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11. 发明申请

US20080033174A1 Method for the Production of 3-Phenyl (Thio) Uracils and Dithiouracils 有权
标题翻译： 3-苯基（硫脲）尿嘧啶和二硫尿嘧啶的制备方法
公开(公告)号：US20080033174A1
公开(公告)日：2008-02-07
申请号：US11631972
申请日：2005-07-13
申请人： Sandra Lohr , Joachim Gebhardt , Guido Mayer , Michael Keil , Thomas Schmidt , Bernd Wolf
发明人： Sandra Lohr , Joachim Gebhardt , Guido Mayer , Michael Keil , Thomas Schmidt , Bernd Wolf
IPC分类号： C07D239/10 , C07C313/18
CPC分类号： C07D239/54
摘要： The present invention relates to a process for preparing 3-phenyl(thio)uracils and -dithiouracils of the formula I where the variables are each as defined in the description, and also intermediates for their preparation.
摘要翻译：本发明涉及一种制备式I的3-苯基（硫代）尿嘧啶和二硫尿嘧啶的方法，其中各变量各自如说明书中所定义，以及它们制备的中间体。

12. 发明授权

US09920002B2 Methods for producing sulfonic acid diamides 有权
公开(公告)号：US09920002B2
公开(公告)日：2018-03-20
申请号：US12681843
申请日：2008-10-10
申请人： Axel Pleschke , Thomas Schmidt , Joachim Gebhardt , Sandra Loehr , Michael Keil , Jan Hendrik Wevers
发明人： Axel Pleschke , Thomas Schmidt , Joachim Gebhardt , Sandra Loehr , Michael Keil , Jan Hendrik Wevers
IPC分类号： C07C303/34 , C07C307/06 , C07D239/54 , A01N43/54 , C07C381/00
CPC分类号： C07C303/34 , A01N43/54 , C07C307/06 , C07C381/00 , C07D239/54
摘要： The present invention relates to a process for preparing sulfuric diamides of the general formula I R1R2N—S(O)2—NH2 (I) in which R1 and R2 are each independently a primary alkyl radical having from 1 to 8 carbon atoms, a secondary alkyl radical having from 3 to 8 carbon atoms or a cycloalkyl radical having from 5 to 8 carbon atoms, or, together with the nitrogen atom, form a 5- to 8-membered, saturated nitrogen heterocycle which, as well as the nitrogen atom, may have a further heteroatom selected from O and S as a ring member, where the nitrogen heterocycle is unsubstituted or may have 1, 2, 3 or 4 alkyl groups having in each case from 1 to 4 carbon atoms as substituents. The process comprises the following steps: i) the reaction of a secondary amine of the formula II R1R2NH (II) in which R1 and R2 are each as defined above with sulfuryl chloride in an inert solvent, especially an aromatic solvent, in the presence of a tertiary amine to give a sulfamoyl chloride of the formula III R1R2N—S(O)2—Cl (III) in which R1 and R2 are each as defined above, and ii) reaction of the sulfamoyl chloride of the formula III obtained in step i) with ammonia, the sulfamoyl chloride of the formula III being used in step ii) in the form of the solution obtained in step i) in the inert solvent, especially the aromatic solvent.

13. 发明申请

US20080293941A1 Method For Production Of 1-Alkyl-3-Phenyluracils 有权
标题翻译： 1-烷基-3-苯基尿嘧啶的制备方法
公开(公告)号：US20080293941A1
公开(公告)日：2008-11-27
申请号：US11913208
申请日：2006-05-18
申请人： Joachim Gebhardt , Sandra Lohr , Michael Keil , Thomas Schmidt , Jan Hendrik Wevers , Helmut Zech , Rudolf Haberler
发明人： Joachim Gebhardt , Sandra Lohr , Michael Keil , Thomas Schmidt , Jan Hendrik Wevers , Helmut Zech , Rudolf Haberler
IPC分类号： C07D239/54
CPC分类号： C07D239/54
摘要： The present invention relates to a process for preparing 1-alkyl-3-phenyluracils of the formula I where the variables R1 to R7 are as defined in the description by reacting 3-phenyluracils of the formula II and alkylating agents of the formula III R1-L1 III, with one another, wherein during the entire reaction the pH is kept in a range from 1 to 6 by adding base a little at a time.
摘要翻译：本发明涉及一种制备式I的1-烷基-3-苯基尿嘧啶的方法，其中变量R1至R7如说明书中所定义，通过使式II的3-苯基尿嘧啶与式III的烷基化剂反应， in-line-formula description =“In-line Formulas”end =“lead”？> R1-L1 III，<？in-line-formula description =“In-line Formulas”end =“tail”？> ，其中在整个反应期间，通过一次添加碱几乎将pH保持在1至6的范围内。

14. 发明申请

US20100222586A1 Methods for Producing Sulfonic Acid Diamides 有权
标题翻译：生产磺酸二酰胺的方法
公开(公告)号：US20100222586A1
公开(公告)日：2010-09-02
申请号：US12681843
申请日：2008-10-10
申请人： Axel Pleschke , Thomas Schmidt , Joachim Gebhardt , Sandra Loehr , Michael Keil , Jan Hendrik Wevers
发明人： Axel Pleschke , Thomas Schmidt , Joachim Gebhardt , Sandra Loehr , Michael Keil , Jan Hendrik Wevers
IPC分类号： C07D239/10 , C07C309/63
CPC分类号： C07C303/34 , A01N43/54 , C07C307/06 , C07C381/00 , C07D239/54
摘要： The present invention relates to a process for preparing sulfuric diamides of the general formula I R1R2N—S(O)2—NH2 (I) in which R1 and R2 are each independently a primary alkyl radical having from 1 to 8 carbon atoms, a secondary alkyl radical having from 3 to 8 carbon atoms or a cycloalkyl radical having from 5 to 8 carbon atoms, or, together with the nitrogen atom, form a 5- to 8-membered, saturated nitrogen heterocycle which, as well as the nitrogen atom, may have a further heteroatom selected from O and S as a ring member, where the nitrogen heterocycle is unsubstituted or may have 1, 2, 3 or 4 alkyl groups having in each case from 1 to 4 carbon atoms as substituents. The process comprises the following steps: i) the reaction of a secondary amine of the formula II R1R2NH (II) in which R1 and R2 are each as defined above with sulfuryl chloride in an inert solvent, especially an aromatic solvent, in the presence of a tertiary amine to give a sulfamoyl chloride of the formula III R1R2N—S(O)2—Cl (III) in which R1 and R2 are each as defined above, and ii) reaction of the sulfamoyl chloride of the formula III obtained in step i) with ammonia, the sulfamoyl chloride of the formula III being used in step ii) in the form of the solution obtained in step i) in the inert solvent, especially the aromatic solvent.
摘要翻译：本发明涉及制备通式为R 1 R 2 N-S（O）2 -NH 2（I）的硫酸二酰胺的方法，其中R 1和R 2各自独立地为具有1至8个碳原子的伯烷基，二级具有3至8个碳原子的烷基或具有5至8个碳原子的环烷基，或与氮原子一起形成5-8元饱和氮杂环，其氮原子，可以具有选自O和S的另外的杂原子作为环成员，其中氮杂环是未取代的或可以具有1,2,3或4个烷基，每个情况下具有1至4个碳原子作为取代基。该方法包括以下步骤：i）在惰性溶剂，特别是芳族溶剂中，在惰性溶剂，特别是芳族溶剂的存在下，使式II的R 1 R 2 NH（II）的仲胺与R 1和R 2各自如上所述与磺酰氯反应，得到式III的R 1 R 2 N-S（O）2 -C（III）的氨磺酰氯，其中R 1和R 2各自如上所定义，和ii）在步骤（a）中获得的式III的氨磺酰氯的反应， i）与氨，式III的氨磺酰氯以步骤ⅱ）中的步骤i）中获得的溶液的形式在惰性溶剂中，特别是芳族溶剂中使用。

15. 发明授权

US07847097B2 Method for production of 1-alkyl-3-phenyluracils 有权
标题翻译： 1-烷基-3-苯基尿嘧啶的制备方法
公开(公告)号：US07847097B2
公开(公告)日：2010-12-07
申请号：US11913208
申请日：2006-05-18
申请人： Joachim Gebhardt , Sandra Loehr , Michael Keil , Thomas Schmidt , Jan Hendrik Wevers , Helmut Zech , Rudolf Haeberle
发明人： Joachim Gebhardt , Sandra Loehr , Michael Keil , Thomas Schmidt , Jan Hendrik Wevers , Helmut Zech , Rudolf Haeberle
IPC分类号： C07D239/54
CPC分类号： C07D239/54
摘要： The present invention relates to a process for preparing 1-alkyl-3-phenyluracils of the formula I where the variables R1 to R7 are as defined in the description by reacting 3-phenyluracils of the formula II and alkylating agents of the formula III R1-L1 III, with one another, wherein during the entire reaction the pH is kept in a range from 1 to 6 by adding base a little at a time.
摘要翻译：本发明涉及一种制备式I的1-烷基-3-苯基尿嘧啶的方法，其中变量R1至R7如说明书中所定义，通过使式II的3-苯基尿嘧啶和式III的1-烷基化剂R1- L1 III，彼此之间，其中在整个反应期间，通过一次添加碱几乎将pH保持在1至6的范围内。

16. 发明授权

US07232926B2 Method for the production of sulphamic acid halogenides 有权
标题翻译：制备氨基磺酸卤化物的方法
公开(公告)号：US07232926B2
公开(公告)日：2007-06-19
申请号：US10513668
申请日：2003-05-15
申请人： Gerhard Hamprecht , Michael Puhl , Robert Reinhard , Ingo Sagasser , Thomas Schmidt , Norbert Götz , Thomas Zierke
发明人： Gerhard Hamprecht , Michael Puhl , Robert Reinhard , Ingo Sagasser , Thomas Schmidt , Norbert Götz , Thomas Zierke
IPC分类号： C07C19/00 , C07D239/02
CPC分类号： C07D295/26 , C07C303/34 , C07C307/00 , C07C2601/14 , C07D207/48 , C07D211/96 , C07D239/46
摘要： The present invention relates to a process for preparing sulfamoyl halides of primary or secondary amines, comprising the following steps: i) reacting a primary or secondary amine A1 with at least equimolar amounts of SO3 or an SO3 source in the presence of at least equimolar amounts of a tertiary amine A2, based in each case on the amine A1, and ii) reacting the reaction mixture obtained in step i) with at least the amount of a phosphorus halide required by the stoichiometry; The invention further relates to a process for preparing sulfonic diamides, comprising the preparation of sulfamoyl halides by means of carrying out steps i) and ii) and subsequently reacting the sulfamoyl halide obtained with ammonia. The invention further relates to the use of this process for preparing active herbicidal ingredients having a sulfuric diamide structure. The invention further relates to novel sulfamoyl chlorides.
摘要翻译：本发明涉及一种制备伯胺或仲胺的氨磺酰卤的方法，包括以下步骤：i）使伯胺或仲胺A1与至少等摩尔量的SO 3或SO 3反应，在至少等摩尔量的叔胺A2的存在下，基于胺A1，基于每种情况，并且ii）使步骤i）中获得的反应混合物与至少一定量的化学计量所需的卤化磷; 本发明还涉及制备磺酰二酰胺的方法，其包括通过进行步骤i）和ii）制备氨磺酰卤，随后使所得氨磺酰卤与氨反应。本发明还涉及该方法用于制备具有硫酸二酰胺结构的活性除草成分的用途。本发明还涉及新的氨磺酰氯。

17. 发明申请

US20050159622A1 Method for the production of sulphamic acid halogenides 有权
标题翻译：制备氨基磺酸卤化物的方法
公开(公告)号：US20050159622A1
公开(公告)日：2005-07-21
申请号：US10513668
申请日：2003-11-27
申请人： Gerhard Hamprecht , Michael Puhl , Robert Reinhard , Ingo Sagasser , Thomas Schmidt , Norbert Gotz , Thomas Zierke
发明人： Gerhard Hamprecht , Michael Puhl , Robert Reinhard , Ingo Sagasser , Thomas Schmidt , Norbert Gotz , Thomas Zierke
IPC分类号： C07D239/54 , C07C303/34 , C07C303/38 , C07C303/40 , C07C307/00 , C07C307/06 , C07C307/08 , C07C307/10 , C07D207/48 , C07D211/96 , C07D239/46 , C07D295/26 , C07C33/38
CPC分类号： C07D295/26 , C07C303/34 , C07C307/00 , C07C2601/14 , C07D207/48 , C07D211/96 , C07D239/46
摘要： The present invention relates to a process for preparing sulfamoyl halides of primary or secondary amines, comprising the following steps: i) reacting a primary or secondary amine Al with at least equimolar amounts of SO3 or an SO3 source in the presence of at least equimolar amounts of a tertiary amine A2, based in each case on the amine A1, and ii) reacting the reaction mixture obtained in step i) with at least the amount of a phosphorus halide required by the stoichiometry; The invention further relates to a process for preparing sulfonic diamides, comprising the preparation of sulfamoyl halides by means of carrying out steps i) and ii) and subsequently reacting the sulfamoyl halide obtained with ammonia. The invention further relates to the use of this process for preparing active herbicidal ingredients having a sulfuric diamide structure. The invention further relates to novel sulfamoyl chlorides.
摘要翻译：本发明涉及一种制备伯胺或仲胺的氨磺酰卤的方法，包括以下步骤：i）使伯胺或仲胺A1与至少等摩尔量的SO 3或SO 3反应，在至少等摩尔量的叔胺A2的存在下，基于胺A1，基于每种情况，并且ii）使步骤i）中获得的反应混合物与至少一定量的化学计量所需的卤化磷; 本发明进一步涉及一种制备磺酰二酰胺的方法，包括通过进行步骤i）和ii）制备氨磺酰卤，随后使得到的氨磺酰卤与氨反应。本发明还涉及该方法用于制备具有硫酸二酰胺结构的活性除草成分的用途。本发明还涉及新的氨磺酰氯。

18. 发明授权

US08628684B2 Process for the preparation of a powder comprising one or more derivatives of glycine-N,N diacetic acid and/or one or more derivatives of glutamine-N,N diacetic acid and methylglycine-N,N diacetic acid trisodium salt powder 有权
标题翻译：制备包含甘氨酸-N，N二乙酸和/或谷氨酰胺-N，N-二乙酸和甲基甘氨酸-N，N二乙酸三钠盐粉末的一种或多种衍生物的一种或多种衍生物的粉末的方法
公开(公告)号：US08628684B2
公开(公告)日：2014-01-14
申请号：US13318513
申请日：2010-05-19
申请人： Frank Mrzena , Hans-Juergen Kinder , Michael Schoenherr , Gerhard Cox , Thomas Schmidt , Volker Huett
发明人： Frank Mrzena , Hans-Juergen Kinder , Michael Schoenherr , Gerhard Cox , Thomas Schmidt , Volker Huett
IPC分类号： C09K3/00 , C07C61/08
CPC分类号： C07C229/24 , C07B2200/13 , C07C227/42 , C07C229/16
摘要： A process is proposed for the preparation of a powder comprising one or more derivatives of glycine-N,N-diacetic acid and/or one or more derivatives of glutamine-N,N-diacetic acid with a degree of crystallinity of ≧30%,starting from an aqueous solution comprising the one or more derivatives of glycine-N,N-diacetic acid and/or the one or more derivatives of glutamine-N,N-diacetic acid in a concentration range from 20 to 60% by weight, based on the total weight of the aqueous solution, where the aqueous solution is concentrated in a first process step in an evaporator with rotating internals, which are arranged at a distance relative to the inside wall of the evaporator of ≦1% of the diameter of the evaporator, to give a crystal slurry with a solids concentration in the range from 60 to 85% by weight, based on the total weight of the crystal slurry, and where in a second process step the crystal slurry is left to ripen in a paste bunker and then in a thin-film contact dryer, and where the residence time in the paste bunker and in the thin-film contact dryer is in total ≧15 minutes.
摘要翻译：提出了制备包含一种或多种甘氨酸-N，N-二乙酸衍生物和/或谷氨酰胺-N，N-二乙酸衍生物的结晶度> 30％的粉末的方法，从包含甘氨酸-N，N-二乙酸的一种或多种衍生物和/或浓度为20至60重量％的谷氨酰胺-N，N-二乙酸的一种或多种衍生物的水溶液开始，基于所述水溶液的总重量，其中所述水溶液在具有旋转内部件的蒸发器中的第一工艺步骤中被浓缩，所述蒸发器相对于所述蒸发器的内壁相对于所述蒸发器的所述内壁的一定距离设置，蒸发器，得到基于晶体浆料的总重量的固体浓度为60至85重量％的晶体浆料，并且其中在第二工艺步骤中，使晶体浆料以糊状物成熟地堡，然后在薄膜接触式烘干机中，以及哪里在糊状掩模和薄膜接触式干燥器中的停留时间总共> = 15分钟。

19. 发明申请

US20120046491A1 PROCESS FOR THE PREPARATION OF A POWDER COMPRISING ONE OR MORE DERIVATIVES OF GLYCINE-N,N DIACETIC ACID AND /OR ONE OR MORE DERIVATIVES OF GLUTAMINE-N,N DIACETIC ACID AND METHYLGLYCINE-N,N DIACETIC ACID TRISODIUM SALT POWDER 有权
标题翻译：制备含有GLYCINE-N，N二酸和/或一种或多种谷氨酰胺-N，N二酸和甲基甘氨酸-N，N二酸三钠盐粉末的一种或多种衍生物的粉末的制备方法
公开(公告)号：US20120046491A1
公开(公告)日：2012-02-23
申请号：US13318513
申请日：2010-05-19
申请人： Frank Mrzena , Hans-Juergen Kinder , Michael Schoenherr , Gerhard Cox , Thomas Schmidt , Volker Huett
发明人： Frank Mrzena , Hans-Juergen Kinder , Michael Schoenherr , Gerhard Cox , Thomas Schmidt , Volker Huett
IPC分类号： C07C229/24
CPC分类号： C07C229/24 , C07B2200/13 , C07C227/42 , C07C229/16
摘要： A process is proposed for the preparation of a powder comprising one or more derivatives of glycine-N,N-diacetic acid and/or one or more derivatives of glutamine-N,N-diacetic acid with a degree of crystallinity of ≧30%,starting from an aqueous solution comprising the one or more derivatives of glycine-N,N-diacetic acid and/or the one or more derivatives of glutamine-N,N-diacetic acid in a concentration range from 20 to 60% by weight, based on the total weight of the aqueous solution, where the aqueous solution is concentrated in a first process step in an evaporator with rotating internals, which are arranged at a distance relative to the inside wall of the evaporator of ≦1% of the diameter of the evaporator, to give a crystal slurry with a solids concentration in the range from 60 to 85% by weight, based on the total weight of the crystal slurry, and where in a second process step the crystal slurry is left to ripen in a paste bunker and then in a thin-film contact dryer, and where the residence time in the paste bunker and in the thin-film contact dryer is in total ≧15 minutes.
摘要翻译：提出了制备包含一种或多种甘氨酸-N，N-二乙酸衍生物和/或一种或多种结晶度为≥30％的谷氨酰胺-N，N-二乙酸衍生物的粉末的方法，从包含甘氨酸-N，N-二乙酸的一种或多种衍生物和/或浓度范围为20至60重量％的谷氨酰胺-N，N-二乙酸的一种或多种衍生物的水溶液开始，基于在水溶液的总重量中，其中水溶液在具有旋转内部件的蒸发器中的第一工艺步骤中被浓缩，所述蒸发器相对于蒸发器的内壁设置一定距离，其直径为蒸发器，得到基于晶体浆料的总重量的固体浓度为60至85重量％的晶体浆料，并且其中在第二工艺步骤中，使晶体浆料以糊状物成熟然后在薄膜接触式干燥器中，并且w 这里在糊状物掩体和薄膜接触式干燥器中的停留时间总共≥15分钟。

20. 发明授权

US09640688B2 Solar cell assembly and also solar cell arrangement 有权
公开(公告)号：US09640688B2
公开(公告)日：2017-05-02
申请号：US13386292
申请日：2010-07-19
申请人： Armin Bösch , Joachim Jaus , Andreas Bett , Gerhard Peharz , Peter Nitz , Thomas Schmidt
发明人： Armin Bösch , Joachim Jaus , Andreas Bett , Gerhard Peharz , Peter Nitz , Thomas Schmidt
IPC分类号： H01L33/52 , H01L31/048 , H01L31/02 , H01L31/0236 , H01L31/054
CPC分类号： H01L31/048 , H01L31/02008 , H01L31/0236 , H01L31/0543 , H01L2224/73265 , Y02E10/52
摘要： A light-absorbing or light-emitting solar cell assembly comprises an electrical insulator disposed on an electrically conductive substrate and that is provided with a metallized surface and at least one solar cell connected to the electrically conductive substrate, wherein the solar cell includes refractive secondary optics and is disposed in a recess in the insulator. The solar cell is connected to the substrate by the side orientated towards the substrate via an electrically conductive connection and the recess is dimensioned such that an interspace is produced laterally between the solar cell and the electrical insulator, the interspace being filled with a coupling medium and the solar cell being connected to the metallized surface by at least one electrical contact.

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