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11. 发明申请

US20110315919A1 PRODUCTION PROCESS FOR LITHIUM-BORATE-SYSTEM COMPOUND 审中-公开
标题翻译：硼酸系统化合物的生产工艺
公开(公告)号：US20110315919A1
公开(公告)日：2011-12-29
申请号：US13255447
申请日：2010-03-04
申请人： Toshikatsu Kojima , Tetsuo Sakai , Takuhiro Miyuki , Akira Kojima , Junichi Niwa , Hitotoshi Murase
发明人： Toshikatsu Kojima , Tetsuo Sakai , Takuhiro Miyuki , Akira Kojima , Junichi Niwa , Hitotoshi Murase
IPC分类号： H01M4/04 , H01M4/525
CPC分类号： C01B35/128 , B82Y30/00 , C01P2002/72 , C01P2004/03 , C01P2004/64 , H01M4/136 , H01M4/5825 , H01M10/0525
摘要： A process is provided, process which makes it possible to produce lithium-borate-system materials by means of relatively simple means, lithium-borate-system materials which are useful as positive-electrode active materials for lithium-ion secondary battery, and the like, whose cyclic characteristics, capacities, and so forth, are improved, and which have better performance. The present production is characterized in that a divalent metallic compound including at least one member of compounds that is selected from the group consisting of divalent-iron compounds and divalent-manganese compounds, and boric acid as well as lithium hydroxide are reacted at 400-650° C. in a molten salt of a carbonate mixture comprising lithium carbonate and at least one member of alkali-metal carbonates that is selected from the group consisting of potassium carbonate, sodium carbonate, rubidium carbonate and cesium carbonate in a reducing atmosphere.
摘要翻译：提供了一种方法，其可以通过相对简单的方法生产锂 - 硼酸盐体系材料，可用作锂离子二次电池的正极活性物质等的锂 - 硼酸盐体系材料，其循环特性，能力等得到改进，具有更好的性能。本发明的特征在于，包含选自二价铁化合物和二价锰化合物的化合物中的至少一种的二价金属化合物以及硼酸以及氢氧化锂在400-650℃下反应在包含碳酸锂的碳酸盐混合物和至少一种选自碳酸钾，碳酸钠，碳酸铷和碳酸铯中的至少一种碱金属碳酸盐成分的熔融盐中的还原气氛中。

12. 发明申请

US20110291055A1 PRODUCTION PROCESS FOR LITHIUM-SILICATE-SYSTEM COMPOUND 有权
标题翻译：硅酸盐体系化合物的生产工艺
公开(公告)号：US20110291055A1
公开(公告)日：2011-12-01
申请号：US13147747
申请日：2009-11-20
申请人： Toshikatsu Kojima , Tetsuo Sakai , Takuhiro Miyuki , Yasue Okumura , Akira Kojima , Junichi Niwa , Hitotoshi Murase
发明人： Toshikatsu Kojima , Tetsuo Sakai , Takuhiro Miyuki , Yasue Okumura , Akira Kojima , Junichi Niwa , Hitotoshi Murase
IPC分类号： H01M4/58 , H01B1/18
CPC分类号： H01M4/5825 , C01B33/32 , H01M10/052 , Y02E60/122 , Y02P70/54
摘要： The present invention is one which provides a production process for lithium-silicate-system compound, the production process being characterized in that: a lithium-silicate compound being expressed by Li2SiO3 is reacted with a substance including at least one member of transition-metal elements that is selected from the group consisting of iron and manganese at 400-650° C. in a molten salt of a carbonate mixture comprising lithium carbonate and at least one member of alkali-metal carbonates that is selected from the group consisting of potassium carbonate, sodium carbonate, rubidium carbonate and cesium carbonate in a mixed-gas atmosphere including carbon dioxide and a reducing gas; and a positive-electrode active material for lithium-ion secondary battery that comprises a lithium-silicate-system compound being obtained by the aforesaid process.In accordance with the present invention, it becomes feasible to produce lithium-silicate-system materials, which are useful as positive-electrode active materials for lithium-ion secondary battery, and the like, by means of relatively simple and easy means.
摘要翻译：本发明是提供一种硅酸锂系化合物的制造方法，其制造方法的特征在于：将由Li 2 SiO 3表示的硅酸锂化合物与包含至少一种过渡金属元素的物质选自铁和锰在400-650℃的碳酸盐混合物的熔融盐中的碳酸盐混合物，所述碳酸盐混合物包含碳酸锂和至少一种碱金属碳酸盐成员，所述碱金属碳酸盐选自碳酸钾，碳酸钠，碳酸铷和碳酸铯在包括二氧化碳和还原气体的混合气体气氛中; 以及锂离子二次电池用正极活性物质，其包含通过上述方法得到的硅酸锂系化合物。根据本发明，通过相对简单且容易的手段，可以生产用作锂离子二次电池的正极活性物质等的硅酸锂系材料。

13. 发明授权

US08940436B2 Sulfur-modified polyacrylonitrile, manufacturing method therefor, and application thereof 有权
标题翻译：硫改性聚丙烯腈及其制造方法及其应用
公开(公告)号：US08940436B2
公开(公告)日：2015-01-27
申请号：US13123933
申请日：2009-10-15
申请人： Takuhiro Miyuki , Tetsuo Sakai , Junichi Niwa , Hitotoshi Murase
发明人： Takuhiro Miyuki , Tetsuo Sakai , Junichi Niwa , Hitotoshi Murase
IPC分类号： H01M4/60 , C08F20/44 , C01B31/04 , H01M4/04 , H01M4/1399 , H01M4/66 , H01M6/50 , H01M10/052
CPC分类号： C08F20/44 , C01B32/20 , C08F8/34 , H01M4/0404 , H01M4/1399 , H01M4/60 , H01M4/604 , H01M4/661 , H01M4/663 , H01M6/5088 , H01M10/052 , Y02T10/7011 , C08F120/44
摘要： Provided is a sulfur-modified polyacrylonitrile manufacturing method that is characterized in that a starting base powder that comprises sulfur powder and polyacrylonitrile powder is mixed and the mixture is heated in a non-oxidizing environment while outflow of sulfur vapor is prevented. Also provided are a cathode for lithium batteries that uses, as the active substance, the sulfur-modified polyacrylonitrile manufactured with the method, and a lithium secondary battery that includes the cathode as a component element. This enables the practical use of an inexpensive sulfur-based material as the cathode material for lithium secondary batteries, and in particular, a sulfur-based cathode material that enables higher output and has excellent cycle life characteristics, as well as other characteristics, and secondary lithium batteries using the same can be obtained.
摘要翻译：提供一种硫改性聚丙烯腈制造方法，其特征在于，将包含硫粉末和聚丙烯腈粉末的起始基础粉末混合，并且在非氧化环境中加热混合物，同时防止硫蒸气流出。还提供了使用以该方法制造的硫改性聚丙烯腈作为活性物质的锂电池阴极和包含阴极作为组分元素的锂二次电池。这使得可以实际使用廉价的硫基材料作为锂二次电池的阴极材料，特别是能够实现更高产量并且具有优异的循环寿命特性以及其它特性的硫基阴极材料，以及二次可以获得使用其的锂电池。

14. 发明申请

US20110200875A1 SULFUR-MODIFIED POLYACRYLONITRILE, MANUFACTURING METHOD THEREFOR, AND APPLICATION THEREOF 有权
标题翻译：硫改性聚丙烯腈，其制造方法及其应用
公开(公告)号：US20110200875A1
公开(公告)日：2011-08-18
申请号：US13123933
申请日：2009-10-15
申请人： Takuhiro Miyuki , Tetsuo Sakai , Junichi Niwa , Hitotoshi Murase
发明人： Takuhiro Miyuki , Tetsuo Sakai , Junichi Niwa , Hitotoshi Murase
IPC分类号： H01M4/60 , C08F20/44
CPC分类号： C08F20/44 , C01B32/20 , C08F8/34 , H01M4/0404 , H01M4/1399 , H01M4/60 , H01M4/604 , H01M4/661 , H01M4/663 , H01M6/5088 , H01M10/052 , Y02T10/7011 , C08F120/44
摘要： Provided is a sulfur-modified polyacrylonitrile manufacturing method that is characterized in that a starting base powder that comprises sulfur powder and polyacrylonitrile powder is mixed and the mixture is heated in a non-oxidizing environment while outflow of sulfur vapor is prevented. Also provided are a cathode for lithium batteries that uses, as the active substance, the sulfur-modified polyacrylonitrile manufactured with the method, and a lithium secondary battery that includes the cathode as a component element. This enables the practical use of an inexpensive sulfur-based material as the cathode material for lithium secondary batteries, and in particular, a sulfur-based cathode material that enables higher output and has excellent cycle life characteristics, as well as other characteristics, and secondary lithium batteries using the same can be obtained.
摘要翻译：提供一种硫改性聚丙烯腈制造方法，其特征在于，将包含硫粉末和聚丙烯腈粉末的起始基础粉末混合，并且在非氧化环境中加热混合物，同时防止硫蒸气流出。还提供了使用以该方法制造的硫改性聚丙烯腈作为活性物质的锂电池阴极和包含阴极作为组分元素的锂二次电池。这使得可以实际使用廉价的硫基材料作为锂二次电池的阴极材料，特别是能够实现更高产量并且具有优异的循环寿命特性以及其它特性的硫基阴极材料，以及二次可以获得使用其的锂电池。

15. 发明授权

US08927157B2 Condensed polycyclic aromatic compound, production process of same, and positive electrode active material for lithium ion secondary battery containing same 有权
标题翻译：缩合多环芳香族化合物，其制造方法以及含有该锂离子二次电池的正极活性物质
公开(公告)号：US08927157B2
公开(公告)日：2015-01-06
申请号：US13701544
申请日：2011-05-26
申请人： Osamu Ohmori , Akiko Shima , Hitotoshi Murase , Masataka Nakanishi , Junichi Niwa , Kimihisa Yamamoto
发明人： Osamu Ohmori , Akiko Shima , Hitotoshi Murase , Masataka Nakanishi , Junichi Niwa , Kimihisa Yamamoto
IPC分类号： H01M4/60 , C07C251/22 , C07C249/02 , H01M10/052 , C07B61/00 , H01M4/02
CPC分类号： H01M4/606 , C07C251/22 , H01M4/60 , H01M4/608 , H01M10/052 , H01M2004/028 , Y02E60/122 , Y02P70/54
摘要： Provided is a condensed polycyclic aromatic compound, having lithium ion responsivity and is suitable for lithium ion secondary battery applications, a production process thereof, a positive electrode active material containing that condensed polycyclic aromatic compound, and a positive electrode for a lithium ion secondary battery provided therewith, and further provided is a lithium ion secondary battery, having high capacity and cycling adaptability, that has the positive electrode as a constituent thereof. The condensed polycyclic aromatic compound has at least four imino groups in a molecule thereof.
摘要翻译：提供了具有锂离子响应性并适用于锂离子二次电池应用的缩合多环芳香族化合物，其制造方法，含有缩合多环芳香族化合物的正极活性物质和提供的锂离子二次电池用正极并且还提供具有高容量和循环适应性的锂离子二次电池，其具有正极作为其组成。缩合多环芳族化合物在其分子中具有至少四个亚氨基。

16. 发明申请

US20130078514A1 CONDENSED POLYCYCLIC AROMATIC COMPOUND, PRODUCTION PROCESS OF SAME, AND POSITIVE ELECTRODE ACTIVE MATERIAL FOR LITHIUM ION SECONDARY BATTERY CONTAINING SAME 有权
标题翻译：稠合多环芳香族化合物，其生产方法和用于含有其的锂离子二次电池的正极电极活性材料
公开(公告)号：US20130078514A1
公开(公告)日：2013-03-28
申请号：US13701544
申请日：2011-05-26
申请人： Osamu Ohmori , Akiko Shima , Hitotoshi Murase , Masataka Nakanishi , Junichi Niwa , Kimihisa Yamamoto
发明人： Osamu Ohmori , Akiko Shima , Hitotoshi Murase , Masataka Nakanishi , Junichi Niwa , Kimihisa Yamamoto
IPC分类号： H01M4/60
CPC分类号： H01M4/606 , C07C251/22 , H01M4/60 , H01M4/608 , H01M10/052 , H01M2004/028 , Y02E60/122 , Y02P70/54
摘要： Provided is a condensed polycyclic aromatic compound, having superior lithium ion responsivity and is suitable for lithium ion secondary battery applications, a production process thereof, a positive electrode active material containing that condensed polycyclic aromatic compound, and a positive electrode for a lithium ion secondary battery provided therewith, and further provided is a lithium ion secondary battery, having high capacity and superior cycling adaptability, that has the positive electrode as a constituent thereof.The condensed polycyclic aromatic compound according to the present invention has at least four imino groups in a molecule thereof.
摘要翻译：提供了具有优异的锂离子响应性并且适合于锂离子二次电池应用的缩合多环芳香族化合物，其制造方法，含有缩合多环芳香族化合物的正极活性物质和锂离子二次电池用正极并且还提供具有高容量和优异的循环适应性的锂离子二次电池，其具有正极作为其组成。根据本发明的缩合多环芳族化合物在其分子中具有至少四个亚氨基。

17. 发明申请

US20110031935A1 NEGATIVE ELECTRODE FOR LITHIUM-ION SECONDARY BATTERY AND MANUFACTURING PROCESS FOR THE SAME 审中-公开
标题翻译：用于锂离子二次电池的负极及其制造方法
公开(公告)号：US20110031935A1
公开(公告)日：2011-02-10
申请号：US12988491
申请日：2009-03-17
申请人： Manabu Miyoshi , Hitotoshi Murase , Akira Kojima , Junichi Niwa , Takayuki Hirose , Kazuhiro Izumoto , Hideki Goda
发明人： Manabu Miyoshi , Hitotoshi Murase , Akira Kojima , Junichi Niwa , Takayuki Hirose , Kazuhiro Izumoto , Hideki Goda
IPC分类号： H01M10/44 , H01M4/58 , H01M2/14 , H01M4/62
CPC分类号： H01M4/622 , H01M4/134 , H01M4/136 , H01M4/1395 , H01M4/38 , H01M4/386 , H01M4/387 , H01M4/5825 , H01M4/621 , H01M4/661 , H01M4/74 , H01M10/052 , H01M10/44
摘要： The present invention is characterized in that, in a negative electrode for lithium-ion secondary battery, the negative electrode being manufactured via an application step of applying a binder resin and an active material onto a surface of collector, the binder resin is an alkoxysilyl group-containing resin that has a structure being specified by formula (I); and the active material includes a lithium-inactive metal that does not form any intermetallic compounds with lithium, or a silicide of the lithium-inactive metal, and an elemental substance of Si. It is possible to upgrade cyclic characteristics by means of using the negative electrode for lithium-ion secondary battery according to the present invention. wherein “R1” is an alkyl group whose number of carbon atoms is from 1 to 8; “R2” is an alkyl group or alkoxyl group whose number of carbon atoms is from 1 to 8; and “q” is an integer of from 1 to 100.
摘要翻译：本发明的特征在于，在锂离子二次电池用负极中，通过将粘合剂树脂和活性物质涂布在集电体的表面上的施加步骤制造负极，粘合剂树脂为烷氧基甲硅烷基（I）所示结构的树脂; 并且活性材料包括不与锂形成任何金属间化合物的锂惰性金属，或锂惰性金属的硅化物和Si的元素物质。通过使用本发明的锂离子二次电池用负极，能够提高循环特性。其中“R1”是碳原子数为1〜8的烷基; “R2”是碳原子数为1〜8的烷基或烷氧基; “q”为1〜100的整数。

18. 发明申请

US20140186704A1 LITHIUM ION SECONDARY BATTERY ELECTRODE, MANUFACTURING PROCESS FOR THE SAME, AND LITHIUM ION SECONDARY BATTERY USING THE ELECTRODE 有权
标题翻译：锂离子二次电池电极，其制造方法和使用电极的锂离子二次电池
公开(公告)号：US20140186704A1
公开(公告)日：2014-07-03
申请号：US14119239
申请日：2012-05-02
申请人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
发明人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
IPC分类号： H01M4/62 , H01M4/04 , H01M4/139
CPC分类号： H01M4/139 , H01M4/0404 , H01M4/0471 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/1391 , H01M4/1397 , H01M4/366 , H01M4/38 , H01M4/485 , H01M4/505 , H01M4/62 , H01M4/622 , H01M10/0525 , Y02E60/122 , Y02P70/54
摘要： To provide a lithium ion secondary battery electrode in which a coated layer is held on a surface of an active material layer over a long period of time to suppress decomposition of the electrolysis solution and to enhance the cyclability, a manufacturing process for the same, and a lithium ion secondary battery using the electrode.A lithium ion secondary battery electrode includes a current collector, an active material layer containing a binder formed on a surface of the current collector, and a coated layer formed on the surface of at least a part of the active material layer, wherein the coated layer consists of an acrylic type copolymer cured substance comprising an acrylic type main chain and a side chain having polyester or polyether graft-polymerized to said acrylic type main chain and the coated layer is chemically bonded with the binder.
摘要翻译：为了提供一种锂离子二次电池电极，其中将涂层长时间地保持在活性物质层的表面上，以抑制电解液的分解并提高其循环性，其制造方法和使用该电极的锂离子二次电池。锂离子二次电池电极包括集电体，含有形成在集电体的表面上的粘合剂的活性物质层和形成在活性物质层的至少一部分的表面上的被覆层，其中，涂布层由丙烯酸型主链和丙烯酸类主链接枝聚合的聚酯或聚醚的侧链构成的丙烯酸类共聚物固化物，涂层与粘合剂化学键合。

19. 发明授权

US09306220B2 Lithium ion secondary battery electrode, manufacturing process for the same, and lithium ion secondary battery using the electrode 有权
标题翻译：锂离子二次电池电极，制造工艺相同，锂离子二次电池使用电极
公开(公告)号：US09306220B2
公开(公告)日：2016-04-05
申请号：US14119235
申请日：2012-05-02
申请人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
发明人： Junichi Niwa , Yuichi Hirakawa , Manabu Miyoshi , Keiichi Hayashi , Hitotoshi Murase
IPC分类号： H01M4/62 , H01M4/04 , H01M4/13 , H01M4/139 , H01M10/42
CPC分类号： H01M4/628 , H01M4/0404 , H01M4/13 , H01M4/139 , H01M4/622 , H01M10/4235 , Y02E60/122 , Y02P70/54
摘要： To provide a lithium ion secondary battery electrode in which a coated layer is held on a surface of an active material layer over a long period of time to suppress decomposition of the electrolysis solution and to enhance the cyclability, a manufacturing process for the same, and a lithium ion secondary battery using the electrode.A lithium ion secondary battery electrode includes a current collector, an active material layer containing a binder formed on a surface of the current collector, and a coated layer formed on the surface of at least a part of the active material layer, wherein the coated layer contains a silicone-acrylic graft copolymer cured substance including an acrylic type main chain having a functional group and a side chain having a silicone graft-polymerized to the acrylic type main chain, and the coated layer is chemically bonded with the binder.
摘要翻译：为了提供一种锂离子二次电池电极，其中将涂层长时间地保持在活性物质层的表面上，以抑制电解液的分解并提高其循环性，其制造方法和使用该电极的锂离子二次电池。锂离子二次电池电极包括集电体，含有形成在集电体的表面上的粘合剂的活性物质层和形成在活性物质层的至少一部分的表面上的涂层，其中，涂布层含有具有官能团的丙烯酸类主链和具有与丙烯酸类主链接枝聚合的硅氧烷的侧链的有机硅 - 丙烯酸接枝共聚物固化物，并且涂层与粘合剂化学键合。

20. 发明申请

US20120321955A1 LITHIUM-ION SECONDARY BATTERY 审中-公开
标题翻译：锂离子二次电池
公开(公告)号：US20120321955A1
公开(公告)日：2012-12-20
申请号：US13581355
申请日：2011-04-01
申请人： Naoto Yasuda , Toru Abe , Junichi Niwa
发明人： Naoto Yasuda , Toru Abe , Junichi Niwa
IPC分类号： H01M4/505 , H01M4/485 , H01M4/52 , H01M4/54
CPC分类号： H01M4/505 , H01M4/131 , H01M4/386 , H01M4/387 , H01M4/525 , H01M4/587 , H01M10/052 , Y02T10/7011
摘要： A lithium-ion secondary battery is characterized in that it is equipped with: a positive electrode comprising a positive-electrode active material that includes a lithium-transition metal composite oxide including at least lithium and manganese and possessing a layered rock-salt structure; a negative electrode comprising a negative-electrode active material that includes at least one kind of carbon-based materials, silicon-based materials, and tin-based materials; and a non-aqueous electrolytic solution, wherein: said lithium-transition metal composite oxide exhibits an irreversible capacity; and an actual capacity of said negative electrode at the time of first-round charging up to 0 V with respect to metallic lithium is smaller than an actual capacity of said positive electrode at the time of first-round charging up to 4.7 V with respect to metallic lithium. Even when an employment amount of the active materials is reduced less than those conventional amounts, the resulting battery capacity hardly declines.
摘要翻译：锂离子二次电池的特征在于，其具备：包含正极活性物质的正极，所述正极活性物质包括至少包含锂和锰的锂 - 过渡金属复合氧化物，并具有层状岩盐结构; 包含负极活性物质的负极，所述负极活性物质包含至少一种碳类材料，硅类材料和锡类材料; 和非水电解液，其中：所述锂 - 过渡金属复合氧化物具有不可逆容量; 并且相对于金属锂在第一次充电至0V时的所述负极的实际容量小于相对于第一次充电高达4.7V时的所述正极的实际容量金属锂。即使活性物质的使用量比常规量减少，所得电池容量几乎不下降。

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