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11. 发明授权

US09120293B2 Preliminary-cured material, roughened preliminary-cured material, and laminated body 有权
标题翻译：预固化材料，粗化预固化材料和层压体
公开(公告)号：US09120293B2
公开(公告)日：2015-09-01
申请号：US13582214
申请日：2011-03-31
申请人： Reona Yokota , Koichi Shibayama , Akihiro Uenishi , Hidenobu Deguchi , Tomoki Kunikawa , Tatsushi Hayashi
发明人： Reona Yokota , Koichi Shibayama , Akihiro Uenishi , Hidenobu Deguchi , Tomoki Kunikawa , Tatsushi Hayashi
IPC分类号： B32B5/16 , B32B27/20 , B32B27/38 , C08J7/00 , G11B5/64 , B32B15/092 , C08G59/40 , C08G59/42 , C08G59/62 , C08G59/68 , C08L63/00 , C08K3/36
CPC分类号： B32B15/092 , B32B15/08 , B32B15/20 , B32B27/20 , B32B27/38 , B32B2264/102 , B32B2307/538 , C08G59/4014 , C08G59/42 , C08G59/621 , C08G59/686 , C08J7/00 , C08K3/36 , C08L63/00 , Y10T428/259 , Y10T428/268 , C08L71/12
摘要： A preliminary-cured material permits reduced surface roughness of a roughening-treated surface, and increase of an adhesive strength between a cured object and a metal layer. The preliminary-cured material is obtained by advancing curing of an epoxy resin material that contains an epoxy resin, a curing agent, and a silica. The preliminary-cured material includes a first principal surface to be roughening-treated, and a second principal surface. The silica includes a first small particle-diameter silica whose particle diameter is not smaller than 0.01 μm but smaller than 0.5 μm, and a second large particle-diameter silica whose particle diameter is not smaller than 0.5 μm but not larger than 20 μm. The first small particle-diameter silica is localized to exist in large quantity on a side of the first principal surface, and the second large particle-diameter silica is localized to exist in large quantity on a side of the second principal surface.
摘要翻译：预固化材料允许粗糙化处理的表面的表面粗糙度降低，并且增加固化物体和金属层之间的粘合强度。预固化材料是通过使包含环氧树脂，固化剂和二氧化硅的环氧树脂材料进行固化而得到的。预固化材料包括待粗化处理的第一主表面和第二主表面。二氧化硅包括粒径不小于0.01μm但小于0.5μm的第一小粒径二氧化硅和粒径不小于0.5μm但不大于20μm的第二大粒径二氧化硅。第一小粒径二氧化硅被定位成大量存在于第一主表面的一侧，第二大颗粒直径二氧化硅在第二主表面的一侧大量存在。

12. 发明授权

US08765862B2 Metal nanoparticle composite and production method thereof 有权
标题翻译：金属纳米复合材料及其制备方法
公开(公告)号：US08765862B2
公开(公告)日：2014-07-01
申请号：US13581800
申请日：2011-02-08
申请人： Yasufumi Matsumura , Ryuzo Shinta , Yasushi Enomoto
发明人： Yasufumi Matsumura , Ryuzo Shinta , Yasushi Enomoto
IPC分类号： C08J7/00 , C08J7/12 , C08J7/14 , C08K3/08 , C08L79/08
CPC分类号： C08J7/00 , B22F9/20 , C08G73/1042 , C08G73/1067 , C08J7/08 , C08J7/14 , C08K3/08 , C08L79/08 , C09D5/30 , C09D5/32 , C09D7/69 , C22C1/1026 , C22C32/0094 , C22C2001/1089 , C23C18/08 , H01B1/22 , Y10S977/778 , Y10S977/90
摘要： A metal nanoparticle composite is provided, in which a matrix resin layer and metal nanoparticles are immobilized on the matrix resin layer. The metal nanoparticle composite has the following characteristics: a) the metal nanoparticles are obtained by heat-reducing metal ions or metal salts contained in the matrix resin layer or a precursor resin layer thereof; b) the metal nanoparticles exist within a region from the surface of the matrix resin layer to a depth of at least 50 nm; c) particle diameters of the metal nanoparticles are in the range of 1 nm to 100 nm with the mean particle diameter of greater than and equal to 3 nm; and d) a spacing between adjacent metal nanoparticles is greater than and equal to the particle diameter of a larger one of the adjacent metal nanoparticles.
摘要翻译：提供了一种金属纳米颗粒复合材料，其中将基体树脂层和金属纳米颗粒固定在基体树脂层上。金属纳米粒子复合体具有以下特征：a）金属纳米粒子是通过将金属离子或基体树脂层中含有的金属盐或其前体树脂层进行还原而得到的， b）金属纳米粒子存在于从基体树脂层的表面到至少50nm的深度的区域内; c）金属纳米粒子的粒径在1nm〜100nm的范围内，平均粒径大于等于3nm; 和d）相邻的金属纳米颗粒之间的间距大于并且等于较大的相邻金属纳米颗粒的粒径。

13. 发明授权

US08133549B2 Method for modifying insulating or semi-conductive surfaces, and resulting products 有权
标题翻译：用于改变绝缘或半导体表面的方法以及所得产品
公开(公告)号：US08133549B2
公开(公告)日：2012-03-13
申请号：US12091894
申请日：2006-10-09
申请人： Christophe Bureau , Jean Pinson
发明人： Christophe Bureau , Jean Pinson
IPC分类号： C08F2/00 , C08J7/00 , H01L21/31
CPC分类号： H01L21/306 , C08J7/12 , C08J2323/10 , C08J2371/10
摘要： The present invention relates to the use of a R—N2+ diazonium salt carrying an aromatic group R, for grafting of the aromatic group onto insulating, semiconductor, binary or ternary compound or composite material surfaces, the diazonium salt being present at a concentration close to its solubility limit, notably at a concentration higher than 0.05 M, and preferably varying between approximately 0.5 M to approximately 4 M.
摘要翻译：本发明涉及携带芳族基团R的R-N2 +重氮盐用于将芳族基团接枝到绝缘，半导体，二元或三元化合物或复合材料表面上的用途，重氮盐以接近其溶解度极限，特别是在高于0.05M的浓度下，优选在约0.5M至约4M之间变化。

14. 发明申请

US20100227119A1 PROCESS FOR PLASMA COATING A POLYPROPYLENE OBJECT 审中-公开
标题翻译：聚丙烯等离子体涂料的工艺
公开(公告)号：US20100227119A1
公开(公告)日：2010-09-09
申请号：US12682952
申请日：2008-10-08
申请人： Angela Taha , Christopher M. Weikart , Hoang T. Pham , Terry W. Glass , Matthew Larive , Jason C. Brodil
发明人： Angela Taha , Christopher M. Weikart , Hoang T. Pham , Terry W. Glass , Matthew Larive , Jason C. Brodil
IPC分类号： B32B3/00 , C08J7/00 , B05D7/24 , B29C59/00
CPC分类号： B05D7/02 , B05D1/62 , B29B11/08 , B29B11/14 , B29B2911/1402 , B29B2911/14026 , B29B2911/14033 , B29B2911/1404 , B29B2911/14106 , B29B2911/14133 , B29B2911/1498 , B29C49/0073 , B29C49/06 , B29C49/08 , B29K2023/12 , B29K2105/258 , B29K2995/0022 , B29K2995/0073 , C08J7/18 , C08J2323/10 , C08J2483/04 , C23C16/02 , C23C16/045 , C23C16/401 , Y10T428/24355
摘要： A process for improving the barrier performance of a plasma coated object comprising a polyolefin is disclosed. The process involves ensuring that the surface of the object to be coated is smooth as characterized by having a root-mean-square surface roughness that varies by less than the thickness of the coating to be applied, typically less than 100 nm. The invention also relates to a process for improving the stain resistance of polyolefin based articles comprising plasma polymerizing an organosilicon compound under conditions to deposit a polyorganosiloxane layer onto the article and/or (b) plasma polymerizing a organosilicon compound under conditions to deposit a silicon oxide layer directly on the article or onto a polyorganosiloxane layer prepared according to step (a).
摘要翻译：公开了一种用于改善包含聚烯烃的等离子涂覆物体的阻隔性能的方法。该方法包括确保要涂覆的物体的表面是光滑的，其特征在于具有通常小于100nm的涂层的厚度变化小于等于100nm的均方根表面粗糙度。本发明还涉及一种改善聚烯烃基制品的耐污性的方法，其包括在将聚有机硅氧烷层沉积到制品上的条件下等离子体聚合有机硅化合物和/或（b）在沉积氧化硅的条件下等离子体聚合有机硅化合物层直接在物品上或根据步骤（a）制备的聚有机硅氧烷层上。

15. 发明授权

US07550521B2 Toughening of thermosets 失效
标题翻译：热固性增韧
公开(公告)号：US07550521B2
公开(公告)日：2009-06-23
申请号：US10519251
申请日：2003-06-27
申请人： Ho Sung Kim , Nam Ho Kim
发明人： Ho Sung Kim , Nam Ho Kim
IPC分类号： C08L63/00 , C08J9/00 , C08J7/00 , B32B27/38
CPC分类号： C08J9/32 , B29C70/66 , C08J2203/22 , C08J2363/00 , C08K7/22
摘要： A method of manufacturing thermosets such as epoxy resins includes adding expandable hollow microspheres, which expand with temperature as shown in the accompanying graph, to the base thermoset components in the liquid phase and applying heat treatment to the mixture so formed causing the micropsheres to expand during or after curing of the thermoset. This results in a toughening mechanism caused by compressive residual stress around the microspheres which significantly increases the specific fracture energy of the epoxy resin.
摘要翻译：制造诸如环氧树脂的热固性材料的方法包括将如附图所示的随温度膨胀的可膨胀中空微球体添加到液相中的基础热固性组分，并对如此形成的混合物进行热处理，导致微球体膨胀或固化后的热固性材料。这导致由微球附近的压缩残余应力引起的增韧机理，这显着增加了环氧树脂的特定断裂能。

16. 发明申请

US20070212496A1 Process for Producing Metal Nonoparticle Composite Film 审中-公开
标题翻译：生产金属非颗粒复合膜的工艺
公开(公告)号：US20070212496A1
公开(公告)日：2007-09-13
申请号：US10595398
申请日：2004-10-13
申请人： Satoshi Tomita , Hidemi Nawafune , Kensuke Akamatsu
发明人： Satoshi Tomita , Hidemi Nawafune , Kensuke Akamatsu
IPC分类号： C08J7/00
CPC分类号： C08J7/06 , B82B3/00 , C08J7/12 , C08J7/14 , C08J2379/08
摘要： The present invention provides a process for producing a metal nanoparticle composite film, which is capable of independently controlling the particle diameter and the volume filling ratio of metal nanoparticles in the metal nanoparticle composite film. The process comprises the steps of (a) treating a polyimide resin film with an alkali aqueous solution to thereby introduce a carboxyl group, (b) bringing the resin film into contact with a solution containing metal ions, to thereby dope the metal ions in the resin film, and (c) performing thermal reduction treatment in a reducing gas, thereby producing the metal nanoparticle composite film containing the metal nanoparticles dispersed in the polyimide resin film, wherein the volume filling ratio of the metal nanoparticles in the composite film is controlled by regulating the thickness of a nanoparticle dispersed layer formed in the polyimide resin film with the thermal reduction treatment in the reducing gas in the step (c).
摘要翻译：本发明提供一种能够独立地控制金属纳米粒子复合膜中的金属纳米粒子的粒径和体积填充率的金属纳米粒子复合膜的制造方法。该方法包括以下步骤：（a）用碱水溶液处理聚酰亚胺树脂膜，从而引入羧基，（b）使树脂膜与含有金属离子的溶液接触，从而将金属离子掺入树脂膜，（c）在还原气体中进行热还原处理，由此制造含有分散在聚酰亚胺树脂膜中的金属纳米粒子的金属纳米粒子复合膜，其中复合膜中的金属纳米粒子的体积填充率由通过步骤（c）中的还原气体中的热还原处理来调节在聚酰亚胺树脂膜中形成的纳米粒子分散层的厚度。

17. 发明申请

US20050267229A1 Method for producing poly(methyl methacrylate)-metal cluster composite 审中-公开
标题翻译：聚（甲基丙烯酸甲酯） - 金属簇复合材料的生产方法
公开(公告)号：US20050267229A1
公开(公告)日：2005-12-01
申请号：US10527052
申请日：2003-09-03
申请人： Shin Horiuchi
发明人： Shin Horiuchi
IPC分类号： C08J7/00 , B22F9/20 , C08J7/06 , C23C16/04 , C23C16/44 , C08K3/00
CPC分类号： C23C16/047 , C08J7/06 , C08J2333/12
摘要： A process for efficiently producing a poly(methyl methacrylate)-metal cluster composite, a patterning material obtainable by the process, and its patterning method are provided. The poly(methyl methacrylate)-metal cluster composite is obtained by bringing a poly(methyl methacrylate) base plate having an ultraviolet-irradiated portion into contact with vapor of a heavy metal compound to form heavy metal nanoparticles on the ultraviolet-irradiated portion.
摘要翻译：提供了一种有效生产聚（甲基丙烯酸甲酯） - 金属簇复合物的方法，可通过该方法获得的图案形成材料及其图案化方法。通过使具有紫外线照射部分的聚甲基丙烯酸甲酯基板与重金属化合物的蒸气接触，在紫外线照射部分上形成重金属纳米粒子，得到聚（甲基丙烯酸甲酯） - 金属簇复合物。

18. 发明申请

US20050247402A1 Adhesive film 审中-公开
标题翻译：胶粘膜
公开(公告)号：US20050247402A1
公开(公告)日：2005-11-10
申请号：US10525067
申请日：2003-08-20
申请人： Toru Fujiki , Toshiki Mori , Toshiyuki Hasegawa , Hironobu Iyama
发明人： Toru Fujiki , Toshiki Mori , Toshiyuki Hasegawa , Hironobu Iyama
IPC分类号： C08J7/00 , B29C47/00 , B32B27/28 , C08G59/42 , C08K5/00 , C08L23/08 , C08L63/00 , C09J7/00 , C09J123/02 , C09J123/08 , C09J163/00 , B32B31/00
CPC分类号： C09J123/0884 , C08L23/0869 , C08L2666/06 , C09J7/10 , C09J2423/00
摘要： The present invention provides an adhesive film obtainable by irradiating electron beam on a molded article obtainable by molding a resin composition comprising components (A) and (B), the storage method of the film and a laminate comprising the adhesive film and an adherent. Component (A) is an epoxy group-containing copolymer obtainable by polymerizing, wherein (a1) is ethylene and/or propylene, and (a2)is a monomer represented by formula (1): (wherein R represents a hydrocarbon group of a carbon number of 2 to 18 having a double bond, wherein at least one of hydrogen atoms of the hydrocarbon group may be substituted with a halogen atom, a hydroxyl group or a carboxyl group, and X represents a single bond or a carbonyl group). Component (B) is a copolymer obtainable by polymerizing (b1) and (b2), wherein (b1) is ethylene and/or propylene, and (b2) is α,β-unsaturated carboxylic acid anhydride.
摘要翻译：本发明提供一种通过将成型品（A）和（B）的树脂组合物成型而得到的成型品照射到电子束上的粘合膜，该膜的保存方法以及包含粘合膜和粘合剂的层压体。组分（A）是通过聚合可获得的含环氧基的共聚物，其中（a 1→1）是乙烯和/或丙烯，（a 2 S 2）是表示的单体式（1）表示：（式中，R表示碳原子数2〜18的具有双键的烃基，其中，所述烃基的氢原子中的至少一个可以被卤原子取代，羟基或羧基，X表示单键或羰基）。组分（B）是通过聚合（b 1→1）和（b 2/2）获得的共聚物，其中（b 1）是乙烯和/ 或丙烯，和（b 2 H 2）是α，β-不饱和羧酸酐。

19. 发明申请

US20050183747A1 Method for reducing contact angle of water on TAC film 审中-公开
标题翻译：降低TAC膜接触角的方法
公开(公告)号：US20050183747A1
公开(公告)日：2005-08-25
申请号：US10949188
申请日：2004-09-27
申请人： Yi-Ping Wang , Yao-Chung Cheng , Ming-Chih Shih
发明人： Yi-Ping Wang , Yao-Chung Cheng , Ming-Chih Shih
IPC分类号： C08J7/12 , B08B3/00 , B08B3/08 , C08J5/18 , C08J7/00 , C08J7/02 , C08J7/14 , G03C1/735
CPC分类号： B08B3/08 , C08J7/02 , C08J7/047 , C08J7/12 , C08J2301/02 , C08J2301/12 , C08J2429/04
摘要： A TAC film pre-processing method for reducing the contact angle of water on the TAC film is described. In this method, the TAC film is first passed through a base tank to perform a base cleaning process. Next, the TAC film is passed through a first rinse tank to perform a first water cleaning process. The TAC film is then passed through an acid tank to perform an acid cleaning process. Finally, the TAC film is passed through a second rinse tank to performing a second water cleaning process. Alcohol is added at a predetermined concentration to the second rinse tank. The alcohol includes IPA (isopropyl alcohol). The predetermined concentration range of the alcohol is from about 4% to 6%.
摘要翻译：描述了用于降低TAC膜上的水的接触角的TAC膜预处理方法。在该方法中，首先将TAC膜通过基底罐进行基底清洗处理。接下来，将TAC膜通过第一冲洗槽进行第一次水清洗处理。然后将TAC膜通过酸槽进行酸清洗处理。最后，将TAC膜通过第二冲洗槽进行第二次水清洗过程。将醇以预定浓度加入到第二冲洗槽中。酒精包括IPA（异丙醇）。醇的预定浓度范围为约4％至6％。

20. 发明申请

US20050168374A1 Molded component for beam path of radar apparatus 失效
标题翻译：雷达装置的光束路径成型部件
公开(公告)号：US20050168374A1
公开(公告)日：2005-08-04
申请号：US11042113
申请日：2005-01-26
申请人： Itsuo Kamiya , Izumi Takahashi , Hideo Kamiya , Koichi Tanaka
发明人： Itsuo Kamiya , Izumi Takahashi , Hideo Kamiya , Koichi Tanaka
IPC分类号： B60R19/52 , B60R11/02 , C08J7/00 , G01S7/03 , G01S13/93 , H01P1/08 , H01Q1/22 , H01Q1/32 , H01Q1/42 , H01Q1/44 , H01Q17/00
CPC分类号： H01Q1/44 , B60R11/02 , G01S7/03 , G01S2013/9375 , H01Q1/3233 , H01Q1/3283 , H01Q1/42
摘要： A molded component for the beam path of a radar apparatus with low radio transmission loss and improved hardness and abrasion resistance is provided. The molded component for the beam path of the radar apparatus comprises a base body 1 composed of a resin layer, and a bright decoration layer 2 disposed on the surface of the base body, the bright decoration layer being composed of tin and/or a tin alloy.
摘要翻译：提供了具有低无线电传输损耗和改进的硬度和耐磨性的雷达装置的光束路径的模制部件。用于雷达装置的光束路径的模制部件包括由树脂层构成的基体1和设置在基体表面上的明亮装饰层2，明亮的装饰层由锡和/或锡组成合金。

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