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11. 发明申请

US20130078516A1 NEGATIVE ELECTRODE MATERIAL FOR NON-AQUEOUS ELECTROLYTE SECONDARY BATTERY AND NON-AQUEOUS ELECTROLYTE SECONDARY BATTERY 有权
标题翻译：非水电解质二次电池和非水电解质二次电池负极电极材料
公开(公告)号：US20130078516A1
公开(公告)日：2013-03-28
申请号：US13618511
申请日：2012-09-14
申请人： Kazuyuki Taniguchi , Tetsuo Nakanishi
发明人： Kazuyuki Taniguchi , Tetsuo Nakanishi
IPC分类号： H01M4/60
CPC分类号： H01M4/366 , H01M4/386 , H01M4/623 , H01M4/625 , H01M2004/027 , Y02E60/122
摘要： The present invention provides a negative electrode material for a non-aqueous electrolyte secondary battery that includes particles of a silicon-based active material, the particles of a silicon-based active material being coated with a film of an organosilicon compound that contains a perfluoropolyether group, and a non-aqueous electrolyte secondary battery therewith. As a result, there is provided a negative electrode material for a non-aqueous electrolyte secondary battery that is high in capacity, excellent in initial charge/discharge efficiency and cycle characteristics and high in safety and reliability, and a non-aqueous electrolyte secondary battery that uses the negative electrode material.
摘要翻译：本发明提供一种非水电解质二次电池用负极材料，其包含硅系活性物质的粒子，所述硅系活性物质的微粒被含有全氟聚醚基的有机硅化合物膜，和非水电解质二次电池。结果，提供了一种容量高，初始充放电效率和循环特性优异，安全可靠性高的非水电解质二次电池用负极材料，非水电解质二次电池使用负极材料。

12. 发明授权

US07722995B2 Non-aqueous electrolytic solution, secondary battery, and electrochemical capacitor 有权
标题翻译：非水电解液，二次电池和电化学电容器
公开(公告)号：US07722995B2
公开(公告)日：2010-05-25
申请号：US11507529
申请日：2006-08-22
申请人： Tetsuo Nakanishi , Meguru Kashida , Satoru Miyawaki , Mikio Aramata
发明人： Tetsuo Nakanishi , Meguru Kashida , Satoru Miyawaki , Mikio Aramata
IPC分类号： H01M6/16
CPC分类号： H01M10/0567 , H01G9/035 , H01G9/038 , H01G11/64 , H01M10/0525 , H01M10/0587 , Y02E60/122 , Y02E60/13
摘要： A carbonate-modified silane or siloxane is combined with a non-aqueous solvent and an electrolyte salt to form a non-aqueous electrolytic solution, which is used to construct a secondary battery having improved charge/discharge characteristics.
摘要翻译：将碳酸酯改性的硅烷或硅氧烷与非水溶剂和电解质盐结合以形成非水电解液，其用于构建具有改进的充放电特性的二次电池。

13. 发明授权

US08105718B2 Non-aqueous electrolyte secondary battery, negative electrode material, and making method 有权
标题翻译：非水电解质二次电池，负极材料及制造方法
公开(公告)号：US08105718B2
公开(公告)日：2012-01-31
申请号：US12404710
申请日：2009-03-16
申请人： Tetsuo Nakanishi , Koichiro Watanabe , Hirofumi Fukuoka
发明人： Tetsuo Nakanishi , Koichiro Watanabe , Hirofumi Fukuoka
IPC分类号： H01M4/13 , B05D5/12
CPC分类号： H01M10/0525 , H01M4/0428 , H01M4/134 , H01M4/1395 , H01M4/364 , H01M4/366 , H01M4/386 , H01M4/483 , H01M4/622 , H01M4/625
摘要： A negative electrode material comprising an active material and 1-20 wt % of a polyimide resin binder is suitable for use in non-aqueous electrolyte secondary batteries. The active material comprises silicon oxide particles and 1-50 wt % of silicon particles. The negative electrode exhibits improved cycle performance while maintaining the high battery capacity and low volume expansion of silicon oxide. The non-aqueous electrolyte secondary battery has a high initial efficiency and maintains improved performance and efficiency over repeated charge/discharge cycles by virtue of mitigated volumetric changes during charge/discharge cycles.
摘要翻译：包含活性物质的负极材料和1-20重量％的聚酰亚胺树脂粘合剂适用于非水电解质二次电池。活性材料包括氧化硅颗粒和1-50重量％的硅颗粒。负极具有改善的循环性能，同时保持高的电池容量和低的氧化硅体积膨胀。非水电解质二次电池具有高的初始效率，并且通过在充电/放电循环期间减轻的体积变化，在重复的充电/放电循环中保持改进的性能和效率。

14. 发明申请

US20050261133A1 Glycerol-modified silicone spreading agent and a composition comprising the same 有权
标题翻译：甘油改性硅氧烷铺展剂及其组合物
公开(公告)号：US20050261133A1
公开(公告)日：2005-11-24
申请号：US11131268
申请日：2005-05-18
申请人： Tetsuo Nakanishi , Akira Yamamoto , Teruki Ikeda
发明人： Tetsuo Nakanishi , Akira Yamamoto , Teruki Ikeda
IPC分类号： A01N25/30 , C07F7/08 , C08G77/04 , C08G77/38 , A01N1/00 , A01N25/00
CPC分类号： C08G77/38 , C08G77/045
摘要： A spreading agent for agricultural chemicals, said spreading agent comprising at least one of the glycerol-modified silicone represented by the following formula (1), (2) or (3), wherein R1 can the the same with or different from each other and is selected from the group consisting of alkyl, aryl, aralkyl, and fluorinated alkyl groups each having 1 to 30 carbon atoms, p is an integer of from 1 to 3, q is an integer of 1 or 2, and r is an integer of from 0 to 6.
摘要翻译：所述铺展剂包括由下式（1），（2）或（3）表示的甘油改性硅氧烷中的至少一种，其中R 1可以是选自由各自具有1至30个碳原子的烷基，芳基，芳烷基和氟化烷基组成的组，p为1至3的整数，q为1的整数或 2，r为0〜6的整数。

15. 发明授权

US06790451B2 Cosmetic material 有权
标题翻译：化妆品
公开(公告)号：US06790451B2
公开(公告)日：2004-09-14
申请号：US10011320
申请日：2001-12-11
申请人： Tetsuo Nakanishi
发明人： Tetsuo Nakanishi
IPC分类号： A61K600
CPC分类号： A61K8/891 , A61K8/893 , A61K8/894 , A61K8/897 , A61K8/898 , A61Q1/02 , A61Q1/06 , A61Q1/10 , A61Q5/00 , A61Q15/00 , A61Q17/04 , A61Q19/00 , A61Q19/10 , C08G77/50
摘要： A cosmetic material comprising as essential cosmetic constituents (A) a silicone-branched silicone compound and (B) a silicone-branched polyether-modified silicone compound.
摘要翻译：作为必需的化妆品成分（A），硅酮支链的硅氧烷化合物和（B）硅氧烷支化的聚醚改性的硅氧烷化合物的化妆品。

16. 发明授权

US06784271B2 Odorless modified silicone compound, cosmetic preparation containing the same, and method of purifying modified silicone compound having branch polymer comprising hydrophilic group 有权
标题翻译：无水改性硅氧烷化合物，含有该化合物的化妆品，以及具有包含亲水基团的支链聚合物的改性硅氧烷化合物的纯化方法
公开(公告)号：US06784271B2
公开(公告)日：2004-08-31
申请号：US10221274
申请日：2002-09-10
申请人： Tetsuo Nakanishi
发明人： Tetsuo Nakanishi
IPC分类号： C08G7712
CPC分类号： A61K8/894 , A61Q1/02 , A61Q1/06 , A61Q1/10 , A61Q1/14 , A61Q5/00 , A61Q15/00 , A61Q17/04 , A61Q19/00 , A61Q19/04 , A61Q19/10 , C08G77/14 , C08G77/34 , C08G77/46
摘要： A modified silicone compound having a branch polymer comprising a hydrophilic group, this compound being synthesized by performing an addition reaction between an organohydrogenpolysiloxane, and at least one compound chosen from an alkenylated polyoxyalkenylated compound, an alkenylated glycerine compound and an alkenylated sugar in the presence of a platinum catalyst or rhodium catalyst, and a cosmetic material containing this modified silicone compound. This compound is purified by decomposing aldehyde condensation products remaining in the silicone by alkylating the remaining unsaturated bonds after hydrogenating the reaction liquor after said addition reaction, and treating with an aqueous solution of pH 7 or lower containing an acidic substance, or decomposing the propenyl etherated polyether in the reaction liquor after said addition reaction by treating with an aqueous solution of pH 7 or lower containing an acidic substance, and then alkylating the generated aldehydes and alkenylated ether compounds by hydrogenation. The degree of unsaturation (meq/g) in the modified silicone compound is 0.002 or less. The generation amount of aldehydes when heat ageing is performed in 0.23N hydrochloric acid at 50° C. for 0.5 hours is 70 ppm or less of the modified silicone compound.
摘要翻译：一种具有包含亲水基团的分支聚合物的改性硅氧烷化合物，该化合物是通过在有机氢聚硅氧烷和至少一种选自烯基化的聚氧化烯化的化合物，链烯基化的甘油化合物和链烯基糖的化合物之间进行加成反应而合成的，铂催化剂或铑催化剂，以及含有该改性硅酮化合物的化妆品。该化合物通过在加成反应后氢化反应液后将残留的不饱和键进行烷基化，用含有酸性物质的pH7以下的水溶液进行处理，分解存在于硅氧烷中的醛缩合产物，在通过用含有酸性物质的pH7或更低的水溶液处理之后，在所述加成反应后的反应液中的聚醚，然后通过氢化将所生成的醛和烯基醚化合物烷基化。改性硅氧烷化合物中的不饱和度（meq / g）为0.002以下。在0.23N盐酸中，在50℃下进行0.5小时热老化时的醛的产生量为70ppm以下。

17. 发明授权

US6090966A Preparation of contract mass for alkylhalosilane production and process for producing alkylhalosilanes 失效
标题翻译：制备烷基卤硅烷生产的合同质量和制备烷基卤代硅烷的方法
公开(公告)号：US6090966A
公开(公告)日：2000-07-18
申请号：US76153
申请日：1998-05-12
申请人： Tetsuo Nakanishi , Tetsuya Inukai , Kazumasa Tsukioka , Hiroshi Nakayama , Yukinori Satoh
发明人： Tetsuo Nakanishi , Tetsuya Inukai , Kazumasa Tsukioka , Hiroshi Nakayama , Yukinori Satoh
IPC分类号： B01J23/72 , B01J37/08 , C07B61/00 , C07F7/14 , C07F7/16
CPC分类号： B01J23/72 , C07F7/14
摘要： Alkylhalosilanes are produced by first fluidizing a metallic silicon powder with an inert gas, preheating the silicon powder at a temperature between 200.degree. C. and a steady reaction temperature while keeping the silicon powder fluidized, adding a copper catalyst to the preheated silicon powder to form a contact mass, and feeding an alkyl halide into the contact mass whereby the alkylhalosilanes are formed by direct synthesis. This process prevents the copper catalyst from being sintered by thermal hysteresis and activates a high catalysis on the contact mass at the start of reaction. The desired dialkyldihalosilane can be produced at a high selectivity.
摘要翻译：烷基卤代硅烷首先用惰性气体流化金属硅粉末，在保持硅粉末流动的同时在200℃和稳定的反应温度之间预热硅粉末，向预热的硅粉末中加入铜催化剂以形成接触物质，并将烷基卤化物进料到接触物质中，由此通过直接合成形成烷基卤代硅烷。该过程防止铜催化剂通过热滞后烧结，并且在反应开始时对接触质量起到高催化作用。所需的二烷基二卤硅烷可以高选择性制备。

18. 发明授权

US6025513A Preparation of alkylhalosilanes 失效
标题翻译：烷基卤硅烷的制备
公开(公告)号：US6025513A
公开(公告)日：2000-02-15
申请号：US106145
申请日：1998-06-29
申请人： Tetsuo Nakanishi , Tetsuya Inukai , Kazumasa Tsukioka , Hiroshi Nakayama , Yukinori Satoh
发明人： Tetsuo Nakanishi , Tetsuya Inukai , Kazumasa Tsukioka , Hiroshi Nakayama , Yukinori Satoh
IPC分类号： C07F7/16
CPC分类号： C07F7/16
摘要： An alkylhalosilane is prepared by charging a reactor with a contact mass comprising a metallic silicon powder and a copper catalyst, and feeding an alkyl halide into the reactor whereby the silane is formed by direct synthesis. The contact mass contains 1-10,000 ppm of elemental boron. The addition of boron to the contact mass is effective for increasing the throughput of dialkyldihalosilane at desired STY in an inexpensive manner while suppressing formation of unnecessary hydrosilanes and disilanes.
摘要翻译：通过向反应器中加入包含金属硅粉末和铜催化剂的接触物质，并将烷基卤化物进料到反应器中制备烷基卤硅烷，由此通过直接合成形成硅烷。接触质量含有1-10,000 ppm的元素硼。向接触物质中加入硼对于以便宜的方式在期望的STY下提高二烷基二卤代硅烷的通量是有效的，同时抑制不必要的氢硅烷和二硅烷的形成。

19. 发明授权

US5986123A Preparation of alkylhalosilanes 失效
标题翻译：烷基卤硅烷的制备
公开(公告)号：US5986123A
公开(公告)日：1999-11-16
申请号：US053059
申请日：1998-04-01
申请人： Hiroshi Nakayama , Tetsuo Nakanishi , Kazumasa Tsukioka , Yukinori Satoh
发明人： Hiroshi Nakayama , Tetsuo Nakanishi , Kazumasa Tsukioka , Yukinori Satoh
IPC分类号： B01J23/72 , B01J35/00 , C07B61/00 , C07F7/16
CPC分类号： C07F7/16
摘要： An alkylhalosilane is prepared by charging a reactor with a contact mass comprising a metallic silicon powder and a copper catalyst, and feeding an alkyl halide into the reactor whereby the silane is formed by direct synthesis. The use of a metallic silicon powder having a specific particle size distribution ensures effective fluidization whereby the alkylhalosilane of quality is formed at a high selectivity and in high yields.
摘要翻译：通过向反应器中加入包含金属硅粉末和铜催化剂的接触物质，并将烷基卤化物进料到反应器中制备烷基卤硅烷，由此通过直接合成形成硅烷。使用具有特定粒度分布的金属硅粉末确保有效的流化，从而以高选择性和高产率形成质量的烷基卤代硅烷。

20. 发明授权

US5847181A Preparation of alkylhalosilanes 失效
标题翻译：烷基卤硅烷的制备
公开(公告)号：US5847181A
公开(公告)日：1998-12-08
申请号：US812942
申请日：1997-03-04
申请人： Tetsuo Nakanishi , Tetsuya Inukai , Kazumasa Tsukioka , Hiroshi Nakayama , Yukinori Satoh
发明人： Tetsuo Nakanishi , Tetsuya Inukai , Kazumasa Tsukioka , Hiroshi Nakayama , Yukinori Satoh
IPC分类号： C07F7/12 , C07F7/16
CPC分类号： C07F7/16
摘要： An alkylhalosilane is prepared by charging a reactor with a contact mass comprising metallic silicon powder and a copper catalyst and feeding a reactant gas containing an alkyl halide into the reactor whereby the silane is formed by direct synthesis. A phosphorus compound is added to the contact mass in an amount of 3,000-10,000 ppm calculated as phosphorus. The invention produces a more amount of dialkyldihalosilane in a desirable STY while minimizing the amount of unnecessary disilanes.
摘要翻译：通过将包含金属硅粉末和铜催化剂的接触物质装入反应器并将含有烷基卤化物的反应气体进料到反应器中制备烷基卤硅烷，由此通过直接合成形成硅烷。按磷计算，磷化合物的量为3,000〜10000ppm。本发明在所需的STY中产生更多量的二烷基二卤硅烷，同时使不需要的二硅烷的量最小化。

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