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    • 12. 发明授权
    • Method of preparation of 2,6-bis(picrylamino)-3,5-dinitropyridine
    • 制备2,6-二(辛基氨基)-3,5-二硝基吡啶的方法
    • US4948897A
    • 1990-08-14
    • US335158
    • 1989-04-07
    • Robert S. Riggs
    • Robert S. Riggs
    • C07D213/74
    • C07D213/74
    • A method for preparing 2,6-bis(picrylamino)-3,5-dinitropyridine (PYX) which includes the steps of first dissolving crystalline PYX in a primary solvent in which the solvent used is selected from the group consisting of pyridine, dimethylformamide, methylsulfoxide or mixtures thereof. The primary solvent system is then combined with a second solvent in which the PYX is substantially insoluble, but which, in admixture with the primary solvent, forms a true solution of the PYX, referred to as the secondary solution. A third solvent is then added to the binary solvent system, which third solvent is soluble with the binary solvent system but which promotes precipitation of PYX in a form which exhibits improved characteristics as an explosive.
    • 一种制备2,6-二(picrylamino)-3,5-二硝基吡啶(PYX)的方法,其包括首先将结晶PYX溶解在其中使用的溶剂中的溶剂中的结晶PYX选自吡啶,二甲基甲酰胺, 甲基亚砜或其混合物。 然后将主要溶剂体系与其中PYX基本上不溶的第二溶剂组合,但与主溶剂混合形成称为第二溶液的PYX的真实溶液。 然后将第三溶剂加入到二元溶剂系统中,其中第三溶剂可溶于二元溶剂体系,但促进PYX以表现出爆炸性能改善的形式的沉淀。
    • 13. 发明授权
    • Apparatus and method for feeding strip material for application to a drum
    • 用于将条带材料供给到滚筒中的装置和方法
    • US4617074A
    • 1986-10-14
    • US711652
    • 1985-03-14
    • Steven J. PortalupiRobert S. Riggs
    • Steven J. PortalupiRobert S. Riggs
    • B29D30/30
    • B29D30/3007B65H2801/93Y10T83/6579
    • An apparatus and method wherein strip material is clamped to a shuttle finger slidably mounted in a shuttle casing which in turn is slidably mounted on a strip applier frame. The shuttle casing and shuttle finger are movable simultaneously from a retracted first position to a second position with the end of the shuttle casing adjacent an applicator roll. The shuttle finger is then movable by itself from the second position to a third position for transferring a tongue portion of the strip onto the applicator roll. The tongue portion may then be elevated into clamping engagement with the drum and the strip released from the shuttle finger. The shuttle casing and shuttle finger may then be returned to the first position, the drum rotated a predetermined amount to partially wrap the strip around the drum and the strip cut at a predetermined location whereupon the drum is rotated to fully wrap the strip of flexible material around the drum. Guide members at the front edges of the feed path are retractable to permit movement of the shuttle casing into close proximity with the applicator roll. Also a cycle reset clamping assembly is provided for clamping a portion of the strip of flexible material to the applicator roll to allow the shuttle casing to move to the retracted position for cutting of the strip of flexible material in that position when the applicator roll is not elevated into contact with the drum.
    • 一种装置和方法,其中条带材料被夹紧到可滑动地安装在梭壳中的梭形手指,所述往复式壳体又可滑动地安装在带状施加器框架上。 穿梭套管和梭梭可以从缩回的第一位置同时移动到第二位置,同时梭壳的端部与施加辊相邻。 穿梭手指然后可以自身从第二位置移动到第三位置,用于将条带的舌部传送到涂抹辊上。 然后可以将舌部升高成与鼓和从梭指释放的带的夹紧接合。 穿梭套管和穿梭手指然后可以返回到第一位置,滚筒旋转预定量以将带围绕滚筒部分包裹,并且条带在预定位置切割,从而滚筒旋转以完全包裹柔性材料条 围绕鼓。 在进给路径的前边缘处的引导构件是可缩回的,以允许梭壳运动靠近施胶辊。 还提供了一种循环复位夹紧组件,用于将柔性材料条的一部分夹紧到施加辊上,以允许梭壳移动到缩回位置,以在施加辊不是时在该位置切割柔性材料条 升高与鼓接触。