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11. 发明授权

US07713449B2 Polymer electrolytic material, polymer electrolytic part, membrane electrode assembly, and polymer electrolyte fuel cell 有权
标题翻译：聚合物电解材料，聚合物电解部分，膜电极组件和聚合物电解质燃料电池
公开(公告)号：US07713449B2
公开(公告)日：2010-05-11
申请号：US10548110
申请日：2004-03-05
申请人： Shinya Adachi , Daisuke Izuhara , Masataka Nakamura , Nobuaki Ito
发明人： Shinya Adachi , Daisuke Izuhara , Masataka Nakamura , Nobuaki Ito
IPC分类号： H01B1/12 , H01M8/02 , C08G79/04 , C08G75/02 , C08G75/20 , C08J9/28
CPC分类号： H01M8/04186 , C09K5/20 , H01B1/122 , H01M4/8605 , H01M4/92 , H01M8/1004 , H01M8/1009 , H01M8/1027 , H01M8/1034 , H01M8/1067 , H01M8/1088 , Y02P70/56
摘要： A polymer electrolytic material has excellent proton conductivity and excellent fuel shutting property, and accordingly provide a polymer electrolytic fuel cell with a high efficiency. This polymer electrolytic material has an unfreezable water ratio Rw1 defined by the following expression (S1) in a range of 20 to 100% by weight in hydrated state: Rw1=[Wnf/Wfc+Wnf)]×100 (S1) in which Wnf represents the unfreezable water content per 1 g of the polymer electrolytic material in dry state and Wfc represents the low freezing point water content per 1 g of the polymer electrolytic material in dry state.
摘要翻译：聚合物电解质材料具有优异的质子传导性和优异的燃料切断性能，因此提供高效率的聚合物电解燃料电池。该聚合物电解质材料在水合状态下具有由下式（S1）定义的不可冻结水比Rw1：水合状态下的20〜100重量％的范围：Rw1 = [Wnf /（Wfc + Wnf）]×100（S1） Wnf表示干燥状态下每1g聚合物电解质材料的不可溶水含量，Wfc表示干燥状态下每1g聚合物电解质材料的低凝固点含水量。

12. 发明申请

US20100196782A1 POLYMER ELECTROLYTE MATERIAL, POLYMER ELECTROLYTE MOLDED PRODUCT USING THE POLYMER ELECTROLYTE MATERIAL, AND METHOD FOR MANUFACTURING THE POLYMER ELECTROLYE MOLDED PRODUCT, MEMBRANE ELECTRODE COMPOSITE, AND SOLID POLYMER FUEL CELL 审中-公开
标题翻译：聚合物电解质材料，使用聚合物电解质材料的聚合物电解质成型产品，以及制造聚合物电解质成型产品，膜电极复合材料和固体聚合物燃料电池的方法
公开(公告)号：US20100196782A1
公开(公告)日：2010-08-05
申请号：US12377263
申请日：2007-08-08
申请人： Daisuke Izuhara , Yuriko Okada
发明人： Daisuke Izuhara , Yuriko Okada
IPC分类号： H01M8/10 , H01M6/18
CPC分类号： H01M8/1025 , C08G65/4012 , C08G65/4056 , C08J5/2256 , C08J5/2262 , C08J2371/10 , C08J2371/12 , C08J2387/00 , C08L2205/05 , H01B1/122 , H01M8/1067 , H01M8/1072 , H01M2008/1095 , H01M2300/0082 , Y02P20/582 , Y02P70/56
摘要： It is an object of the present invention to provide a polymer electrolyte material which has excellent proton conductivity even under the conditions of a low humidity or a low temperature and is excellent in mechanical strength and fuel barrier properties, and which moreover can achieve high output, high energy density and long-term durability in forming a polymer electrolyte fuel cell therefrom, and a polymer electrolyte form article using the same and a method for producing the same, a membrane electrode assembly and a polymer electrolyte fuel cell, each using the same.The present invention employs the following means. Namely, the polymer electrolyte material of the present invention is a polymer electrolyte material including a constituent unit (A1) containing an ionic group and a constituent unit (A2) substantially not containing an ionic group, wherein a phase separation structure is observed by a transmission electron microscope and a crystallization heat measured by differential scanning calorimetry is 0.1 J/g or more, or a phase separation structure is observed by a transmission electron microscope and the degree of crystallinity measured by wide angle X-ray diffraction is 0.5% or more. Also, the polymer electrolyte form article, the membrane electrode assembly and the polymer electrolyte fuel cell of the present invention are characterized by being composed of such polymer electrolyte materials.
摘要翻译：本发明的目的是提供即使在低湿度或低温条件下也具有优异的质子传导性并且机械强度和燃料阻隔性优异的高分子电解质材料，并且还可实现高输出，高能量密度和从其形成聚合物电解质燃料电池的长期耐久性，以及使用该固体高分子型燃料电池的高分子电解质成形体及其制造方法，膜电极组件和聚合物电解质型燃料电池。本发明采用以下方式。也就是说，本发明的高分子电解质材料是包含具有离子性基团的构成单元（A1）和基本上不含有离子性基团的构成单元（A2）的高分子电解质材料，其中通过透射率观察到相分离结构电子显微镜和通过差示扫描量热法测量的结晶热为0.1J / g以上，或者通过透射电子显微镜观察到相分离结构，通过广角X射线衍射测定的结晶度为0.5％以上。此外，本发明的高分子电解质成形体，膜电极接合体以及固体高分子型燃料电池的特征在于，由上述高分子电解质材料构成。

13. 发明申请

US20140322628A1 POLYMER ELECTROLYTE MEMBRANE, MEMBRANE ELECTRODE ASSEMBLY USING SAME AND POLYMER ELECTROLYTE FUEL CELL 审中-公开
标题翻译：聚合物电解质膜，使用其的膜电极组件和聚合物电解质燃料电池
公开(公告)号：US20140322628A1
公开(公告)日：2014-10-30
申请号：US14240754
申请日：2012-08-24
申请人： Hiroaki Umeda , Daisuke Izuhara , Emi Amano
发明人： Hiroaki Umeda , Daisuke Izuhara , Emi Amano
IPC分类号： H01M8/10
CPC分类号： H01M8/102 , C08G65/40 , C08G65/4012 , C08G65/4043 , C08G65/48 , C08G2650/40 , C08J5/2256 , C08J2371/12 , H01B1/122 , H01M8/1023 , H01M2008/1095
摘要： To provide a polymer electrolyte membrane that has excellent proton conductivity even under low-humidification conditions, has excellent mechanical strength and chemical stability, and can achieve high output and excellent physical durability when made into a polymer electrolyte fuel cell.The polymer electrolyte membrane includes a block copolymer containing each one or more of: a segment (A1) containing anionic group; and a segment (A2) not containing an ionic group. The polymer electrolyte membrane forms a co-continuous (M1) or lamellar phase-separated (M2) structure, and gives a crystallization heat quantity of 0.1 J/g or larger determined by differential scanning calorimetry, or a degree of crystallinity of 0.5% or larger determined by wide-angle X-ray diffractometry.
摘要翻译：为了提供即使在低加湿条件下也具有优异的质子传导性的聚合物电解质膜，具有优异的机械强度和化学稳定性，并且在制成聚合物电解质燃料电池时可以实现高产出和优异的物理耐久性。聚合物电解质膜包括含有以下中的一种或多种的嵌段共聚物：含有阴离子基团的链段（A1）和不含离子基团的链段（A2）。聚合物电解质膜形成共连续（M1）或层状相分离（M2）结构，并且通过差示扫描量热法或结晶度为0.5％得到0.1J / g以上的结晶热量或由广角X射线衍射测定。

14. 发明申请

US20140193742A1 BLOCK COPOLYMER, MANUFACTURING METHOD THEREFOR, AND POLYMER ELECTROLYTE MATERIAL, MOLDED POLYMER ELECTROLYTE, AND SOLID-POLYMER FUEL CELL USING SAID BLOCK COPOLYMER 有权
标题翻译：嵌段共聚物，其制造方法和聚合物电解质材料，模塑聚合物电解质和使用嵌段共聚物的固体聚合物燃料电池
公开(公告)号：US20140193742A1
公开(公告)日：2014-07-10
申请号：US14187243
申请日：2012-08-23
申请人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
发明人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
IPC分类号： H01M8/10
CPC分类号： H01M8/1025 , C08G65/4012 , C08G65/4025 , C08G65/4037 , C08G65/405 , C08G65/4056 , C08G65/48 , C08G2650/40 , C08J5/2256 , C08J2371/12 , H01B1/122 , H01M8/0289 , H01M8/1083 , H01M2300/0082 , Y02E60/523 , Y02P70/56
摘要： To provide: a block copolymer that exhibits excellent proton conductivity even under low-humidification conditions, exhibits excellent mechanical strength and chemical stability, and when used in a polymer electrolyte fuel cell, allows high output and excellent physical durability; a polymer electrolyte material; and a polymer electrolyte form article and a polymer electrolyte fuel cell, using the same.The block copolymer of the present invention includes each one or more of: a segment (A1) containing an ionic group; a segment (A2) not containing an ionic group; and a linker moiety connecting the segments. The segment (A1) containing an ionic group comprises a constituent unit represented by a specific structure. The polymer electrolyte material, the polymer electrolyte form article, and the polymer electrolyte fuel cell according to the present invention are manufactured by using the above block copolymer.
摘要翻译：为了提供：即使在低加湿条件下也显示出优异的质子传导性的嵌段共聚物，显示出优异的机械强度和化学稳定性，并且当用于聚合物电解质燃料电池时，可以实现高输出和优异的物理耐久性; 聚合物电解质材料; 以及使用其的聚合物电解质成型体和固体高分子型燃料电池。本发明的嵌段共聚物包括以下各项中的一种或多种：含有离子性基团的链段（A1）不含离子基团的片段（A2）; 和连接部分的连接体部分。含有离子基团的链段（A1）包括由特定结构表示的结构单元。通过使用上述嵌段共聚物制造本发明的高分子电解质材料，高分子电解质成形体和固体高分子型燃料电池。

15. 发明授权

US09653745B2 Block copolymer, manufacturing method therefor, and polymer electrolyte material, molded polymer electrolyte, and solid-polymer fuel cell using said block copolymer 有权
公开(公告)号：US09653745B2
公开(公告)日：2017-05-16
申请号：US14187243
申请日：2012-08-21
申请人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
发明人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
IPC分类号： H01M8/102 , H01M8/1025 , H01B1/12 , H01M8/1069 , C08J5/22 , C08G65/40 , C08G65/48 , H01M8/0289
CPC分类号： H01M8/1025 , C08G65/4012 , C08G65/4025 , C08G65/4037 , C08G65/405 , C08G65/4056 , C08G65/48 , C08G2650/40 , C08J5/2256 , C08J2371/12 , H01B1/122 , H01M8/0289 , H01M8/1083 , H01M2300/0082 , Y02E60/523 , Y02P70/56
摘要： To provide: a block copolymer that exhibits excellent proton conductivity even under low-humidification conditions, exhibits excellent mechanical strength and chemical stability, and when used in a polymer electrolyte fuel cell, allows high output and excellent physical durability; a polymer electrolyte material; and a polymer electrolyte form article and a polymer electrolyte fuel cell, using the same.The block copolymer of the present invention includes each one or more of: a segment (A1) containing an ionic group; a segment (A2) not containing an ionic group; and a linker moiety connecting the segments. The segment (A1) containing an ionic group comprises a constituent unit represented by a specific structure. The polymer electrolyte material, the polymer electrolyte form article, and the polymer electrolyte fuel cell according to the present invention are manufactured by using the above block copolymer.

16. 发明申请

US20150094446A1 SULFONIC ACID GROUP-CONTAINING POLYMER, SULFONIC ACID GROUP-CONTAINING AROMATIC COMPOUND AND METHOD OF MAKING THE SAME, AS WELL AS POLYMER ELECTROLYTE MATERIAL, POLYMER ELECTROLYTE MOLDED PRODUCT AND SOLID POLYMER FUEL CELL USING THE SAME 有权
标题翻译：含有磺酸基团的聚合物，含有磺酸基团的芳族化合物及其制备方法，作为聚合物电解质材料，聚合物电解质成型产品和使用该聚合物的固体聚合物燃料电池
公开(公告)号：US20150094446A1
公开(公告)日：2015-04-02
申请号：US14346288
申请日：2012-09-06
申请人： Qiao Chen , Fangke Shao , Gang Wu , Daisuke Izuhara , Hiroaki Umeda
发明人： Qiao Chen , Fangke Shao , Gang Wu , Daisuke Izuhara , Hiroaki Umeda
IPC分类号： C08G65/00 , C07C317/14 , H01M8/10 , C07C309/00
CPC分类号： C08G65/00 , C07C309/00 , C07C309/44 , C07C317/14 , C08G65/4043 , C08G65/4056 , H01B1/122 , H01M8/1023 , H01M8/1025 , H01M8/1032 , H01M8/1034 , H01M2008/1095 , H01M2300/0082 , Y02P70/56
摘要： It is an object of the present invention to provide a sulfonic acid group-containing polymer and a sulfonic acid group-containing aromatic compound, which have excellent proton conductivity even under the low humidification condition, are excellent in mechanical strength and chemical stability and, moreover, can attain high output and excellent physical durability when processed into a solid polymer fuel cell, as well as a polymer electrolyte material, a polymer electrolyte molded product and a solid polymer fuel cell respectively using the same. The sulfonic acid group-containing polymer of the present invention is a sulfonic acid group-containing polymer comprising a constituent unit containing a sulfonic acid group (A1), and a constituent unit not containing a sulfonic acid group (A2), wherein the polymer contains a constituent unit having a specified structure as at least one constituent unit containing a sulfonic acid group (A1) at 25 mol % or more based on a sum of the constituent unit containing a sulfonic acid group (A1). Further, the polymer electrolyte material, polymer electrolyte molded product and solid polymer fuel cell of the present invention are constituted using such a sulfonic acid group-containing polymer.
摘要翻译：本发明的目的是提供即使在低加湿条件下也具有优异的质子传导性的含磺酸基的聚合物和含磺酸基的芳族化合物，其机械强度和化学稳定性优异，而且当加工成固体聚合物燃料电池时，可以获得高产量和优异的物理耐久性，以及分别使用它们的聚合物电解质材料，聚合物电解质模制产品和固体聚合物燃料电池。本发明的含磺酸基的聚合物是含有含有磺酸基（A1）的构成单元和不含磺酸基（A2）的构成单元的含磺酸基的聚合物，其中，聚合物含有基于含有磺酸基（A1）的构成单元的总和，具有指定结构的构成单元作为至少一种含有25mol％以上的磺酸基（A1）的构成单元。此外，本发明的高分子电解质材料，高分子电解质成型体和固体高分子型燃料电池使用这样的含有磺酸基的聚合物构成。

17. 发明授权

US08318894B2 Charged polymers and their uses in electronic devices 失效
标题翻译：带电聚合物及其在电子设备中的应用
公开(公告)号：US08318894B2
公开(公告)日：2012-11-27
申请号：US13033441
申请日：2011-02-23
申请人： Timothy M. Swager , Daisuke Izuhara
发明人： Timothy M. Swager , Daisuke Izuhara
IPC分类号： C08G73/00
CPC分类号： C08G61/122 , C08G2261/3221 , C08G2261/344 , C08G2261/412 , C08G2261/72 , C08G2261/91 , C08G2261/92 , H01B1/128 , H01L51/0036 , H01L51/0043 , H01L51/424 , Y02E10/549
摘要： The present invention generally relates to compositions and methods comprising charged polymers. The compositions can be used in a variety of applications, for example, in photovoltaic cells, field-effect transistors, and light emitting diodes. In some embodiments, the backbone of a charged polymer comprises at least one quaternary nitrogen and/or is conjugated.
摘要翻译：本发明一般涉及包含带电聚合物的组合物和方法。该组合物可用于各种应用中，例如在光伏电池，场效应晶体管和发光二极管中。在一些实施方案中，带电聚合物的主链包含至少一个季氮和/或共轭。

18. 发明授权

US09701789B2 Sulfonic acid group-containing polymer, sulfonic acid group-containing aromatic compound and method of making the same, as well as polymer electrolyte material, polymer electrolyte molded product and solid polymer fuel cell using the same 有权
公开(公告)号：US09701789B2
公开(公告)日：2017-07-11
申请号：US14346288
申请日：2012-09-06
申请人： Qiao Chen , Fangke Shao , Gang Wu , Daisuke Izuhara , Hiroaki Umeda
发明人： Qiao Chen , Fangke Shao , Gang Wu , Daisuke Izuhara , Hiroaki Umeda
IPC分类号： C08G65/40 , C08G65/00 , C07C309/44 , H01B1/12 , H01M8/1023 , H01M8/1025 , H01M8/1032 , H01M8/1034 , C07C309/00 , C07C317/14 , H01M8/1018
CPC分类号： C08G65/00 , C07C309/00 , C07C309/44 , C07C317/14 , C08G65/4043 , C08G65/4056 , H01B1/122 , H01M8/1023 , H01M8/1025 , H01M8/1032 , H01M8/1034 , H01M2008/1095 , H01M2300/0082 , Y02P70/56
摘要： It is an object of the present invention to provide a sulfonic acid group-containing polymer and a sulfonic acid group-containing aromatic compound, which have excellent proton conductivity even under the low humidification condition, are excellent in mechanical strength and chemical stability and, moreover, can attain high output and excellent physical durability when processed into a solid polymer fuel cell, as well as a polymer electrolyte material, a polymer electrolyte molded product and a solid polymer fuel cell respectively using the same. The sulfonic acid group-containing polymer of the present invention is a sulfonic acid group-containing polymer comprising a constituent unit containing a sulfonic acid group (A1), and a constituent unit not containing a sulfonic acid group (A2), wherein the polymer contains a constituent unit having a specified structure as at least one constituent unit containing a sulfonic acid group (A1) at 25 mol % or more based on a sum of the constituent unit containing a sulfonic acid group (A1). Further, the polymer electrolyte material, polymer electrolyte molded product and solid polymer fuel cell of the present invention are constituted using such a sulfonic acid group-containing polymer.

19. 发明授权

US09126908B2 Aromatic sulfonic acid derivative, sulfonic acid group-containing polymer, block copolymer, polymer electrolyte material, polymer electrolyte form article, and polymer electrolyte fuel cell 有权
标题翻译：芳族磺酸衍生物，含磺酸基的聚合物，嵌段共聚物，聚合物电解质材料，聚合物电解质成型体和聚合物电解质燃料电池
公开(公告)号：US09126908B2
公开(公告)日：2015-09-08
申请号：US14130300
申请日：2012-06-27
申请人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
发明人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
IPC分类号： C08G75/24 , C08G65/40 , C07C317/22 , H01B1/12 , C07C309/60 , H01B1/06 , H01M4/86 , H01M8/02 , H01M8/10
CPC分类号： H01M8/1032 , C07C309/44 , C07C309/60 , C07C317/22 , C08G65/40 , C08G65/4012 , C08G65/4056 , C08G2650/40 , H01B1/122 , H01M8/1025 , H01M8/1027 , H01M8/1039 , H01M2008/1095 , H01M2300/0082 , Y02E60/521
摘要： Provided are an aromatic sulfonic acid derivative and a sulfonic acid group-containing polymer, each of which has excellent proton conductivity even under low humidification conditions, while having excellent mechanical strength and chemical stability, and enables a solid polymer fuel cell to achieve high output and excellent physical durability when used therein. This aromatic sulfonic acid derivative has a specific structure and is characterized in that a sulfonic acid group is introduced into more than 50% of all the phenyl groups. This sulfonic acid group-containing polymer is characterized by being obtained by polymerization using the aromatic sulfonic acid derivative, and is also characterized by having a specific structure.
摘要翻译：提供了即使在低加湿条件下也具有优异的质子传导性的芳香族磺酸衍生物和含磺酸基的聚合物，同时具有优异的机械强度和化学稳定性，并且能够使固体高分子型燃料电池实现高输出，使用时具有良好的物理耐久性。该芳香族磺酸衍生物具有特定的结构，其特征在于，在全部苯基的50％以上引入磺酸基。该含磺酸基的聚合物的特征在于通过使用芳香族磺酸衍生物的聚合得到，特征在于具有特定的结构。

20. 发明申请

US20140213671A1 AROMATIC SULFONIC ACID DERIVATIVE, SULFONIC ACID GROUP-CONTAINING POLYMER, BLOCK CO-POLYMER, POLYMER ELECTROLYTE MATERIAL, POLYMER ELECTROLYTE MOLDED BODY, AND SOLID POLYMER FUEL CELL 有权
标题翻译：芳香磺酸衍生物，含硫酸基团聚合物，嵌段共聚物，聚合物电解质材料，聚合物电解质模体和固体聚合物燃料电池
公开(公告)号：US20140213671A1
公开(公告)日：2014-07-31
申请号：US14130300
申请日：2012-06-27
申请人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
发明人： Daisuke Izuhara , Hiroaki Umeda , Emi Amano , Tomoyuki Kunita
IPC分类号： C07C317/22 , H01M8/10 , C07C309/60
CPC分类号： H01M8/1032 , C07C309/44 , C07C309/60 , C07C317/22 , C08G65/40 , C08G65/4012 , C08G65/4056 , C08G2650/40 , H01B1/122 , H01M8/1025 , H01M8/1027 , H01M8/1039 , H01M2008/1095 , H01M2300/0082 , Y02E60/521
摘要： Provided are an aromatic sulfonic acid derivative and a sulfonic acid group-containing polymer, each of which has excellent proton conductivity even under low humidification conditions, while having excellent mechanical strength and chemical stability, and enables a solid polymer fuel cell to achieve high output and excellent physical durability when used therein. This aromatic sulfonic acid derivative has a specific structure and is characterized in that a sulfonic acid group is introduced into more than 50% of all the phenyl groups. This sulfonic acid group-containing polymer is characterized by being obtained by polymerization using the aromatic sulfonic acid derivative, and is also characterized by having a specific structure.
摘要翻译：提供了即使在低加湿条件下也具有优异的质子传导性的芳香族磺酸衍生物和含磺酸基的聚合物，同时具有优异的机械强度和化学稳定性，并且能够使固体高分子型燃料电池实现高输出，使用时具有良好的物理耐久性。该芳香族磺酸衍生物具有特定的结构，其特征在于，在全部苯基的50％以上引入磺酸基。该含磺酸基的聚合物的特征在于通过使用芳香族磺酸衍生物的聚合得到，特征在于具有特定的结构。

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