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21. 发明授权

US5607723A Method for making continuous thin diamond film 失效
标题翻译：制造连续薄金刚石薄膜的方法
公开(公告)号：US5607723A
公开(公告)日：1997-03-04
申请号：US238989
申请日：1994-05-05
申请人： Linda S. Plano , Michael G. Peters , Kramadhati V. Ravi , John M. Pinneo
发明人： Linda S. Plano , Michael G. Peters , Kramadhati V. Ravi , John M. Pinneo
IPC分类号： C30B29/04 , C23C16/27 , C30B25/02 , G03F1/22 , C23C16/26 , H05H1/24
CPC分类号： C23C16/272 , C30B25/02 , C30B29/04 , G03F1/22
摘要： A continuous thin diamond film having a thickness of less than about 2 microns has a low leakage. The thin diamond film may be supported on a supporting grid and may be incorporated into an X-ray window. The film may be formed in a DC assisted CVD process where in a first phase a relatively high concentration of a carbonaceous gas is introduced into the reactor and in a second phase the concentration of the carbonaceous gas is reduced to a lower value.
摘要翻译：具有小于约2微米厚度的连续薄金刚石膜具有低泄漏。薄金刚石膜可以被支撑在支撑网格上并且可以被结合到X射线窗口中。该膜可以以直流辅助CVD方法形成，其中在第一阶段将相对高浓度的碳质气体引入反应器中，而在第二阶段，碳质气体的浓度降低到较低的值。

22. 发明授权

US5571616A Ultrasmooth adherent diamond film coated article and method for making same 失效
标题翻译：超平滑贴面金刚石薄膜涂层制品及其制作方法
公开(公告)号：US5571616A
公开(公告)日：1996-11-05
申请号：US442259
申请日：1995-05-16
申请人： William Phillips , John M. Pinneo
发明人： William Phillips , John M. Pinneo
IPC分类号： C23C16/02 , C23C16/27 , C23C16/56 , C01B31/06
CPC分类号： C23C16/279 , C23C16/0227 , C23C16/274 , C23C16/277 , C23C16/56 , Y10T428/265 , Y10T428/30
摘要： An ultrasmooth diamond film has a thickness greater than about ten microns and an average grain size less than about 0.5 micron. The ultrasmooth diamond film of the present invention is grown using ordinary microwave plasma CVD methods, with a metal vapor source included in the reactor to produce vapor during the growth of the film. The metal vapor source may be chosen from the first row transition elements, chromium, iron, cobalt, and nickel, or from the lanthanides praseodymium, europeum, or erbium. Any metal capable of existing in the vapor phase in the presence of the hydrogen plasma, will cause formation of the ultrasmooth film of the present invention.
摘要翻译：超平滑金刚石膜的厚度大于约10微米，平均粒度小于约0.5微米。使用普通微波等离子体CVD方法生长本发明的超平滑金刚石膜，其中包含在反应器中的金属蒸汽源在膜生长期间产生蒸气。金属蒸汽源可以选自第一排过渡元素，铬，铁，钴和镍，或来自镧系元素镨，欧洲或铒。在氢等离子体存在下，能够存在于气相中的任何金属都将导致本发明的超静电膜的形成。

23. 发明授权

US5432003A Continuous thin diamond film and method for making same 失效
标题翻译：连续薄金刚石薄膜及其制造方法
公开(公告)号：US5432003A
公开(公告)日：1995-07-11
申请号：US747948
申请日：1991-08-21
申请人： Linda S. Plano , Michael G. Peters , Kramadhati V. Ravi , John M. Pinneo
发明人： Linda S. Plano , Michael G. Peters , Kramadhati V. Ravi , John M. Pinneo
IPC分类号： C23C16/27 , C30B25/02 , G03F1/22 , G21K1/00 , B32B9/00
CPC分类号： C23C16/272 , C30B25/02 , C30B29/04 , G03F1/22 , G21K1/00 , Y10T428/24942 , Y10T428/265 , Y10T428/30
摘要： A continuous thin diamond film having a thickness of less than about 2 microns has a permeability to helium lower than about 1.times.10.sup.-6 standard cubic centimeters of helium per second per square millimeter of surface area. The thin diamond film may be supported on a supporting grid and may be incorporated into an x-ray window. The thin diamond film of the present invention may be formed in a two-stage growth process wherein a first stage a carbonaceous gas at a first concentration is introduced in to the reactor and in a second stage the concentration of the carbonaceous gas is reduced to a second lower concentration.
摘要翻译：具有小于约2微米厚度的连续薄金刚石薄膜具有低于每平方毫米表面积每秒大约1×10-6标准立方厘米氦气氦的渗透性。薄金刚石膜可以被支撑在支撑网格上并且可以被结合到x射线窗口中。本发明的金刚石薄膜可以以两阶段生长方法形成，其中第一阶段将第一浓度的碳质气体引入反应器，而在第二阶段，碳质气体的浓度降低到第二低浓度。

24. 发明授权

US5413772A Diamond film and solid particle composite structure and methods for fabricating same 失效
标题翻译：金刚石薄膜和固体颗粒复合结构及其制造方法
公开(公告)号：US5413772A
公开(公告)日：1995-05-09
申请号：US889120
申请日：1992-07-06
申请人： John M. Pinneo
发明人： John M. Pinneo
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B01J3/06
CPC分类号： C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C23C16/274 , C04B2235/427 , C04B2235/667 , Y10T428/249953 , Y10T428/249967 , Y10T428/249986 , Y10T428/249987 , Y10T428/24999 , Y10T428/25 , Y10T428/2933 , Y10T428/2938 , Y10T428/298 , Y10T428/30 , Y10T428/31938
摘要： Porous and non-porous compositions include diamond particles, non-diamond particles, or mixtures of particles consolidated with polycrystalline diamond. The composite compositions of the present invention may be formed by a process which includes the steps of preforming the particles into a preform having a desired shape, and consolidating the preform with polycrystalline diamond. The polycrystalline diamond is preferably formed using CVD techniques including application of sufficient microwave energy to maintain the preform at a temperature of between about 670.degree. and 850.degree. C. The preform may be rotated during a portion of the deposition process.
摘要翻译：多孔和无孔组合物包括金刚石颗粒，非金刚石颗粒或与多晶金刚石固结的颗粒的混合物。本发明的复合组合物可以通过一种方法形成，该方法包括以下步骤：将颗粒预成型为具有所需形状的预成型体，并将预型体与多晶金刚石固结。多晶金刚石优选使用CVD技术形成，包括施加足够的微波能量以将预制件保持在约670℃至850℃之间的温度。预成型件可以在沉积过程的一部分期间旋转。

25. 发明授权

US5015528A Fluidized bed diamond particle growth 失效
标题翻译：流化床金刚石颗粒生长
公开(公告)号：US5015528A
公开(公告)日：1991-05-14
申请号：US171720
申请日：1988-03-22
申请人： John M. Pinneo
发明人： John M. Pinneo
IPC分类号： C01B31/06 , B01J8/44 , C30B25/02 , C30B25/18 , C30B29/04
CPC分类号： C30B25/18 , B01J8/44 , C30B25/02 , C30B29/04 , Y10T428/2991 , Y10T428/30
摘要： A process is provided for forming synthetic diamond by vapor deposition of a carbon gas source in the presence of atomic hydrogen on a substrate contained in a fluidized bed. The diamond may be overcoated by vapor deposition of a non-diamond material.

26. 发明授权

US1832218A Process for the production of acid and lime resisting derivatives of unsaturated fatty acids 失效
公开(公告)号：US1832218A
公开(公告)日：1931-11-17
申请号：US23898927
申请日：1927-12-09
申请人： GEN ANILINE WORKS INC
发明人： GEORG KALISCHER , FERDINAND BIEHLER
IPC分类号： C11C3/00
CPC分类号： C11C3/00

27. 发明授权

US07939367B1 Method for growing an adherent diamond layer atop an interlayer bonded to a compound semiconductor substrate 有权
标题翻译：在粘合到化合物半导体衬底上的层间生长粘附金刚石层的方法
公开(公告)号：US07939367B1
公开(公告)日：2011-05-10
申请号：US12338783
申请日：2008-12-18
申请人： Firooz Nasser-Faili , Niels Christopher Engdahl
发明人： Firooz Nasser-Faili , Niels Christopher Engdahl
IPC分类号： H01L21/00
CPC分类号： H01L21/3146 , H01L21/02115 , H01L21/02274 , H01L21/02304
摘要： The invention is a method for growing a critical adherent diamond layer on a substrate by Chemical Vapor Deposition (CVD) and the article produced by the method. The substrate can be a compound semiconductor coated with an adhesion layer. The adhesion layer is preferably a dielectric, such as silicon nitride, silicon carbide, aluminum nitride or amorphous silicon, to name some primary examples. The typical thickness of the adhesion layer is one micrometer or less. The resulting stack of layers, (e.g. substrate layer, adhesion layer and diamond layer) is structurally free of plastic deformation and the diamond layer is well adherent to the dielectric adhesion layer such that it can be processed further, such as by increasing the thickness of the diamond layer to a desired level, or by subjecting it to additional thin film fabrication process steps. In addition to preventing plastic deformation of the layer stack, the process also reduces the formation of soot during the CVD process. The reduction of soot allows for better adhesion between the adhesion layer and diamond layer of the layer stack.
摘要翻译：本发明是通过化学气相沉积（CVD）和通过该方法制备的制品在衬底上生长关键粘附金刚石层的方法。衬底可以是涂覆有粘合层的化合物半导体。粘附层优选为诸如氮化硅，碳化硅，氮化铝或非晶硅的电介质，以列举一些主要实例。粘合层的典型厚度为1微米或更小。所得到的层叠层（例如，基底层，粘合层和金刚石层）在结构上没有塑性变形，并且金刚石层与电介质粘合层良好粘附，使得其可进一步加工，例如通过增加厚度金刚石层到所需的水平，或者通过使其进一步的薄膜制造工艺步骤。除了防止层叠体的塑性变形之外，该过程还减少了CVD工艺期间烟灰的形成。烟灰的减少允许粘附层和层叠层的金刚石层之间的更好的粘附。

28. 发明授权

US5902675A Diamond film and solid diamond particle composite compositions 失效
标题翻译：金刚石薄膜和固体金刚石颗粒复合组合物
公开(公告)号：US5902675A
公开(公告)日：1999-05-11
申请号：US327355
申请日：1994-10-20
申请人： John M. Pinneo
发明人： John M. Pinneo
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B32B9/00
CPC分类号： C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C23C16/274 , C04B2235/427 , C04B2235/667 , Y10T428/249953 , Y10T428/249967 , Y10T428/249986 , Y10T428/249987 , Y10T428/24999 , Y10T428/25 , Y10T428/2933 , Y10T428/2938 , Y10T428/298 , Y10T428/30 , Y10T428/31938
摘要： Porous and non-porous compositions include diamond particles, non-diamond particles, or mixtures of particles consolidated with polycrystalline diamond. The composite compositions of the present invention may be formed by a process which includes the steps of preforming the particles into a preform having a desired shape, and consolidating the preform with polycrystalline diamond. The polycrystalline diamond is preferably formed using CVD techniques including application of sufficient microwave energy to maintain the preform at a temperature of between about 670.degree. and 850.degree. C. The preform may be rotated during a portion of the deposition process.
摘要翻译：多孔和无孔组合物包括金刚石颗粒，非金刚石颗粒或与多晶金刚石固结的颗粒的混合物。本发明的复合组合物可以通过一种方法形成，该方法包括以下步骤：将颗粒预成型为具有所需形状的预成型体，并将预型体与多晶金刚石固结。多晶金刚石优选使用CVD技术形成，包括施加足够的微波能量以将预制件保持在约670℃至850℃之间的温度。预成型件可以在沉积过程的一部分期间旋转。

29. 发明授权

US5609955A Diamond film and mixed diamond and non-diamond particle composite compositions 失效
标题翻译：金刚石薄膜和混合金刚石和非金刚石颗粒复合材料组合物
公开(公告)号：US5609955A
公开(公告)日：1997-03-11
申请号：US327354
申请日：1994-10-20
申请人： John M. Pinneo
发明人： John M. Pinneo
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B32B9/00
CPC分类号： C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C23C16/274 , C04B2235/427 , C04B2235/667 , Y10T428/249953 , Y10T428/249967 , Y10T428/249986 , Y10T428/249987 , Y10T428/24999 , Y10T428/25 , Y10T428/2933 , Y10T428/2938 , Y10T428/298 , Y10T428/30 , Y10T428/31938
摘要： Porous and non-porous compositions include diamond particles, non-diamond particles, or mixtures of particles consolidated with polycrystalline diamond. The composite compositions of the present invention may be formed by a process which includes the steps of preforming the particles into a preform having a desired shape, and consolidating the preform with polycrystalline diamond. The polycrystalline diamond is preferably formed using CVD techniques including application of sufficient microwave energy to maintain the preform at a temperature of between about 670.degree. and 850.degree. C. The preform may be rotated during a portion of the deposition process.
摘要翻译：多孔和无孔组合物包括金刚石颗粒，非金刚石颗粒或与多晶金刚石固结的颗粒的混合物。本发明的复合组合物可以通过一种方法形成，该方法包括以下步骤：将颗粒预成型为具有所需形状的预成型体，并将预型体与多晶金刚石固结。多晶金刚石优选使用CVD技术形成，包括施加足够的微波能量以将预制件保持在约670℃至850℃之间的温度。预成型件可以在沉积过程的一部分期间旋转。

30. 发明授权

US5277975A High thermal-conductivity diamond-coated fiber articles 失效
标题翻译：高导热性金刚石涂层纤维制品
公开(公告)号：US5277975A
公开(公告)日：1994-01-11
申请号：US954358
申请日：1992-09-30
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B32B9/00
CPC分类号： C23C16/274 , C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C04B2235/427 , C04B2235/667 , Y10T428/249955 , Y10T428/249956 , Y10T428/249957 , Y10T428/249967 , Y10T428/24997 , Y10T428/24999 , Y10T428/2938 , Y10T428/2991 , Y10T428/30
摘要： The present invention comprises an article formed for a plurality of diamond-coated fibers preformed into a desired shape. Each of the fibers has first surface regions in contact with immediately adjacent other ones of the fibers, and second surface regions spaced apart from the immediately adjacent other ones of said fibers to define boundaries of inter-fiber voids between the immediately adjacent ones of the fibers. The voids are infiltrated with high thermal conductivity CVD diamond material continuously coating the second surface regions of the fibers and comprising merged growth fronts from the second surface regions of individual immediately adjacent ones of the fibers into the inter-particle voids. The high thermal conductivity CVD diamond material has an average crystallite size greater than about 15 microns, an intensity ratio of diamond-Raman-peak-to-photoluminescence background intensity greater than about 20, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1 and a diamond-to-graphite Raman ratio greater than about 25. The thermal conductivity of the CVD diamond material is in excess of 17 Wcm.sup.-1 K.sup.-1.
摘要翻译：本发明包括形成用于预成形为所需形状的多个金刚石涂层纤维的制品。每个纤维具有与直接相邻的另一个纤维接触的第一表面区域和与紧邻的另一个纤维间隔开的第二表面区域，以限定紧邻的纤维之间的纤维间空隙的边界。空隙通过高导热性CVD金刚石材料渗透，连续地涂覆纤维的第二表面区域，并且包括从单独紧邻的纤维的第二表面区域到颗粒间空隙的合并生长前沿。高导热性CVD金刚石材料具有大于约15微米的平均微晶尺寸，金刚石 - 拉曼峰 - 光致发光背景强度的强度比大于约20，金刚石拉曼峰的最大强度（以计数/秒计）除了大于约3的1270cm-1处的光致发光强度，小于约6cm -1的拉曼sp3全宽半最大值和大于约25的金刚石 - 石墨拉曼比。CVD的热导率金刚石材料超过17 Wcm-1K-1。

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