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11. 发明授权

US6077930A Preparation process of polymer 失效
标题翻译：聚合物的制备工艺
公开(公告)号：US6077930A
公开(公告)日：2000-06-20
申请号：US79230
申请日：1998-05-15
申请人： Tadahito Nobori , Shinji Kiyono , Takaomi Hayashi , Usaji Takaki
发明人： Tadahito Nobori , Shinji Kiyono , Takaomi Hayashi , Usaji Takaki
IPC分类号： C08G63/82 , C08G65/26 , C08G69/20 , C08G77/08 , C08G63/08
CPC分类号： C08G69/20 , C08G63/823 , C08G65/2675 , C08G77/08
摘要： A preparation process of a polymer comprising conducting ring-opening polymerization of a 4- to 10-membered ring-opening polymerizable cyclic monomer in the presence of a phosphazenium salt of an active hydrogen compound represented by the chemical formula (1): ##STR1## wherein n is an integer of 1 to 8 and indicates the number of phosphazenium cations, Z.sup.n- is an anion of a n-valent active hydrogen compound derived by releasing n protons from an active hydrogen compound having a maximum of 8 active hydrogen atoms, a, b, c and d are individually a positive integer or 0 and are not all 0 at the same time, R's are the same or different hydrocarbons having 1 to 10 carbon atoms, and two R's located on each common nitrogen atom may be coupled together to form a ring structure; or in the presence of the phosphazenium salt of the active hydrogen compound and the active hydrogen compound is disclosed. The process can prepare polymer by ring-opening polymerization of a 4- to 10-membered ring-opening polymerizable cyclic monomer in the presence of an initiator which causes no specific problem or preparation and handling, contains quite no installic ingredient and has no residual odor.
摘要翻译：一种聚合物的制备方法，包括在由化学式（1）表示的活性氢化合物的磷氮烯基鏻盐的存在下进行4-至10-元可开环聚合的环状单体的开环聚合：其中n为 1〜8的整数，表示磷氮烯基鏻阳离子的数量，Zn-是通过从具有最多8个活性氢原子的活性氢化合物释放n个质子得到的n价活性氢化合物的阴离子，a，b， c和d分别为正整数或0并且同时不全部为0，R为相同或不同的碳原子数为1〜10的烃，并且位于每个常见氮原子上的两个R可以连接在一起形成环结构; 或在活性氢化合物的磷腈鎓盐和活性氢化合物的存在下进行。该方法可以通过在不引起特定问题或制备和处理的引发剂的存在下开环聚合4-至10-元可开环聚合的环状单体来制备聚合物，其中不含安装成分并且没有残留气味。

12. 发明申请

US20110288240A1 NOVEL PHOSPHAZENE-SUPPORTED CATALYST, NOVEL COMPOUND THEREOF AND USE THEREOF 审中-公开
标题翻译：新型磷酸盐载体催化剂，其新颖化合物及其用途
公开(公告)号：US20110288240A1
公开(公告)日：2011-11-24
申请号：US13198397
申请日：2011-08-04
申请人： Naritoshi YOSHIMURA , Shinji Kiyono , Kazumi Mizutani , Isao Hara , Takaomi Hayashi , Tadahito Nobori , Yoshihiro Yamamoto , Miyuki Konno , Yoshihisa Inoue , Akira Matsuura , Tuneyuki Ohkubo
发明人： Naritoshi YOSHIMURA , Shinji Kiyono , Kazumi Mizutani , Isao Hara , Takaomi Hayashi , Tadahito Nobori , Yoshihiro Yamamoto , Miyuki Konno , Yoshihisa Inoue , Akira Matsuura , Tuneyuki Ohkubo
IPC分类号： C08F8/40 , C07C45/45 , C07C41/16 , C07C41/02 , C07F9/06 , C07F9/22
CPC分类号： C08G63/823 , B01J31/0265 , B01J2231/12 , C07F9/065 , C07F9/224
摘要： A phosphazene-supported catalyst in which a support is bonded to a group represented by the general formula (1): wherein n, Zn−, a, b, c, d, R, R1 and D are all defined. The phosphazene-supported catalyst is highly effective to catalyze various organic reactions, and further has no reduction of activity even after recovery and reuse of the catalyst, thus it being economically advantageous. In addition, the polymerization of cyclic monomers, substitution of substituents, carbon-carbon bond forming reactions and the like can be conducted with extremely high efficiency.
摘要翻译：载体与由通式（1）表示的基团键合的磷腈担载催化剂：其中n，Zn-，a，b，c，d，R，R1和D全部定义。磷腈担载的催化剂对于催化各种有机反应是非常有效的，即使在回收和再利用催化剂之后也不会降低活性，因此在经济上是有利的。此外，可以极高效率进行环状单体的聚合，取代基的取代，碳 - 碳键形成反应等。

13. 发明申请

US20080318767A1 Novel Phosphazene-Supported Catalyst, Novel Compound Thereof and Use Thereof 审中-公开
标题翻译：新型磷腈载体催化剂，新型化合物及其用途
公开(公告)号：US20080318767A1
公开(公告)日：2008-12-25
申请号：US11631286
申请日：2005-06-28
申请人： Naritoshi Yoshimura , Shinji Kiyono , Kazumi Mizutani , Isao Hara , Takaomi Hayashi , Tadahito Nobori , Yoshihiro Yamamoto , Miyuki Konno , Yoshihisa Inoue , Akira Matsuura , Tuneyuki Ohkubo
发明人： Naritoshi Yoshimura , Shinji Kiyono , Kazumi Mizutani , Isao Hara , Takaomi Hayashi , Tadahito Nobori , Yoshihiro Yamamoto , Miyuki Konno , Yoshihisa Inoue , Akira Matsuura , Tuneyuki Ohkubo
IPC分类号： C07F9/06 , B01J31/02
CPC分类号： C08G63/823 , B01J31/0265 , B01J2231/12 , C07F9/065 , C07F9/224
摘要： A phosphazene-supported catalyst in which a support is bonded to a group represented by the general formula (1): wherein n, Zn−, a, b, c, d, R, R1 and D are all defined. The phosphazene-supported catalyst is highly effective to catalyze various organic reactions, and further has no reduction of activity even after recovery and reuse of the catalyst, thus it being economically advantageous. In addition, the polymerization of cyclic monomers, substitution of substituents, carbon-carbon bond forming reactions and the like can be conducted with extremely high efficiency.
摘要翻译：载体与由通式（1）表示的基团键合的磷腈担载催化剂：其中n，Zn-，a，b，c，d，R，R1和D全部定义。磷腈担载的催化剂对于催化各种有机反应是非常有效的，即使在回收和再利用催化剂之后也不会降低活性，因此在经济上是有利的。此外，可以极高效率进行环状单体的聚合，取代基的取代，碳 - 碳键形成反应等。

14. 发明申请

US20080033154A1 Process for Producing 3-Aminomethyltetrahydrofuran Derivative 审中-公开
标题翻译：生产3-氨基甲基四氢呋喃衍生物的方法
公开(公告)号：US20080033154A1
公开(公告)日：2008-02-07
申请号：US11629517
申请日：2005-06-02
申请人： Yoshihisa Inoue , Setsuko Funaki , Tetsuya Hamada , Yoshihiro Yamamoto , Isao Hara , Takaomi Hayashi , Miyuki Konno , Shinobu Aoki
发明人： Yoshihisa Inoue , Setsuko Funaki , Tetsuya Hamada , Yoshihiro Yamamoto , Isao Hara , Takaomi Hayashi , Miyuki Konno , Shinobu Aoki
IPC分类号： C07D307/02 , C07H5/06
CPC分类号： C07D307/14
摘要： A 3-aminomethyltetrahydrofuran derivative is produced by preparing a 3-cyanotetrahydrofuran derivative in a high yield from a malic acid derivative, and reducing the cyano group of the 3-cyanotetrahydrofuran derivative. The process can produce the 3-cyanotetrahydrofuran derivative in a high yield from inexpensive industrial materials.
摘要翻译：通过从苹果酸衍生物制备高收率的3-氰基四氢呋喃衍生物，并还原3-氰基四氢呋喃衍生物的氰基，制备3-氨基甲基四氢呋喃衍生物。该方法可以从廉价的工业材料以高产率生产3-氰基四氢呋喃衍生物。

15. 发明申请

US20110034735A1 METHOD FOR PRODUCING CATECHOL 有权
标题翻译：生产CATECHOL的方法
公开(公告)号：US20110034735A1
公开(公告)日：2011-02-10
申请号：US12936269
申请日：2009-04-07
申请人： Tsuneji Suzuki , Takaomi Hayashi , Hideo Kitagawa , Naritoshi Yoshimura
发明人： Tsuneji Suzuki , Takaomi Hayashi , Hideo Kitagawa , Naritoshi Yoshimura
IPC分类号： C07C45/00 , C07C33/30
CPC分类号： C07B53/00 , C07C37/07 , C07C45/62 , C07C45/66 , C07C51/00 , C07C2601/14 , C07C2601/16 , C07C39/08 , C07C49/497 , C07C49/713
摘要： Provided is a method for producing catechol in a one-pot by reacting (4S,5R,6S)-4,5,6-trihydroxy-2-cyclohexene-1-one under hydrogen-reducing conditions while heating.
摘要翻译：本发明提供通过在加氢条件下在氢还原条件下使（4S，5R，6S）-4,5,6-三羟基-2-环己烯-1-酮反应而在一锅中生产儿茶酚的方法。

16. 发明授权

US08604253B2 Method for producing polyhydric phenol 有权
标题翻译：多元酚的制造方法
公开(公告)号：US08604253B2
公开(公告)日：2013-12-10
申请号：US13266393
申请日：2010-04-27
申请人： Hideo Kitagawa , Junya Kiyosu , Susumu Saito , Takaomi Hayashi , Naritoshi Yoshimura , Aya Nakagawa
发明人： Hideo Kitagawa , Junya Kiyosu , Susumu Saito , Takaomi Hayashi , Naritoshi Yoshimura , Aya Nakagawa
IPC分类号： C07C37/07
CPC分类号： C07C37/07 , C07B2200/07 , C07C45/513 , C07C45/66 , C07C2601/16 , Y02P20/52 , C07C39/10 , C07C39/08 , C07C49/713
摘要： The present invention is a method for producing a polyhydric phenol, including the following steps (a) to (d): (a) a first step of producing (4S,5R,6S)-4,5,6-trihydroxy-2-cyclohexcene-1-one from 2-deoxy-scyllo-inosose by a dehydration reaction; (b) a second step of producing 1,2,4-trihydroxybenzene from the (4S,5R,6S)-4,5,6-trihydroxy-2-cyclohexene-1-one obtained in the first step by a dehydration reaction; (c) a third step of producing 4-hydroxycyclohexane-1,3-dione from the 1,2,4-trihydroxybenzene by a catalytic hydrogenation reaction with the use of a metal catalyst; and (d) a fourth step of producing hydroquinone by heating the 4-hydroxycyclohexane-1,3-dione.
摘要翻译：本发明是一种生产多元酚的方法，包括以下步骤（a）至（d）：（a）制备（4S，5R，6S）-4,5,6-三羟基-2- 环己烯-1-酮通过脱水反应从2-脱氧 - 十字糖 - （b）通过脱水反应从第一步获得的（4S，5R，6S）-4,5,6-三羟基-2-环己烯-1-酮生成1,2,4-三羟基苯的第二步骤; （c）通过使用金属催化剂的催化氢化反应从1,2,4-三羟基苯生产4-羟基环己烷-1,3-二酮的第三步骤; 和（d）通过加热4-羟基环己烷-1,3-二酮制备氢醌的第四步骤。

17. 发明授权

US08378146B2 Method for producing catechol 有权
标题翻译：邻苯二酚生产方法
公开(公告)号：US08378146B2
公开(公告)日：2013-02-19
申请号：US12936269
申请日：2009-04-07
申请人： Tsuneji Suzuki , Takaomi Hayashi , Hideo Kitagawa , Naritoshi Yoshimura
发明人： Tsuneji Suzuki , Takaomi Hayashi , Hideo Kitagawa , Naritoshi Yoshimura
IPC分类号： C07C45/00 , C07C33/30
CPC分类号： C07B53/00 , C07C37/07 , C07C45/62 , C07C45/66 , C07C51/00 , C07C2601/14 , C07C2601/16 , C07C39/08 , C07C49/497 , C07C49/713
摘要： Provided is a method for producing catechol in a one-pot by reacting (4S,5R,6S)-4,5,6-trihydroxy-2-cyclohexene-1-one under hydrogen-reducing conditions while heating.
摘要翻译：本发明提供通过在加氢条件下在氢还原条件下使（4S，5R，6S）-4,5,6-三羟基-2-环己烯-1-酮反应而在一锅中生产儿茶酚的方法。

18. 发明申请

US20120046498A1 METHOD FOR PRODUCING POLYHYDRIC PHENOL 有权
标题翻译：生产聚苯酚的方法
公开(公告)号：US20120046498A1
公开(公告)日：2012-02-23
申请号：US13266393
申请日：2010-04-27
申请人： Hideo Kitagawa , Junya Kiyosu , Susumu Saito , Takaomi Hayashi , Naritoshi Yoshimura , Aya Nakagawa
发明人： Hideo Kitagawa , Junya Kiyosu , Susumu Saito , Takaomi Hayashi , Naritoshi Yoshimura , Aya Nakagawa
IPC分类号： C07C37/07
CPC分类号： C07C37/07 , C07B2200/07 , C07C45/513 , C07C45/66 , C07C2601/16 , Y02P20/52 , C07C39/10 , C07C39/08 , C07C49/713
摘要： The present invention is a method for producing a polyhydric phenol, including the following steps (a) to (d): (a) a first step of producing (4S,5R,6S)-4,5,6-trihydroxy-2-cyclohexcene-1-one from 2-deoxy-scyllo-inosose by a dehydration reaction; (b) a second step of producing 1,2,4-trihydroxybenzene from the (4S,5R,6S)-4,5,6-trihydroxy-2-cyclohexene-1-one obtained in the first step by a dehydration reaction; (c) a third step of producing 4-hydroxycyclohexane-1,3-dione from the 1,2,4-trihydroxybenzene by a catalytic hydrogenation reaction with the use of a metal catalyst; and (d) a fourth step of producing hydroquinone by heating the 4-hydroxycyclohexane-1,3-dione.
摘要翻译：本发明是一种生产多元酚的方法，包括以下步骤（a）至（d）：（a）制备（4S，5R，6S）-4,5,6-三羟基-2- 环己烯-1-酮通过脱水反应从2-脱氧 - 十字糖 - （b）通过脱水反应从第一步获得的（4S，5R，6S）-4,5,6-三羟基-2-环己烯-1-酮生成1,2,4-三羟基苯的第二步骤; （c）通过使用金属催化剂的催化氢化反应从1,2,4-三羟基苯生产4-羟基环己烷-1,3-二酮的第三步骤; 和（d）通过加热4-羟基环己烷-1,3-二酮制备氢醌的第四步骤。

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