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    • 22. 发明授权
    • Method for preparation of an anthraquinone colorant composition
    • 蒽醌着色剂组合物的制备方法
    • US06861541B2
    • 2005-03-01
    • US10758347
    • 2004-01-15
    • Arun Nandkishor DixitAdil Minoo Dhalla
    • Arun Nandkishor DixitAdil Minoo Dhalla
    • C09B1/32C07C231/02
    • C09B1/325
    • Disclosed herein is a method for producing a 1-[4-(biphenyl-4-carbonyl)]phenylaminonthraquinone colorant composition where the method comprises: reacting 4-halobenzoic acid with about 1 mole to about 4 moles of a halogenating agent per mole of said 4-halobenzoic acid to form a 4-halobenzoyl halide composition; reacting in the presence of a first catalyst composition, said 4-halobenzoyl halide composition with biphenyl, in a solvent, to form a 1-[4-(biphenyl-4-carbonyl)]halobenzene composition, and reacting in the presence of a second catalyst composition and an acid scavenger, said 1-[4-(biphenyl-4-carbonyl)]phenylaminonthraquinone with a 1-aminoanthraquinone, in a reaction medium comprising a dipolar aprotic solvent, to form said 1-[4-(biphenyl-4-carbonyl)]phenylaminoanthraquinone colorant composition.
    • 本文公开了1- [4-(联苯-4-羰基)]苯基氨基醌醌着色剂组合物的制备方法,其中所述方法包括:使4-卤代苯甲酸与约1摩尔至约4摩尔卤化剂/摩尔所述 形成4-卤代苯甲酰卤化合物; 在第一催化剂组合物存在下,使所述4-卤代苯甲酰卤化合物与联苯在溶剂中反应形成1- [4-(联苯-4-羰基)]卤代苯组合物,并在第二催化剂组合物 催化剂组合物和酸清除剂,在包含偶极非质子溶剂的反应介质中,所述1- [4-(联苯-4-羰基)]苯基氨基醌与1-氨基蒽醌反应,形成所述1- [4-(联苯-4-基) - 羰基)]苯基氨基蒽醌着色剂组合物。