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11. 发明授权

US08507404B2 Regenerable sulfur traps for on-board vehicle applications 有权
标题翻译：可再生的用于车载应用的硫捕集器
公开(公告)号：US08507404B2
公开(公告)日：2013-08-13
申请号：US12082351
申请日：2008-04-10
申请人： El-Mekki El-Malki , Walter Weissman , Paul J. Polini
发明人： El-Mekki El-Malki , Walter Weissman , Paul J. Polini
IPC分类号： B01J23/00 , B01J21/00 , B01J20/00
CPC分类号： B01D53/9495 , B01D53/9404 , B01D53/9459 , B01D53/9477 , B01D2251/202 , B01D2255/1021 , B01D2255/2042 , B01D2255/2063 , B01D2255/2065 , B01D2255/2073 , B01D2255/20738 , B01D2255/50 , B01D2255/9207 , B01D2257/302 , F01N3/0807 , F01N3/0814 , F01N3/0821 , F01N3/0842 , F01N3/085 , F01N13/009 , F01N2370/02 , F01N2610/04
摘要： Provided are improved regenerable SOx trap formulations for on-board vehicle applications. The regenerable sulfur trap formulations reduce the rate of sulfur poisoning of a downstream nitrogen storage reduction (NSR) catalyst trap in exhaust gas cleaning systems for combustion engines by adsorbing SOx as metal sulfate under lean exhaust conditions and desorbing the accumulated SOx under rich exhaust conditions. The regenerable sulfur oxides trap catalyst compositions include a metal (M) oxide, wherein M is selected from Cu, Fe, Mn, Ag, Co and combinations thereof and a metal (M)-La—Zr oxide, wherein M is selected from Cu, Fe, Mn, Ag, Co and combinations thereof. In addition, provided are improved exhaust gas cleaning systems and methods for treating exhaust gas from a combustion source that include a hydrogen generation system, a regenerable sulfur oxides trap, and a regenerable nitrogen storage reduction (NSR) catalyst trap. The improved exhaust gas cleaning systems and methods allow for the sulfur released from the sulfur trap to pass through the nitrogen oxide trap with no or little poisoning of NOx storage and reduction sites, which significantly improves NSR catalyst trap lifetime and performance to meet future emissions standards. The disclosed exhaust gas cleaning systems are suitable for use in internal combustion engines (e.g., diesel, gasoline, CNG) which operate with lean air/fuel ratios over most of the operating period.
摘要翻译：提供了用于车载车辆应用的改进的可再生SOx捕集剂配方。可再生硫捕集器配方通过在贫排气条件下吸附SO x作为金属硫酸盐并在富排气条件下解吸累积的SOx，降低了内燃机废气净化系统中下游氮储存还原（NSR）催化剂阱的硫中毒速率。可再生硫氧化物捕集催化剂组合物包括金属（M）氧化物，其中M选自Cu，Fe，Mn，Ag，Co及其组合和金属（M）-La-Zr氧化物，其中M选自Cu ，Fe，Mn，Ag，Co及其组合。此外，提供了改进的废气净化系统和用于处理来自燃烧源的废气的废气净化系统和方法，所述燃烧源包括氢气产生系统，可再生硫氧化物捕集器和可再生氮储存还原（NSR）催化剂阱。改进的废气净化系统和方法允许从硫捕获器释放的硫通过氮氧化物捕集器，没有或少量的NOx储存和还原位点的中毒，这显着地提高了NSR催化剂捕集器的使用寿命和性能以满足未来的排放标准。所公开的废气清洁系统适用于在大部分操作周期内以稀薄空气/燃料比运行的内燃机（例如柴油，汽油，CNG）。

12. 发明申请

US20080307779A1 Regenerable sulfur traps for on-board vehicle applications 有权
标题翻译：可再生的用于车载应用的硫捕集器
公开(公告)号：US20080307779A1
公开(公告)日：2008-12-18
申请号：US12082351
申请日：2008-04-10
申请人： El-Mekki El-Malki , Walter Weissman , Paul J. Polini
发明人： El-Mekki El-Malki , Walter Weissman , Paul J. Polini
IPC分类号： B01J23/745 , B01J23/58 , B01J23/34 , B01J23/42 , B01J23/50 , B01J23/56 , B01J23/66 , B01J23/72 , F01N3/20 , F01N3/023
CPC分类号： B01D53/9495 , B01D53/9404 , B01D53/9459 , B01D53/9477 , B01D2251/202 , B01D2255/1021 , B01D2255/2042 , B01D2255/2063 , B01D2255/2065 , B01D2255/2073 , B01D2255/20738 , B01D2255/50 , B01D2255/9207 , B01D2257/302 , F01N3/0807 , F01N3/0814 , F01N3/0821 , F01N3/0842 , F01N3/085 , F01N13/009 , F01N2370/02 , F01N2610/04
摘要： Provided are improved regenerable SOx trap formulations for on-board vehicle applications. The regenerable sulfur trap formulations reduce the rate of sulfur poisoning of a downstream nitrogen storage reduction (NSR) catalyst trap in exhaust gas cleaning systems for combustion engines by adsorbing SOx as metal sulfate under lean exhaust conditions and desorbing the accumulated SOx under rich exhaust conditions. The regenerable sulfur oxides trap catalyst compositions include a metal (M) oxide, wherein M is selected from Cu, Fe, Mn, Ag, Co and combinations thereof and a metal (M)-La—Zr oxide, wherein M is selected from Cu, Fe, Mn, Ag, Co and combinations thereof. In addition, provided are improved exhaust gas cleaning systems and methods for treating exhaust gas from a combustion source that include a hydrogen generation system, a regenerable sulfur oxides trap, and a regenerable nitrogen storage reduction (NSR) catalyst trap. The improved exhaust gas cleaning systems and methods allow for the sulfur released from the sulfur trap to pass through the nitrogen oxide trap with no or little poisoning of NOx storage and reduction sites, which significantly improves NSR catalyst trap lifetime and performance to meet future emissions standards. The disclosed exhaust gas cleaning systems are suitable for use in internal combustion engines (e.g., diesel, gasoline, CNG) which operate with lean air/fuel ratios over most of the operating period.
摘要翻译：提供了用于车载车辆应用的改进的可再生SOx捕集剂配方。可再生硫捕集器配方通过在贫排气条件下吸附SO x作为金属硫酸盐并在富排气条件下解吸累积的SOx，降低了内燃机废气净化系统中下游氮储存还原（NSR）催化剂阱的硫中毒速率。可再生硫氧化物捕集催化剂组合物包括氧化金属（M），其中M选自Cu，Fe，Mn，Ag，Co及其组合和金属（M）-La-Zr氧化物，其中M选自Cu ，Fe，Mn，Ag，Co及其组合。此外，提供了改进的废气净化系统和用于处理来自燃烧源的废气的废气净化系统和方法，所述燃烧源包括氢气产生系统，可再生硫氧化物捕集器和可再生氮储存还原（NSR）催化剂阱。改进的废气净化系统和方法允许从硫捕获器释放的硫通过氮氧化物捕集器，没有或少量的NOx储存和还原位点的中毒，这显着地提高了NSR催化剂捕集器的使用寿命和性能以满足未来的排放标准。所公开的废气清洁系统适用于在大部分操作周期内以稀薄空气/燃料比运行的内燃机（例如柴油，汽油，CNG）。

13. 发明授权

US07282192B2 Mixed metal oxide containing sulfur 有权
标题翻译：含硫的混合金属氧化物
公开(公告)号：US07282192B2
公开(公告)日：2007-10-16
申请号：US11644619
申请日：2006-12-22
申请人： James Clarke Vartuli , Jeffrey T. Elks , El-Mekki El-Malki , William G. Borghard , Doron Levin , Stephen John McCarthy
发明人： James Clarke Vartuli , Jeffrey T. Elks , El-Mekki El-Malki , William G. Borghard , Doron Levin , Stephen John McCarthy
IPC分类号： C01F17/00 , C01G23/00 , C01G25/00 , C01G27/00
CPC分类号： B01J23/002 , B01J23/10 , B01J27/053 , B01J35/002 , B01J2523/00 , C07C1/20 , C07C29/10 , C07C11/02 , B01J2523/3712 , B01J2523/48 , B01J2523/62 , C07C31/10
摘要： The invention relates to a composition of matter comprising at least one metal from Group 3, at least one metal from Group 4, sulfur and oxygen, particularly useful as a catalyst for ether decomposition to alkanols and alkenes.
摘要翻译：本发明涉及包含至少一种第3族金属，至少一种第4族金属，硫和氧的物质组合物，特别可用作乙醚分解成链烷醇和烯烃的催化剂。

14. 发明授权

US08536085B2 Preparation of high activity cobalt catalysts, the catalysts and their use 有权
标题翻译：制备高活性钴催化剂，催化剂及其用途
公开(公告)号：US08536085B2
公开(公告)日：2013-09-17
申请号：US13279709
申请日：2011-10-24
申请人： Stuart L. Soled , Joseph E. Baumgartner , Christine E. Kliewer , El-Mekki El-Malki , Patricia A. Bielenberg
发明人： Stuart L. Soled , Joseph E. Baumgartner , Christine E. Kliewer , El-Mekki El-Malki , Patricia A. Bielenberg
IPC分类号： B01J23/75 , B01J23/36
CPC分类号： B01J23/75 , B01J21/06 , B01J21/063 , B01J23/8896 , B01J35/002 , B01J35/006 , B01J35/1014 , B01J35/1038 , B01J37/0045 , B01J37/088 , B01J37/18 , C10G2/332
摘要： A method is provided for preparing a supported cobalt-containing catalyst having substantially homogeneously dispersed, small cobalt crystallites. The method comprises depositing cobalt nitrate on a support and then subjecting the support to a two-step decomposition protocol. In the first step, the support is heated in an oxygen-containing, substantially water-free atmosphere to about 160° C. to form an intermediate decomposition product. This intermediate product is then or hydrolyzed and reduced, or hydrolyzed, calcined and reduced.
摘要翻译：提供了一种制备具有基本上均匀分散的小钴微晶的负载的含钴催化剂的方法。该方法包括在载体上沉积硝酸钴，然后使载体经受两步分解方案。在第一步骤中，将载体在含氧的基本上无水的气氛中加热至约160℃以形成中间分解产物。然后将该中间产物水解并还原或水解，煅烧和还原。

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