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21. 发明授权

US5482692A Selective catalytic reduction of nitrogen oxides using a ferrocene impregnated zeolite catalyst 失效
标题翻译：使用二茂铁浸渍的沸石催化剂选择性还原氮氧化物
公开(公告)号：US5482692A
公开(公告)日：1996-01-09
申请号：US271694
申请日：1994-07-07
申请人： Costandi A. Audeh , Sanjay B. Sharma , David S. Shihabi
发明人： Costandi A. Audeh , Sanjay B. Sharma , David S. Shihabi
IPC分类号： B01D53/86 , B01D53/94 , B01J29/072 , B01J29/46 , B01J37/02 , B01J37/08 , C01B21/04 , F01N3/20 , F02B1/04
CPC分类号： F01N3/2066 , B01D53/8621 , B01D53/8628 , B01D53/865 , B01D53/9418 , B01J29/072 , B01J29/46 , B01J37/0203 , B01J37/086 , B01D2251/2062 , B01D2255/20738 , B01D2255/50 , B01J2229/26 , B01J2229/42 , F01N2610/02 , F02B1/04 , Y02T10/24
摘要： An exhaust gas treatment process useful for the removal of nitrogen oxides using an iron impregnated zeolite as the catalyst and ammonia as a reducing agent. It is desired to extend the effective temperature range for the selective catalytic reduction (SCR) of nitrogen oxides below about 400.degree. C. This is accomplished in the instant invention through the use of an intermediate pore size zeolite, such as ZSM-5, based catalyst which has been ferrocene treated to substantially incorporate iron into its pores. The catalyst may also be hydrothermally treated at least once, if desired.
摘要翻译：使用铁浸渍沸石作为催化剂除去氮氧化物的废气处理方法，氨作为还原剂。期望将氮氧化物的选择性催化还原（SCR）的有效温度范围延伸到低于约400℃。这在本发明中通过使用中等孔径的沸石，例如ZSM-5，基于已经将二茂铁处理以将铁基本上并入其孔中的催化剂。如果需要，也可以将催化剂水热处理至少一次。

22. 发明授权

US5461180A Catalytic norbornylation of aromatics 失效
标题翻译：芳烃的催化降冰片基化
公开(公告)号：US5461180A
公开(公告)日：1995-10-24
申请号：US239189
申请日：1994-05-05
申请人： Costandi A. Audeh , James R. Boulton , Ross A. Kremer , Yusheng Xiong
发明人： Costandi A. Audeh , James R. Boulton , Ross A. Kremer , Yusheng Xiong
IPC分类号： C07C2/66
CPC分类号： C07C2/66 , C07C2102/42 , C07C2529/40 , C07C2529/65 , C07C2529/70
摘要： A process is disclosed for the catalytic norbornylation of aromatics comprising the steps of contacting norborene and an aromatic hydrocarbon with a solid catalyst comprising a porous crystalline material having a Constraint Index of from about 0.1 to about 12 under norbornylation conditions to evolve a product containing norbornylated aromatics.
摘要翻译：公开了用于芳族化合物催化降冰片基化的方法，该方法包括以下步骤：将降冰片烯和芳烃与固体催化剂接触，所述固体催化剂包含在降冰片烷化条件下具有约0.1至约12约束指数的多孔结晶材料，以放出含有降冰片基化芳族化合物的产物。

23. 发明授权

US5292493A Clean up of ethanolamine solution by treating with weak ion exchange resins 失效
标题翻译：用弱离子交换树脂处理清洗乙醇胺溶液
公开(公告)号：US5292493A
公开(公告)日：1994-03-08
申请号：US802586
申请日：1991-12-05
申请人： Costandi A. Audeh , Tsoung Y. Yan
发明人： Costandi A. Audeh , Tsoung Y. Yan
IPC分类号： B01D53/14 , B01J39/04 , B01J41/04 , B01J49/00 , C07C213/10 , C01B17/16 , C01B31/20 , C02F1/42
CPC分类号： B01D53/1456 , B01D53/1425 , B01J39/04 , B01J41/043 , B01J49/0017 , C07C213/10
摘要： The present invention provides a process for removing heat stable salts which accumulate in alkanolamine gas purification process units. Surprisingly, it has been found that weakly acidic cationic exchange resins are dramatically more effective for removing heat stable salts from alkanolamine solutions than strongly acidic cationic exchange resins.Specifically, it has been found in accordance with the invention that ion exchange resins are useful for purifying used aqueous alkanolamine solutions, in the following order of preference: Weak Acid IX>Weak Base IX>Strong Acid IX>Strong Base IX.
摘要翻译：本发明提供一种除去积聚在烷醇胺气体净化处理单元中的热稳定盐的方法。令人惊讶的是，已经发现，弱酸性阳离子交换树脂比强酸性阳离子交换树脂更有效地从烷醇胺溶液中除去热稳定的盐。具体地说，根据本发明已经发现离子交换树脂可用于按以下优先顺序纯化所用的链烷醇胺水溶液：弱酸IX>弱碱IX>强酸IX>强碱IX。

24. 发明授权

US5190908A Racked bed for removal of residual mercury from gaseous hydrocarbons 失效
标题翻译：用于从气态碳氢化合物中除去残留汞的反应床
公开(公告)号：US5190908A
公开(公告)日：1993-03-02
申请号：US719408
申请日：1991-06-24
申请人： Costandi A. Audeh , Barry E. Hoffman
发明人： Costandi A. Audeh , Barry E. Hoffman
IPC分类号： B01D53/02 , B01J20/02 , B01J20/08
CPC分类号： B01D53/02 , B01J20/02 , B01J20/0237 , B01J20/0285 , B01J20/06 , B01J20/08 , B01J20/18 , B01J20/3204 , B01J20/3236 , B01J20/3289
摘要： The present invention advantageously provides a desiccant bed with means for removing residual mercury from a gas, such as a natural gas stream. The desiccant bed includes a silver and/or gold-containing layer and a protective layer of pellets having an active compound comprising at least one of copper hydroxide, copper oxide and copper sulfide. The active compound provides the desiccant bed with the additional advantage of removing H.sub.2 S and CO.sub.2 as well as mercury from the gaseous stream. The desiccant bed removes the mercury, H.sub.2 S and CO.sub.2 without incurring the pressure loss inherent in utilizing a separate downstream adsorbent bed for removing Hg.
摘要翻译：本发明有利地提供了一种干燥剂床，其具有用于从诸如天然气流的气体中除去残留的汞的装置。干燥剂床包括银和/或含金层和具有包含至少一种氢氧化铜，氧化铜和硫化铜的活性化合物的颗粒保护层。活性化合物为干燥剂床提供了从气流中除去H 2 S和CO 2以及汞的额外优点。干燥剂床除去汞，H2S和CO2，而不会产生利用单独的下游吸附剂床去除Hg的固有压力损失。

25. 发明授权

US5173286A Fixation of elemental mercury present in spent molecular sieve desiccant for disposal 失效
标题翻译：固定在废分子筛干燥剂中用于处置的元素汞
公开(公告)号：US5173286A
公开(公告)日：1992-12-22
申请号：US732690
申请日：1991-07-19
申请人： Costandi A. Audeh
发明人： Costandi A. Audeh
IPC分类号： A62D3/00 , A62D3/30 , A62D3/33 , A62D3/36 , A62D3/38 , A62D101/24 , A62D101/43 , B01J20/18 , B09B3/00
CPC分类号： A62D3/38 , A62D3/33 , B01J20/186 , B09B3/00 , B09B3/0025 , A62D2101/43 , A62D2203/04
摘要： A process for fixing elemental mercury (Hg.degree.) in a spent molecular sieve desiccant is disclosed. The process includes isolating gspent molecular sieve desiccant containing elemental mercury, and contacting the spent desiccant in a dilute aqueous solution of an alkaline metal salt. The reaction traps the mercury within the spent desiccant as an insoluble heavy metal salt. The alkaline metal salt can include, for example, sodium thiosulfate (Na.sub.2 S.sub.2 O.sub.3), sodium polysulfide (Na.sub.2 S.sub.x), or potassium peroxomonosulfate (KHSO.sub.5). The reaction with any of these aqueous solutions acts to fix the elemental mercury (Hg.degree.) as a mercury compound within the solid desiccant. If sodium thiosulfate or sodium polysulfide is utilized, then the process also includes introducing hydrochloric acid (HCl) in a suitable quantity to liberate sufficient elemental sulfur to react with the elemental mercury (Hg.degree.) to form an HgS salt. The formation of HgS fixes the elemental mercury (Hg.degree.) in the form of a heavy metal salt in the solid desiccant. If, however, an aqueous potassium peroxomonosulfate (KHSO.sub.5) solution is utilized, then HCl is not needed. The aqueous potassium peroxomonosulfate solution is used in a suitable concentration to convert the elemental mercury (Hg.degree.) in the spent desiccant to HgO, so that the elemental mercury (Hg.degree.) is fixed as an insoluble heavy metal oxide in the solid desiccant.
摘要翻译：公开了一种在废分子筛干燥剂中固定元素汞（Hg DEG）的方法。该方法包括分离含有元素汞的分子筛干燥剂，并将废弃的干燥剂与碱性金属盐的稀水溶液接触。该反应将废水中的汞捕获为不溶性重金属盐。碱金属盐可以包括例如硫代硫酸钠（Na 2 S 2 O 3），多硫化钠（Na 2 S x）或过硫酸钾（KHSO 5）。与任何这些水溶液的反应用于将固体干燥剂中的汞化合物的元素汞（Hg DEG）固定。如果使用硫代硫酸钠或多硫化钠，则该方法还包括引入适量的盐酸（HCl）以释放足够的元素硫以与元素汞（HgO）反应形成HgS盐。 HgS的形成固定在固体干燥剂中的重金属盐形式的元素汞（Hg DEG）。然而，如果使用了含硫酸钾（KHSO 5）水溶液，则不需要HCl。以适当的浓度使用硫酸钾水溶液，将废干燥剂中的元素汞（Hg DEG）转化为HgO，使得元素汞（Hg DEG）在固体干燥剂中固定为不溶重金属氧化物。

26. 发明授权

US5130108A Process for the production of natural gas condensate having a reduced amount of mercury from a mercury-containing natural gas wellstream 失效
标题翻译：用于从含汞天然气井中生产具有减少的汞量的天然气冷凝物的方法
公开(公告)号：US5130108A
公开(公告)日：1992-07-14
申请号：US343705
申请日：1989-04-27
申请人： Costandi A. Audeh , Barry E. Hoffman
发明人： Costandi A. Audeh , Barry E. Hoffman
IPC分类号： B01D53/14 , C10L3/10
CPC分类号： C10L3/10 , B01D53/14 , Y02C10/06 , Y10S210/914
摘要： A process for producing a natural gas condensate having a reduced amount of mercury from a mercury-containing natural gas wellstream, wherein the wellstream is first separated into gaseous and liquid fractions. The treatment of the gaseous fraction includes treatment with a carbonate solution which, upon regeneration, yields an acid gas which is mixed with the liquid fraction. The mixture is then separated from gaseous components and filtered.
摘要翻译：一种生产天然气冷凝物的方法，所述天然气冷凝物具有来自含汞天然气井的汞的量减少，其中所述井流首先被分离为气态和液态馏分。气态馏分的处理包括用碳酸盐溶液进行处理，碳酸盐溶液在再生时产生与液体馏分混合的酸性气体。然后将混合物与气体组分分离并过滤。

27. 发明授权

US5062976A Process for preparing an extreme pressure lubricating oil additive 失效
标题翻译：制备极压润滑油添加剂的方法
公开(公告)号：US5062976A
公开(公告)日：1991-11-05
申请号：US545003
申请日：1990-06-28
申请人： Costandi A. Audeh
发明人： Costandi A. Audeh
IPC分类号： C10M135/04
CPC分类号： C10M135/04 , C10M2219/022
摘要： A process for preparing an oxidized sulfurized isobutylene product having utility as an EP additive. The process comprises the steps of: reacting sulfur monochloride with a stoichiometric excess of isobutylene; reacting the product so produced with an alkali metal monosulfide and free sulfur in an alcohol-water solvent; reacting the product so produced with an aqueous solution containing an alkali metal hydroxide; and reacting the liquid sulfurized isobutylene so produced with a mild oxidizing agent under conditions sufficient to effect the appearance of new infrared frequency bands at 1300 cm.sup.-1 and 1030 cm.sup.-1 indicative of the formation of sulfoxides and sulfones and recovering a liquid oxidized sulfurized isobutylene product which is soluble in a lubricating composition.
摘要翻译：一种用作EP添加剂的氧化硫化异丁烯产物的制备方法。该方法包括以下步骤：使一氯化硫与化学计量过量的异丁烯反应; 使如此生产的产物与醇 - 水溶剂中的碱金属一硫化物和游离硫反应; 使如此制备的产物与含有碱金属氢氧化物的水溶液反应; 并使所生产的液体硫化异丁烯与温和氧化剂在足以在1300cm -1和1030cm -1处出现新的红外频带的条件下反应，表明形成亚砜和砜并回收液体氧化的硫化异丁烯可溶于润滑组合物的产品。

28. 发明授权

US4880527A Process for removing residual mercury from liquid hydrocarbons with aqueous polysulfide solutions 失效
标题翻译：用多硫化物水溶液从液态烃中除去残留汞的方法
公开(公告)号：US4880527A
公开(公告)日：1989-11-14
申请号：US108598
申请日：1987-10-15
申请人： Costandi A. Audeh
发明人： Costandi A. Audeh
IPC分类号： C10G17/04 , C10G29/10
CPC分类号： C10G17/04 , C10G29/10
摘要： Liquid hydrocarbons (natural gas condensate) are depleted of contaminating mercury by contacting them with a solution of an alkali polysulfide.
摘要翻译：液态碳氢化合物（天然气冷凝物）通过与碱性多硫化物的溶液接触而消耗污染的汞。

29. 发明授权

US4786483A Process for removing hydrogen sulfide and mercury from gases 失效
标题翻译：从气体中除去硫化氢和汞的工艺
公开(公告)号：US4786483A
公开(公告)日：1988-11-22
申请号：US100869
申请日：1987-09-25
申请人： Costandi A. Audeh
发明人： Costandi A. Audeh
IPC分类号： B01D53/14 , B01D53/52 , B01D53/64 , B01D53/34
CPC分类号： B01D53/1493 , B01D53/52 , B01D53/64
摘要： Disclosed is a sorbent material for removing mercury and hydrogen sulfide from gases. The sorbent is a porous granular material which has been impregnated with a chemical compound capable of converting mercury to the oxide form and simultaneously hydrogen sulfide to elemental sulfur. Sorbent materials include silica, alumina, silica-alumina, molecular sieves, and mixtures of two or more of these. The reactive compound disclosed is an alkali metal peroxomonosulfate salt, for example, potassium peroxomonosulfate. In a variation the gas can be contacted directly with an aqueous solution of the chemical compound such as the alkali peroxomonsolufate salt.
摘要翻译：公开了一种用于从气体中去除汞和硫化氢的吸附剂材料。吸附剂是多孔颗粒材料，其已经浸渍有能够将汞转化为氧化物形式并且同时将硫化氢转化为元素硫的化合物。吸附剂材料包括二氧化硅，氧化铝，二氧化硅 - 氧化铝，分子筛，以及它们中的两种或更多种的混合物。所公开的反应性化合物是碱金属过硫酸一铵盐，例如硫酸钾。在一个变体中，气体可以直接与化学化合物的水溶液例如碱性过氧化脂肪酸盐接触。

30. 发明授权

US4771030A Process for preparing particulate aluminum metal for adsorbing mercury from natural gas 失效
标题翻译：制备用于从天然气中吸附汞的颗粒状金属铝的方法
公开(公告)号：US4771030A
公开(公告)日：1988-09-13
申请号：US118701
申请日：1987-11-09
申请人： Costandi A. Audeh
发明人： Costandi A. Audeh
IPC分类号： B01D53/64 , C07C7/148 , B01J20/30 , B01J21/02 , B01J27/125 , B01J27/25
CPC分类号： B01D53/64 , C07C7/14841
摘要： Hydrocarbon gases containing trace quantities of mercury are treated to remove the mercury by contacting the gases with a porous bed of aluminum which has been activated by contacting it with an aqueous solution of a soluble mercuric salt and subsequent drying of the activated bed in a non-oxidizing atmosphere.
摘要翻译：通过使气体与铝的多孔床接触来处理含有微量汞的烃气体，该多孔床已经通过使其与可溶性汞盐水溶液接触而被活化，随后在非水溶液中干燥活化床，氧化气氛。

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