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11. 发明申请

US20080141905A1 Method for the Surface Treatment of Solid Particles, Particularly Titanium Dioxide Pigment Particles 审中-公开
标题翻译：固体颗粒，特别是二氧化钛颜料颗粒的表面处理方法
公开(公告)号：US20080141905A1
公开(公告)日：2008-06-19
申请号：US11941156
申请日：2007-11-16
申请人： Volker Juergens , Juergen Orth-Gerber , Lydia Drews-Nicolai
发明人： Volker Juergens , Juergen Orth-Gerber , Lydia Drews-Nicolai
IPC分类号： B05D7/24 , B05D7/14 , C04B14/34
CPC分类号： C09C1/3661 , B82Y30/00 , C01P2004/04 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C09C3/063
摘要： A method for manufacturing inorganic solid particles, particularly titanium dioxide pigment particles, with a smooth and homogeneous surface coating in an aqueous suspension.
摘要翻译：一种在水性悬浮液中制备具有光滑均匀的表面涂层的无机固体颗粒，特别是二氧化钛颜料颗粒的方法。

12. 发明授权

US07135065B2 Method for the post-treatment of titanium dioxide pigments 失效
标题翻译：二氧化钛颜料后处理方法
公开(公告)号：US07135065B2
公开(公告)日：2006-11-14
申请号：US11179985
申请日：2005-07-12
申请人： Lydia Drews-Nicolai , Siegfried Bluemel
发明人： Lydia Drews-Nicolai , Siegfried Bluemel
IPC分类号： C09C1/36 , C01G23/047 , C01G23/08
CPC分类号： C09C1/3661 , C01P2002/30 , C01P2004/84 , C01P2006/64 , C08K3/22 , C08K9/02 , C09D7/62
摘要： The invention relates to a method for the post-treatment of titanium dioxide, in order to produce particularly weather-resistant titanium dioxide pigments with good optical properties. The method is characterized in that, together with the hydrous oxides of tin and zirconium, at least one other from the group comprising aluminium, silicon and titanium is additionally precipitated onto the particle surface. The post-treatment components are added to the aqueous TiO2 suspension either in the acidic range (pH value of 3 at most) or in the alkaline range (pH value of 10 at least). The pH value is subsequently set to between 6 and 8. Final tempering of the pigment at elevated temperatures from over 125° C. to up to 500° C. can improve the tone b. The pigment is particularly suitable for use in paints, coatings and plastics.
摘要翻译：本发明涉及一种后处理二氧化钛的方法，以便制备具有良好光学性能的特别耐候的二氧化钛颜料。该方法的特征在于，与锡和锆的水合氧化物一起，还包括从铝，硅和钛组成的组中的至少一种另外沉淀到颗粒表面上。将后处理组分在酸性范围（pH值为3以下）或碱性范围（至少为pH值为10）中添加到TiO 2水溶液中。 pH值随后设定在6和8之间。颜料在高于125℃至高达500℃的高温下进行最终回火可改善色调b。该颜料特别适用于油漆，涂料和塑料。

13. 发明授权

US07905953B2 Titanium dioxide pigment particles with doped, dense SiO2 skin and methods for their manufacture 有权
标题翻译：具有掺杂，致密SiO 2皮肤的二氧化钛颜料颗粒及其制造方法
公开(公告)号：US07905953B2
公开(公告)日：2011-03-15
申请号：US11668729
申请日：2007-01-30
申请人： Siegfried Bluemel , Lydia Drews-Nicolai
发明人： Siegfried Bluemel , Lydia Drews-Nicolai
IPC分类号： C09C1/36 , B32B5/16 , B32B9/00 , B32B15/02 , B32B17/02 , B32B19/00 , B32B21/02 , B32B23/02 , B32B27/02 , D06N7/04 , E01F9/04 , E04D7/00
CPC分类号： C09C1/3661 , C01G23/07 , C01P2002/52 , C01P2002/84 , C01P2004/84 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/2991 , Y10T428/2993
摘要： A method of predicting photostability of coatings with various dopants on titanium dioxide pigment particles is disclosed. Calculations of the density of states show that a doped coating which reduces the density of states near the band edge or increases the density of states within the band gap of the pigment particles increases the photostability of the doped pigment.
摘要翻译：公开了一种用二氧化钛颜料颗粒预测各种掺杂剂涂层的光稳定性的方法。状态密度的计算表明，降低带边缘附近状态密度或增加颜料颗粒带隙内状态密度的掺杂涂层增加了掺杂颜料的光稳定性。

14. 发明授权

US07682441B2 Weather resistant titanium dioxide pigment and a process for its production 有权
标题翻译：耐候二氧化钛颜料及其生产工艺
公开(公告)号：US07682441B2
公开(公告)日：2010-03-23
申请号：US11158761
申请日：2005-06-21
申请人： Lydia Drews-Nicolai , Siegfried Bluemel
发明人： Lydia Drews-Nicolai , Siegfried Bluemel
IPC分类号： C09C1/36 , C04B14/00
CPC分类号： C09C1/3661 , C01P2002/52 , C01P2004/84 , C01P2006/12 , C08K3/22 , C08K9/02 , C09D7/62
摘要： The invention relates to a weather resistant titanium dioxide pigment with good optical properties having a SiO2 dense skin doped with metal atoms. Particularly suitable elements for doping are tin, zirconium and titanium. The SiO2 dense skin is composed of multiple layers whereby the innermost layer does not contain any significant quantity of metal atoms. The coating according to the invention is produced by adding the components to the alkaline suspension (pH at least 9) one after the other with a sliding pH. Complete formation of the doped SiO2 dense skin requires that the pH subsequently be lowered to below 9. The pigment is particularly suitable for use in surface coatings and plastics.
摘要翻译：本发明涉及具有良好光学性质的耐候二氧化钛颜料，其具有掺杂有金属原子的SiO 2致密表皮。特别合适的掺杂元素是锡，锆和钛。 SiO2致密皮由多层组成，最内层不含任何显着量的金属原子。根据本发明的涂层通过以滑动pH将这些组分一个接一个地添加到碱性悬浮液（pH至少为9）中来制备。完全形成掺杂的SiO 2致密的皮肤需要随后将pH降低至低于9.颜料特别适用于表面涂料和塑料。

15. 发明申请

US20090297852A1 Method for Coating the Surface of Inorganic Solid Particles, Especially Titanium Dioxide Pigment Particles 有权
标题翻译：无机固体颗粒，特别是二氧化钛颜料颗粒的表面涂覆方法
公开(公告)号：US20090297852A1
公开(公告)日：2009-12-03
申请号：US12472498
申请日：2009-05-27
申请人： Heiko Frahm , Joerg Friedrich , Mark Kaminski , Erwin Schmeier , Lydia Drews-Nicolai , Volker Juergens
发明人： Heiko Frahm , Joerg Friedrich , Mark Kaminski , Erwin Schmeier , Lydia Drews-Nicolai , Volker Juergens
IPC分类号： B32B1/00 , C09B67/08 , B05D7/00
CPC分类号： C09C1/3684 , C01P2004/04 , C01P2006/60 , Y10T428/2991
摘要： A method for coating the surface of inorganic solid particles in an aqueous suspension, particularly for coating titanium dioxide with SiO2 includes: a) disagglomeration of the solid particles contained in aqueous suspension, b) addition of a water-soluble precursor of the coating substance to the suspension, c) immediately following step b) homogenization of the suspension, where the temperature and pH value of the suspension do not change significantly in steps a) to c), d) feeding the slurry into a tank and precipitation of the coating substance onto the particle surface and, optionally, application of further coatings, and e) separation of the solid particles from the suspension. The method produces to a highly homogeneous and continuous skin on the particle surface, and to less separately precipitated coating substance.
摘要翻译：在水性悬浮液中涂覆无机固体颗粒表面的方法，特别是用SiO 2涂覆二氧化钛的方法包括：a）包含在水性悬浮液中的固体颗粒的解聚，b）将涂覆物质的水溶性前体加入悬浮液，c）在步骤b）之后立即进行均化，其中悬浮液的温度和pH值在步骤a）至c）中不显着变化，d）将浆料进料到罐中并沉淀涂料到颗粒表面上，并且任选地施加另外的涂层，以及e）从悬浮液中分离出固体颗粒。该方法在颗粒表面上产生高度均匀和连续的皮肤，并产生较少的分离沉淀的涂层物质。

16. 发明申请

US20060032402A1 Weather resistant titanium dioxide pigment and a process for its production 有权
标题翻译：耐候二氧化钛颜料及其生产工艺
公开(公告)号：US20060032402A1
公开(公告)日：2006-02-16
申请号：US11158761
申请日：2005-06-21
申请人： Lydia Drews-Nicolai , Siegfried Bluemel
发明人： Lydia Drews-Nicolai , Siegfried Bluemel
IPC分类号： C04B14/00 , C09C1/36
CPC分类号： C09C1/3661 , C01P2002/52 , C01P2004/84 , C01P2006/12 , C08K3/22 , C08K9/02 , C09D7/62
摘要： The invention relates to a weather resistant titanium dioxide pigment with good optical properties having a SiO2 dense skin doped with metal atoms. Particularly suitable elements for doping are tin, zirconium and titanium. The SiO2 dense skin is composed of multiple layers whereby the innermost layer does not contain any significant quantity of metal atoms. The coating according to the invention is produced by adding the components to the alkaline suspension (pH at least 9) one after the other with a sliding pH. Complete formation of the doped SiO2 dense skin requires that the pH subsequently be lowered to below 9. The pigment is particularly suitable for use in surface coatings and plastics.
摘要翻译：本发明涉及具有良好光学性质的耐候二氧化钛颜料，其具有掺杂有金属原子的SiO 2 2致密表皮。特别合适的掺杂元素是锡，锆和钛。 SiO 2 2致密皮由多层组成，最内层不含任何显着量的金属原子。根据本发明的涂层通过以滑动pH将这些组分一个接一个地添加到碱性悬浮液（pH至少为9）中来制备。完全形成掺杂的SiO 2密实皮肤需要随后将pH降低至低于9.颜料特别适用于表面涂层和塑料。

17. 发明授权

US09909011B2 Method for coating the surface of inorganic solid particles, especially titanium dioxide pigment particles 有权
公开(公告)号：US09909011B2
公开(公告)日：2018-03-06
申请号：US12472498
申请日：2009-05-27
申请人： Heiko Frahm , Joerg Friedrich , Mark Kaminski , Erwin Schmeier , Lydia Drews-Nicolai , Volker Juergens
发明人： Heiko Frahm , Joerg Friedrich , Mark Kaminski , Erwin Schmeier , Lydia Drews-Nicolai , Volker Juergens
IPC分类号： C09C1/36
CPC分类号： C09C1/3684 , C01P2004/04 , C01P2006/60 , Y10T428/2991
摘要： A method for coating the surface of inorganic solid particles in an aqueous suspension, particularly for coating titanium dioxide with SiO2 includes: a) disagglomeration of the solid particles contained in aqueous suspension, b) addition of a water-soluble precursor of the coating substance to the suspension, c) immediately following step b) homogenization of the suspension, where the temperature and pH value of the suspension do not change significantly in steps a) to c), d) feeding the slurry into a tank and precipitation of the coating substance onto the particle surface and, optionally, application of further coatings, and e) separation of the solid particles from the suspension. The method produces to a highly homogeneous and continuous skin on the particle surface, and to less separately precipitated coating substance.

18. 发明申请

US20100282128A1 Titanium dioxide pigment particles with doped, dense SiO2 skin and methods for their manufacture 有权
标题翻译：具有掺杂，致密SiO 2皮肤的二氧化钛颜料颗粒及其制造方法
公开(公告)号：US20100282128A1
公开(公告)日：2010-11-11
申请号：US12843077
申请日：2010-07-26
申请人： Siegfried Blümel , Lydia Drews-Nicolai
发明人： Siegfried Blümel , Lydia Drews-Nicolai
IPC分类号： C09C1/36 , B05D5/06
CPC分类号： C09C1/3661 , C01P2002/52 , C01P2002/54 , C01P2004/84 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/2991
摘要： A method of predicting photostability of coatings with various dopants on titanium dioxide pigment particles is disclosed. Calculations of the density of states show that a doped coating which reduces the density of states near the band edge or increases the density of states within the band gap of the pigment particles increases the photostability of the doped pigment.
摘要翻译：公开了一种用二氧化钛颜料颗粒预测各种掺杂剂涂层的光稳定性的方法。状态密度的计算表明，降低带边缘附近状态密度或增加颜料颗粒带隙内状态密度的掺杂涂层增加了掺杂颜料的光稳定性。

19. 发明申请

US20060034739A1 Method for the post-treatment of titanium dioxide pigments 失效
标题翻译：二氧化钛颜料后处理方法
公开(公告)号：US20060034739A1
公开(公告)日：2006-02-16
申请号：US11179985
申请日：2005-07-12
申请人： Lydia Drews-Nicolai , Siegfried Bluemel
发明人： Lydia Drews-Nicolai , Siegfried Bluemel
IPC分类号： C22B3/00 , C23C16/00 , C23C16/06
CPC分类号： C09C1/3661 , C01P2002/30 , C01P2004/84 , C01P2006/64 , C08K3/22 , C08K9/02 , C09D7/62
摘要： The invention relates to a method for the post-treatment of titanium dioxide, in order to produce particularly weather-resistant titanium dioxide pigments with good optical properties. The method is characterised in that, together with the hydrous oxides of tin and zirconium, at least one other from the group comprising aluminium, silicon and titanium is additionally precipitated onto the particle surface. The post-treatment components are added to the aqueous TiO2 suspension either in the acidic range (pH value of 3 at most) or in the alkaline range (pH value of 10 at least). The pH value is subsequently set to between 6 and 8. Final tempering of the pigment at elevated temperatures from over 125° C. to up to 500° C. can improve the tone b. The pigment is particularly suitable for use in paints, coatings and plastics.
摘要翻译：本发明涉及一种后处理二氧化钛的方法，以便制备具有良好光学性能的特别耐候的二氧化钛颜料。该方法的特征在于，与锡和锆的水合氧化物一起，还包括从铝，硅和钛组成的组中的至少一种另外沉淀到颗粒表面上。将后处理组分在酸性范围（pH值为3以下）或碱性范围（至少为pH值为10）中添加到TiO 2水溶液中。 pH值随后设定在6和8之间。颜料在高于125℃至高达500℃的高温下进行最终回火可改善色调b。该颜料特别适用于油漆，涂料和塑料。

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