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11. 发明申请

US20100249444A1 Method for Preparation of Cross-Condensed Compound Between Amino Acids and Aminoalkylsilane Having Alkoxy Groups Using Microwave 失效
标题翻译：使用微波制备具有烷氧基的氨基酸和氨基烷基硅烷之间交联化合物的方法
公开(公告)号：US20100249444A1
公开(公告)日：2010-09-30
申请号：US12739598
申请日：2008-02-22
申请人： Ik Mo Lee , Dong Hwan Lee , Ho Sub Kim , Sang Eon Park
发明人： Ik Mo Lee , Dong Hwan Lee , Ho Sub Kim , Sang Eon Park
IPC分类号： C07F7/10
CPC分类号： C07F7/1892
摘要： The present invention provides a method of preparing a cross-condensed compound of an amino-acid derivative and (aminoalkyl) trialkoxysilane using microwave, including: irradiating and heating an amino-acid derivative and (aminoalkyl) trialkoxysilane in a microwave reactor to obtain a reaction product (step 1); and refining the reaction product obtained in the step 1 by removing an unreacted solid material from the reaction product and then leaving the reaction product at room temperature under vacuum to remove excess (aminoalkyl) trialkoxysilane therefrom (step 2). According to the method, since a cross-condensation reaction is performed using microwave, unlike a conventional condensation reaction, economic efficiency is increased due to no catalyst, short reaction time and no solvent. Further, the yield and selectivity of products is increased, and the condensation reaction can be environment-friendly performed because a solvent which can badly influence the environment may not be used.
摘要翻译：本发明提供了使用微波制备氨基酸衍生物和（氨基烷基）三烷氧基硅烷的交联稠合化合物的方法，包括：在微波反应器中照射加热氨基酸衍生物和（氨基烷基）三烷氧基硅烷，得到反应产品（步骤1）; 并通过从反应产物中除去未反应的固体物质，然后在真空下将反应产物在室温下离心以从其中除去过量的（氨基烷基）三烷氧基硅烷，从而精制步骤1中获得的反应产物（步骤2）。根据该方法，由于使用微波进行交联缩合反应，与常规的缩合反应不同，由于没有催化剂，反应时间短，无溶剂，经济效率提高。此外，产物的产率和选择性提高，并且缩合反应可以是环境友好的，因为可能不会使用可能严重影响环境的溶剂。

12. 发明申请

US20070169857A1 Single crystal wire and manufacturing method of the same 审中-公开
标题翻译：单晶线及其制造方法相同
公开(公告)号：US20070169857A1
公开(公告)日：2007-07-26
申请号：US11726272
申请日：2007-03-21
申请人： Se Young Jeong , Chae Ryong Cho , Sang Eon Park , Sung Kyu Kim
发明人： Se Young Jeong , Chae Ryong Cho , Sang Eon Park , Sung Kyu Kim
IPC分类号： C22F1/00
CPC分类号： C30B15/00 , C22B11/02 , C30B11/00 , C30B11/14 , C30B15/36 , C30B29/02 , C30B29/62
摘要： Disclosed are a single crystal wire and a manufacturing method thereof. The method comprises the steps of: placing into a growth crucible at least one metal selected from the group consisting of gold, copper, silver, aluminum and nickel; heating and melting the metal placed in the growth crucible; growing a single crystal using the metal crystal as a seed by the Czochralski or Bridgmari method; cutting the grown single crystal by electric discharge machining; and forming the cut single crystal into a wire. In the method, the grown metal single crystal is formed into a disc-shaped piece by electric discharge machining. The piece is formed into a single crystal wire by wire-cut electric discharge machining, and the single crystal wire can be used as a ring, a pendant or a wire within a high-quality cable making a connection in audio and video systems. Also, the single crystal formed into the disc-shaped piece by electric discharge machining can be used as a substrate and a target for deposition.
摘要翻译：公开了一种单晶线及其制造方法。该方法包括以下步骤：将生长坩埚放入至少一种选自金，铜，银，铝和镍的金属; 加热和熔化置于生长坩埚中的金属; 使用Czochralski或Bridgmari方法生长使用金属晶体作为种子的单晶; 通过放电加工切割生长的单晶; 并将切割的单晶形成线。在该方法中，通过放电加工将生长的金属单晶形成为盘状片。该片通过线切割放电加工形成单晶线，并且单晶线可以用作在音频和视频系统中连接的高质量电缆中的环，吊线或线。此外，通过放电加工形成为盘状片的单晶可以用作基板和沉积靶。

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