
发明人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
IPC分类号： A01N53/00 , A01N53/08 , A01N53/10 , B01J31/00 , C07C41/30 , C07C43/225 , C07C45/00 , C07C47/277 , C07C67/00 , C07C69/757 , C07C253/00 , C07C255/39 , C07C313/00 , C07C319/20 , C07C323/62 , C07D303/08 , C07D307/33 , C07D317/52 , C07D317/60 , C07D407/06 , C07F9/40 , C07D325/00 , C07C69/76 , C07C121/60 , C07D317/44
CPC分类号： C07D307/33 , C07C41/30 , C07C45/00 , C07C47/277 , C07D303/08 , C07D317/52 , C07D407/06 , C07F9/4056
摘要： A process for the preparation of a styrylcyclopropane-1-carboxylic acid ester of the formula ##STR1## in which R is C.sub.1-4 -alkyl or an alcohol radical customary in pyrethroids,R.sup.1 is alkoxy or alkylthio, either of which may be optionally substituted by halogen,R.sup.2 is hydrogen or alkoxy, orR.sup.1 and R.sup.2 together are optionally halogen-substituted alkylenedioxy, andR.sup.3 is hydrogen or chlorine,comprising reacting an ester of the formula ##STR2## in which Hal is chlorine or bromine,with a base.The compounds are insecticidally active. Numerous syntheses of the starting materials, some involving new intermediates, are also shown.
摘要翻译：制备式“IMAGE”的苯乙烯基环丙烷-1-羧酸酯的方法，其中R是C1-4烷基或在除虫菊酯中通常的醇基，R 1是烷氧基或烷硫基，其中任一个可以任选地被取代通过卤素，R 2是氢或烷氧基，或者R 1和R 2一起是卤素取代的亚烷基二氧基，并且R 3是氢或氯，包括使Hal是氯或溴的式“IMAGE”的酯与碱反应。这些化合物具有杀虫活性。还显示了许多合成原料，一些涉及新的中间体。

26. 发明授权

US4325873A Process for the preparation of styryl-cyclopropanecarboxylic acid esters and intermediate products for this process 失效
标题翻译：用于制备苯乙烯基 - 环丙烷羧酸酯和该方法的中间产物的方法
公开(公告)号：US4325873A
公开(公告)日：1982-04-20
申请号：US138044
申请日：1980-04-07
申请人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
发明人： Manfred Jautelat , Dieter Arlt , Reinhard Lantzsch , Rainer Fuchs , Hans-Jochem Riebel , Rolf Schroder , Horst Harnisch
IPC分类号： C07C313/00 , A01N53/00 , A01N53/08 , A01N53/10 , C07C59/64 , C07C67/00 , C07C69/757 , C07C319/20 , C07C323/62 , C07D307/33 , C07D325/00 , C07C51/58 , C07C121/60 , C07D317/44
CPC分类号： C07D307/33 , A01N53/00 , C07C59/64
摘要： A process for the preparation of a styryl-cyclopropane-carboxylic acid ester of the formula ##STR1## in which R is C.sub.1-4 -alkyl or an alcohol radical customary in pyrethroids,R.sup.1 is alkoxy or alkylthio, either of which may be optionally substituted by halogen,R.sup.2 is hydrogen or alkoxy, orR.sup.1 and R.sup.2 together are optionally halogen-substituted alkylenedioxy, andR.sup.3 is hydrogen or chlorine, comprising reacting a compound of the formula ##STR2## with, respectively, one, two or three equivalents of a base at a temperature below 60.degree. C. The products are insecticidally active when R is the residue of a pyrethroid-type alcohol. Various syntheses are given for the starting materials which are new.
摘要翻译：制备式IMAMA的苯乙烯基 - 环丙烷 - 羧酸酯的方法，其中R是C1-4烷基或拟除虫菊酯中通常的醇基，R 1是烷氧基或烷硫基，其中任一个可以任选被取代通过卤素，R 2是氢或烷氧基，或者R 1和R 2一起是任选的卤素取代的亚烷基二氧基，并且R 3是氢或氯，包括分别将下式的化合物（IMAGE），IMAGE ，两个或三当量的碱在温度低于60℃。当R是拟除虫菊酯型醇的残基时，产物具有杀虫活性。给出了新的起始材料的各种合成。

27. 发明授权

US4283544A Preparation of 2-(2,2-dimethyl-3-buten-1-yl)-2-oxazolines 失效
标题翻译：制备2-（2,2-二甲基-3-丁烯-1-基）-2-恶唑啉
公开(公告)号：US4283544A
公开(公告)日：1981-08-11
申请号：US15376
申请日：1979-02-26
申请人： Manfred Jautelat , Dieter Arlt
发明人： Manfred Jautelat , Dieter Arlt
IPC分类号： C07D263/04 , C07D263/12 , C07D263/14
CPC分类号： C07D263/04 , C07D263/12
摘要： A process comprising reacting a 2-methyloxazoline of the formula ##STR1## in which R.sup.1, R.sup.2, R.sup.3 and R.sup.4 each indpendently is hydrogen, alkyl, aralkyl, optionally substituted aryl or two of them together form a ring,with a 3-methyl-2-buten-1-yl derivative of the formula ##STR2## in which X is halide, sulphonate or phosphate,thereby to produce a 2-methyl-3-(3-methyl-2-butenyl)-2-oxazolinium salt of the formula ##STR3## reacting the oxazolinium salt with an alcoholate of the formulaR.sup.5 --O--M (V)in whichM is a one equivalent of an alkali metal or alkaline earth metal cation,to produce an oxazolidine of the formula ##STR4## pyrolyzing the oxazolidine to produce a 2-methylene-3-(3-methyl-2-butenyl)-oxazolidine of the formula and heating the 2-methylene-3-(3-methyl-2-butenyl)-oxazolidine to produce a 2-(2,2-dimethyl-3-buten-1-yl)-2-oxazoline of the formula ##STR5## The compounds (II), (III) and (IV) are new.
摘要翻译：一种方法包括使式（VI）的2-甲基恶唑啉（其中R 1，R 2，R 3和R 4各自独立地为氢，烷基，芳烷基，任选取代的芳基或其中的两个一起形成环）与3 （VII）的2-甲基-2-丁烯-1-基衍生物，其中X是卤化物，磺酸盐或磷酸盐，从而产生2-甲基-3-（3-甲基-2-丁烯基） - 式（Ⅳ）的2-恶唑啉盐使恶唑啉盐与式为R5-OM（Ⅴ）的醇化物反应，其中M为1当量碱金属或碱土金属阳离子，以产生恶唑烷（III）热解恶唑烷以制备式（II）的2-亚甲基-3-（3-甲基-2-丁烯基） - 恶唑烷并加热2-亚甲基-3- （3-甲基-2-丁烯基） - 恶唑烷以制备下式的2-（2,2-二甲基-3-丁烯-1-基）-2-恶唑啉（I）化合物（II），（三）和（四）是新的。

28. 发明授权

US4216162A Novel derivatives of cyclopropanecarboxylic acid useful as intermediates for the preparation of insecticides 失效
标题翻译：环丙烷羧酸的新型衍生物可用作制备杀虫剂的中间体
公开(公告)号：US4216162A
公开(公告)日：1980-08-05
申请号：US920031
申请日：1978-06-28
申请人： Dieter Arlt , Manfred Jautelat
发明人： Dieter Arlt , Manfred Jautelat
IPC分类号： C07D263/06 , B01J31/00 , C07C67/00 , C07C231/00 , C07C231/12 , C07C233/38 , C07C235/58 , C07C239/00 , C07C241/00 , C07C243/32 , C07C257/04 , C07C257/16 , C07C259/08 , C07C325/00 , C07C327/46 , C07C327/58 , C07D263/12 , C07D263/52 , C07D263/56 , C07C103/19 , C07C153/063
CPC分类号： C07D263/52 , C07D263/12 , C07D263/56
摘要： Novel 2-(2,2-dihalogenovinyl)-3,3-dimethylcyclopropanecarboxylic acid derivatives of the formula ##STR1## e.g. amides, thioamides, oxazolines, amidoximes and hydroxamic acids, are produced by reacting the new compounds ##STR2## with a base in the presence of a diluent. New compounds of the formula ##STR3## are produced by reacting ##STR4## with ##STR5##
摘要翻译：式（I）的新型2-（2,2-二卤代乙酰基）-3,3-二甲基环丙烷羧酸衍生物酰胺，硫代酰胺，恶唑啉，酰胺肟和异羟肟酸，通过在稀释剂存在下使新化合物＆lt; IMAGE＆gt;（II）与碱反应来制备。通过使（III）化合物与反应生成新化合物

29. 发明授权

US5428073A Antimicrobial agents which are substituted 2-cyclohexan-1-yl-amine compounds. 失效
标题翻译：作为取代的2-环己烷-1-基 - 胺化合物的抗微生物剂。
公开(公告)号：US5428073A
公开(公告)日：1995-06-27
申请号：US956535
申请日：1992-10-05
申请人： Franz Kunisch , Peter Babczinski , Dieter Arlt , Wilhelm Brandes , Heinz-Wilhelm Dehne , Stefan Dutzmann , Manfred Plempel
发明人： Franz Kunisch , Peter Babczinski , Dieter Arlt , Wilhelm Brandes , Heinz-Wilhelm Dehne , Stefan Dutzmann , Manfred Plempel
IPC分类号： C07D275/06 , A01N37/44 , A01N37/46 , A01N43/38 , A01N43/40 , A01N43/80 , B01J23/46 , C07B61/00 , C07C219/24 , C07C227/16 , C07C229/48 , C07C233/52 , C07C237/04 , C07C237/24 , C07C269/06 , C07C271/24 , C07C323/53 , C07C323/62 , C07C327/24 , C07C327/32 , C07D213/30 , C07F9/165 , C07F9/40 , A61K31/19
CPC分类号： C07D213/30 , A01N37/44 , A01N37/46 , A01N43/40 , C07C229/48 , C07C233/52 , C07C237/04 , C07C237/24 , C07C271/24 , C07C327/24 , C07C327/32 , C07F9/4021 , C07C2101/08 , Y02P20/55
摘要： There are described new 2-cyclohexan-1-yl-amine derivatives of formula (I) ##STR1## in which A, R.sup.1, R.sup.2, R.sup.3 and R.sup.4 have the meaning given in the description, and processes for their preparation.The compounds of the formula (I) are used as anti-microbial agents.
摘要翻译：描述了式（I）的新的2-环己烷-1-基 - 胺衍生物其中A，R1，R2，R3和R4具有说明书中给出的含义及其制备方法。式（I）的化合物用作抗微生物剂。

30. 发明授权

US5270340A Substituted 2-cyclohexen-1-yl-amine fungicidal and herbicidal agents 失效
标题翻译：取代的2-环己烯-1-基 - 胺杀真菌剂和除草剂
公开(公告)号：US5270340A
公开(公告)日：1993-12-14
申请号：US762807
申请日：1991-09-20
申请人： Franz Kunisch , Peter Babczinski , Dieter Arlt , Hans-Joachim Santel , Robert R. Schmidt , Wilhelm Brandes , Harry Strang
发明人： Franz Kunisch , Peter Babczinski , Dieter Arlt , Hans-Joachim Santel , Robert R. Schmidt , Wilhelm Brandes , Harry Strang
IPC分类号： A01N33/10 , A01N33/18 , A01N37/02 , A01N37/44 , A01N43/16 , A01N57/20 , C07C211/40 , C07C215/42 , C07C219/24 , C07C225/20 , C07C229/46 , C07C229/48 , C07C229/50 , C07C233/52 , C07C233/63 , C07C237/24 , C07C255/46 , C07C271/24 , C07D209/48 , C07D307/54 , C07D307/89 , C07D311/76 , C07F9/40 , C07C211/39 , A01N33/02
CPC分类号： C07D209/48 , A01N33/10 , A01N33/18 , A01N37/02 , A01N37/44 , A01N43/16 , A01N57/20 , C07C211/40 , C07C215/42 , C07C219/24 , C07C225/20 , C07C229/46 , C07C229/48 , C07C229/50 , C07C233/52 , C07C233/63 , C07C237/24 , C07C255/46 , C07C271/24 , C07D307/54 , C07D307/89 , C07D311/76 , C07F9/4018 , C07C2101/14 , C07C2101/16 , C07C2102/28
摘要： A method of combating pests which comprises applying to such pests or to a pest habitat a pesticidally effective amouht of a substituted 2-cyclohexen-1-yl-amine derivative of the formula ##STR1## and addition products thereof with acids and metal salts. Most of the compounds are new.
摘要翻译：一种防治害虫的方法，其包括将下式（I）的取代的2-环己烯-1-基 - 胺衍生物及其加成产物与酸和金属一起施用于害虫或害虫栖息地盐。大多数化合物是新的。

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