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21. 发明申请

US20100105792A1 RADIATION-CURING BINDERS AND A PROCESS FOR THEIR PREPARATION 有权
标题翻译：辐射固化粘合剂及其制备方法
公开(公告)号：US20100105792A1
公开(公告)日：2010-04-29
申请号：US12651576
申请日：2010-01-04
申请人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitt , Holger Mundstock
发明人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitt , Holger Mundstock
IPC分类号： C08G59/68
CPC分类号： C08G18/8175 , B33Y70/00 , C09D175/14 , Y10T428/31551
摘要： The invention relates to a process for preparing binders which contain 1) allophanate groups, 2) groups that react with ethylenically unsaturated compounds with polymerization on exposure to actinic radiation (radiation-curing groups) and 3) optionally NCO-reactive groups, by reacting at temperatures ≦130° C. A) one or more NCO-functional compounds containing uretdione groups with B) one or more compounds that contain isocyanate-reactive groups and groups that react with ethylenically unsaturated compounds with polymerization on exposure to actinic radiation (radiation-curing groups), and then C) with one or more saturated, hydroxyl-containing compounds other than B), at least one of these compounds having an OH functionality of ≧2, in the presence of D) a catalyst containing one or more ammonium salts or phosphonium salts of aliphatic or cycloaliphatic carboxylic acids, the reaction with compounds C) taking place at least proportionally with the formation of allophanate groups. The present invention also relates to the binders obtained by the process of the invention.
摘要翻译：本发明涉及一种制备粘合剂的方法，其包含1）脲基甲酸酯基团，2）与烯键式不饱和化合物反应的基团与暴露于光化辐射（辐射固化基团）和3）任选的NCO-反应性基团反应的基团， A）一种或多种含有脲二酮基团的NCO-官能化合物，B）一种或多种含有异氰酸酯反应性基团的化合物和与烯键式不饱和化合物反应而与光化辐射（辐射 - 固化基团），然后C）与除了B）之外的一种或多种饱和的含羟基化合物，在D的存在下，在具有OH官能度≥2的这些化合物中的至少一种的化合物中含有一种或多种铵脂肪族或脂环族羧酸的盐或鏻盐，与化合物C）的反应至少与脲基甲酸酯基团的形成成比例地发生。本发明还涉及通过本发明的方法获得的粘合剂。

22. 发明授权

US07659425B2 Process for preparing hydroxyalkyl(meth) acrylates using Lewis acid catalysts 有权
标题翻译：使用路易斯酸催化剂制备（甲基）丙烯酸羟烷基酯的方法
公开(公告)号：US07659425B2
公开(公告)日：2010-02-09
申请号：US11356334
申请日：2006-02-16
申请人： Jan Weikard , Christoph Gürtler
发明人： Jan Weikard , Christoph Gürtler
IPC分类号： C07C67/26 , C07C69/52
CPC分类号： C07C67/26 , C07C69/54
摘要： The present invention relates to a process for preparing hydroxyalkyl (meth)acrylates by reacting at least one compound A which contains at least one epoxide group with at least one compound B which contains at least one carboxylic acid group, wherein A and/or B also contains at least one (meth)acrylate group, in the presence of Lewis acid catalysts, each of which contains at least one directly bonded di(cyclo)alkylamino group.
摘要翻译：本发明涉及通过使至少一种含有至少一个环氧基的化合物A与至少一种含有至少一个羧酸基团的化合物B反应来制备（甲基）丙烯酸羟烷基酯的方法，其中A和/或B也是在路易斯酸催化剂存在下含有至少一种（甲基）丙烯酸酯基团，其各自含有至少一个直接键合的二（环）烷基氨基。

23. 发明授权

US07553906B2 Dual cure systems 有权
标题翻译：双重治疗系统
公开(公告)号：US07553906B2
公开(公告)日：2009-06-30
申请号：US10738879
申请日：2003-12-17
申请人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Diethelm Rappen , Michael Schelhaas
发明人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Diethelm Rappen , Michael Schelhaas
IPC分类号： C08G18/80 , C08G18/81 , C08L75/14 , C07C233/57 , C07C263/00
CPC分类号： C08G18/672 , C08G18/8048 , C08G18/8093 , C08G18/8096 , C08G18/8175 , C08L75/16 , C09D175/16 , Y10T428/31551 , C08G18/62 , C08L2666/20
摘要： An organic polyisocyanate with at least one unsaturated functional group is capable of copolymerizing when exposed to actinic radiation. The polyisocyanate comprises structural units with the formula (1): wherein: X is an electron-attracting group; R1, and R2 are hydrogen atoms, a saturated or unsaturated aliphatic or cycloaliphatic radical, or an aromatic or araliphatic radical; and n is an integer from 0 to 5. A process for producing this polyisocyanate is also disclosed.
摘要翻译：具有至少一个不饱和官能团的有机多异氰酸酯在暴露于光化辐射时能够共聚。多异氰酸酯包括具有式（1）的结构单元：其中：X是吸电子基团; R1和R2是氢原子，饱和或不饱和的脂族或脂环族基团，或芳族或芳脂族基团; 并且n为0至5的整数。还公开了制备该多异氰酸酯的方法。

24. 发明授权

US06756500B1 &agr;,&ohgr;-Diene metathesis in the presence of ionic liquids 失效
公开(公告)号：US06756500B1
公开(公告)日：2004-06-29
申请号：US09514023
申请日：2000-02-25
申请人： Christoph Gürtler , Manfred Jautelat
发明人： Christoph Gürtler , Manfred Jautelat
IPC分类号： C07D20948
CPC分类号： C07F7/083 , C07B37/10 , C07C6/04 , C07C269/06 , C07C2531/24 , C07C2601/16 , C07D207/20 , C07D225/02 , C07D307/28 , C07C13/20 , C07C271/24 , C07C271/56
摘要： A process for preparing a cyclic compound comprising subjecting a starting material in the presence of a catalyst component to metathesis reaction in the presence of an ionic liquid, wherein the starting material is a &agr;,&ohgr;-diene bearing a &agr; substituent NRR1 in the &agr; position to a double bond, wherein R is hydrogen or an organic substituent, R1 is tert-butyl, P(R)2, P(R2)2, COR, SO2PhR, COOR or CONRR2, R2is alkyl or phenyl, or R and R1 together form and in which &agr;,&ohgr;-dienes optionally bear at least one further substituent R in any other position with the exception of the &agr; position, wherein R is selected from the group consisting of hydrogen, fused or unfused aryl, alkyl, CN, COOR2 or halogen, and wherein the starting material optionally contains a member selected from the group containing at least one further substituent that is inert in the metathesis reaction and a heteroatom selected from the group consisting of branched alkyl radicals, unbranched alkyl radicals, aromatic carbocyclic rings, non-aromatic carbocyclic rings, carboxylic acids, esters, ethers, epoxides, silyl ethers, thioethers, thioacetals, anhydrides, imines, silylenol ethers, ammonium salts, amides, nitriles, perfluoroalkyl groups, geminal dialkyl groups, alkynes, alkenes, halogens, alcohols, ketones, aldehydes, carbamates, carbonates, urethanes, sulfonates, sulfones, sulfonamides, nitro groups, organosilane units, metal centers and oxygen-containing heterocycles, nitrogen-containing heterocycles, sulfur-containing heterocycles and phosphorus-containing heterocycles, wherein the catalyst component includes homogeneous catalysts and heterogeneous catalysts selected from the group consisting of (i) transition metal carbenes, (ii) transition metal compounds that form transition metal carbenes under the reaction conditions, and (iii) transition metal salts in combination with an alkylating agent.

25. 发明授权

US09309356B2 Method for activating double metal cyanide catalysts for the production of polyether carbonate polyols 有权
标题翻译：用于生产聚碳酸酯多元醇的双金属氰化物催化剂的活化方法
公开(公告)号：US09309356B2
公开(公告)日：2016-04-12
申请号：US14232633
申请日：2012-07-16
申请人： Thomas Ernst Müller , Christoph Gürtler , Yvonne Dienes , Julien Barruet , Burkhard Köhler , Walter Leitner
发明人： Thomas Ernst Müller , Christoph Gürtler , Yvonne Dienes , Julien Barruet , Burkhard Köhler , Walter Leitner
IPC分类号： C08G64/32 , C08G64/34 , C08G65/26 , C08G64/00 , C08G64/04
CPC分类号： C08G64/323 , C08G64/34 , C08G65/2603 , C08G65/2663
摘要： The present invention relates to a process for the activation of double metal cyanide (DMC) catalysts with heterocumulenes for the preparation of polyether carbonate polyols by catalytic copolymerization of carbon dioxide (CO2) with alkylene oxides in the presence of one or more H-functional starter substances, and to a process for the preparation of polyether carbonate polyols from one or more H-functional starter substances, one or more alkylene oxides and carbon dioxide in the presence of a double metal cyanide catalyst, characterized in that (α) under an inert gas atmosphere, under an atmosphere of an inert gas/carbon dioxide mixture or under a pure carbon dioxide atmosphere, at temperatures of from 90 to 150° C., the DMC catalyst is mixed with a heterocumulene and H-functional starter substance, (β) alkylene oxide is added at temperatures of from 100 to 150° C. to the mixture from step (α) under an inert gas atmosphere, under an atmosphere of an inert gas/carbon dioxide mixture or under a pure carbon dioxide atmosphere, and (γ) one or more alkylene oxides and carbon dioxide are metered continuously into the mixture resulting from step (β).
摘要翻译：本发明涉及一种用于通过在一种或多种H功能性起始剂存在下通过二氧化碳（CO 2）与氧化烯的催化共聚来制备聚醚碳酸酯多元醇的异氰脲酸双金属氰化物（DMC）催化剂的活化方法以及在双金属氰化物催化剂存在下从一种或多种H官能起始物质，一种或多种环氧烷和二氧化碳制备聚醚碳酸酯多元醇的方法，其特征在于（α）在惰性气体气氛中，在惰性气体/二氧化碳混合气氛下或在纯二氧化碳气氛下，在90〜150℃的温度下，将DMC催化剂与杂多烯和H官能起始物质（＆bgr ;）在惰性气体气氛下，在惰性气体/二氧化碳气氛下，将氧化烯在100至150℃的温度下加入步骤（α）的混合物中或者在纯二氧化碳气氛下，将（γ）一种或多种烯化氧和二氧化碳连续计量到由步骤（bgr）得到的混合物中。

26. 发明授权

US09260562B2 Method for producing polycarbonate polyols by the immortal polymerization of cyclic carbonates 有权
标题翻译：通过环状碳酸酯的永生聚合生产聚碳酸酯多元醇的方法
公开(公告)号：US09260562B2
公开(公告)日：2016-02-16
申请号：US13880288
申请日：2011-11-03
申请人： Thomas Ernst Müller , Christoph Gürtler , Anthony Kermagoret , Yvonne Dienes , Igor Busygin , Burkhard Köhler , Walter Leitner , Ganna Lyashenko
发明人： Thomas Ernst Müller , Christoph Gürtler , Anthony Kermagoret , Yvonne Dienes , Igor Busygin , Burkhard Köhler , Walter Leitner
IPC分类号： C08G64/00 , C08G64/30 , C08G64/02 , C08G64/18 , C08G64/38 , C08G75/00
CPC分类号： C08G64/305 , C08G64/0208 , C08G64/183 , C08G64/38
摘要： The invention relates to a process for the preparation of polycarbonate polyols, characterized in that cyclic carbonates are polymerized in the presence of DMC catalysts and chain-transfer agents consisting of polyether carbonate polyols.
摘要翻译：本发明涉及一种制备聚碳酸酯多元醇的方法，其特征在于环状碳酸酯在DMC催化剂和由聚醚碳酸酯多元醇组成的链转移剂存在下聚合。

27. 发明授权

US09200113B2 Multi-amine functional oligomers and method for producing the same by the reduction of corresponding oximes 有权
标题翻译：多胺官能低聚物及其制备方法，通过减少相应的肟
公开(公告)号：US09200113B2
公开(公告)日：2015-12-01
申请号：US13634148
申请日：2011-03-08
申请人： Christoph Gürtler , Thomas Ernst Müller , Ewa Gebauer , Henning Vogt , Yevgen Berezhanskyy , Burkhard Köhler , Walter Leitner
发明人： Christoph Gürtler , Thomas Ernst Müller , Ewa Gebauer , Henning Vogt , Yevgen Berezhanskyy , Burkhard Köhler , Walter Leitner
IPC分类号： C08G61/04 , C08G67/02 , C08G64/36 , C08G64/42 , C08G59/50 , C08L63/00 , C08L73/00
CPC分类号： C08G67/02 , C08G59/5006 , C08G61/04 , C08G64/36 , C08G64/42 , C08L63/00 , C08L73/00 , C08L2666/22
摘要： The invention relates to multi-amine functional oligomers and multi-oxime functional oligomers in addition to a method for producing the same by means of the co-polymerization of carbonyl carriers such as olefins or dienes, reaction with hydroxylamine and a subsequent selective catalytic hydrogenation.
摘要翻译：本发明除了通过羰基载体如烯烃或二烯的共聚合，与羟胺的反应和随后的选择性催化氢化之外，还涉及多胺官能低聚物和多肟官能低聚物的制备方法。

28. 发明授权

US09120894B2 Method for producing polyether polyols 有权
标题翻译：聚醚多元醇的制备方法
公开(公告)号：US09120894B2
公开(公告)日：2015-09-01
申请号：US14131977
申请日：2012-07-17
申请人： Thomas Ernst Müller , Christoph Gürtler , Matthias Wohak , Jörg Hofmann , Muhammad Afzal Subhani , Maurice Cosemans , Walter Leitner
发明人： Thomas Ernst Müller , Christoph Gürtler , Matthias Wohak , Jörg Hofmann , Muhammad Afzal Subhani , Maurice Cosemans , Walter Leitner
IPC分类号： C08G85/00 , C08G65/00 , C08G65/26 , C08G64/34
CPC分类号： C08G65/2663 , C08G64/34 , C08G65/2603
摘要： The present invention relates to a process for the preparation of polyether carbonate polyols from one or more H-functional starter compounds, one or more alkylene oxides and carbon dioxide in the presence of a double metal cyanide catalyst, wherein (α) the H-functional starter substance or a mixture of at least two H-functional starter substances is initially introduced into the reaction vessel, (β) for the activation, a part amount (based on the total amount of the amount of alkylene oxides employed in steps (β) and (γ)) of one or more alkylene oxides is added to the mixture resulting from step (α), it also being possible for step (β) to be carried out several times for the activation, (γ) one or more alkylene oxides and carbon dioxide are metered continuously into the mixture resulting from step (β) (“copolymerization”), the alkylene oxides employed for the copolymerization being identical to or different from the alkylene oxides employed in step (β), characterized in that in step (γ) the carbon dioxide is passed into the mixture by (i) gassing the reaction mixture in the reactor from the bottom, (ii) using a hollow shaft stirrer, (iii) a combination of the metering operations according to (i) and (ii), and/or (iv) gassing over the surface of the liquid by using stirrer units configured in several stages.
摘要翻译：本发明涉及在双金属氰化物催化剂存在下由一种或多种H官能起始化合物，一种或多种环氧烷和二氧化碳制备聚醚碳酸酯多元醇的方法，其中（α）H官能团起始物质或至少两种H功能性起始物质的混合物最初被引入反应容器（（bgr））中用于活化，部分量（基于步骤（bgr）中使用的环氧烷烃的总量（γ））和（γ））加入到由步骤（α）得到的混合物中，对于活化，（γ）一个或多个步骤（＆bgr）可以进行几次，更多的环氧烷和二氧化碳被连续地计量到由步骤（（bgr））（“共聚”）得到的混合物中，用于共聚的烯化氧与步骤（bgr）中使用的环氧烷烃相同或不同，其特征在于在步骤（γ）中，二氧化碳通过以下步骤进入混合物：（i）从底部将反应混合物放入反应器中，（ii）使用中空轴搅拌器，（iii）根据至（i）和（ii），和/或（iv）通过使用在几个阶段中配置的搅拌器单元在液体的表面上放气。

29. 发明申请

US20140228537A1 METHOD FOR ACTIVATING DOUBLE METAL CYANIDE CATALYSTS FOR PRODUCING POLYETHER POLYOLS 有权
标题翻译：用于生产聚醚多元醇的双金属氰化物催化剂的活化方法
公开(公告)号：US20140228537A1
公开(公告)日：2014-08-14
申请号：US14232015
申请日：2012-07-17
申请人： Thomas Ernst Müller , Christoph Gürtler , Matthias Wohak , Jörg Hofmann , Muhammad Afzal Subhani , Maurice Cosemans , Walter Leitner
发明人： Thomas Ernst Müller , Christoph Gürtler , Matthias Wohak , Jörg Hofmann , Muhammad Afzal Subhani , Maurice Cosemans , Walter Leitner
IPC分类号： C08G64/32
CPC分类号： C08G64/323 , C08G64/34 , C08G65/2603 , C08G65/2663
摘要： The present invention relates to a process for the activation of double metal cyanide (DMC) catalysts and to a process for the preparation of polyethercarbonate polyols from one or more H-functional starter compounds, one or more alkylene oxides and carbon dioxide in the presence of a double metal cyanide catalyst, characterized in that (α) (α1) the DMC catalyst and one or more H-functional starter compounds are placed in a reactor, (α2) an inert gas, an inert gas/carbon dioxide mixture or carbon dioxide is passed through the reactor at a temperature of 50 to 200° C. and at the same time a reduced pressure (absolute) of 10 mbar to 800 mbar is established in the reactor by removal of the inert gas or carbon dioxide, (β) under an atmosphere of inert gas/carbon dioxide mixture or under a pure carbon dioxide atmosphere, alkylene oxide is added to the mixture from step (α) at temperatures of 50 to 200° C., and (γ) one or more alkylene oxides and carbon dioxide are metered into the mixture resulting from step (β).
摘要翻译：本发明涉及一种活化双金属氰化物（DMC）催化剂的方法，以及一种由一种或多种H官能起始化合物，一种或多种环氧烷和二氧化碳在存在下制备聚醚碳酸酯多元醇的方法一种双金属氰化物催化剂，其特征在于将（α）（α1）DMC催化剂和一种或多种H官能起始化合物置于反应器中，（α2）惰性气体，惰性气体/二氧化碳混合物或二氧化碳在50至200℃的温度下通过反应器，同时通过除去惰性气体或二氧化碳，在反应器中建立10毫巴至800毫巴的减压（绝对）（绝对）。）在惰性气体/二氧化碳混合物的气氛下或在纯二氧化碳气氛下，在步骤（α）的混合物中，在50〜200℃的温度下加入环氧烷，（γ）一种或多种环氧烷烃并将二氧化碳计量加入由（步骤（bgr））产生的混合物。

30. 发明申请

US20140018517A1 METHOD FOR PRODUCING POLYCARBONATE POLYOLS BY THE IMMORTAL POLYMERIZATION OF CYCLIC CARBONATES 有权
标题翻译：通过循环碳酸酯的固体聚合制备聚碳酸酯多元醇的方法
公开(公告)号：US20140018517A1
公开(公告)日：2014-01-16
申请号：US13880288
申请日：2011-11-03
申请人： Igor Busygin , Thomas Ernst Müller , Christoph Gürtler , Anthony Kermagoret , Yvonne Dienes , Igor Busygin , Burkhard Köhler , Walter Leitner
发明人： Igor Busygin , Thomas Ernst Müller , Christoph Gürtler , Anthony Kermagoret , Yvonne Dienes , Igor Busygin , Burkhard Köhler , Walter Leitner
IPC分类号： C08G64/30
CPC分类号： C08G64/305 , C08G64/0208 , C08G64/183 , C08G64/38
摘要： The invention relates to a process for the preparation of polycarbonate polyols, characterised in that cyclic carbonates are polymerised in the presence of DMC catalysts and chain-transfer agents consisting of polyether carbonate polyols.
摘要翻译：本发明涉及一种制备聚碳酸酯多元醇的方法，其特征在于环状碳酸酯在DMC催化剂和由聚醚碳酸酯多元醇组成的链转移剂的存在下聚合。

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