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11. 发明申请

US20080287636A1 Curable Composition 有权
标题翻译：可固化成分
公开(公告)号：US20080287636A1
公开(公告)日：2008-11-20
申请号：US11579630
申请日：2005-04-25
申请人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
发明人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
IPC分类号： C08G77/00
CPC分类号： C08G65/336 , C08K3/014 , C08K5/0091 , C08K5/544 , C09D171/02 , C09J171/02 , C09K3/10 , C08L101/10 , C08L71/02
摘要： [PROBLEMS] There is provided a curable composition having good curability and adhesiveness. [MEANS FOR SOLVING] A curable composition by comprising (A) an reactive silicon group-containing organic polymer,(B) a titanium chelate represented by the general formula (1) or (2),(C) a high molecular weight plasticizer having a number average molecular weight of 1000 to 15000:General Formula (1): wherein each of n R1's is independently a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, each of (4-n) R2's is independently hydrogen atom or a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, each of (4-n) A1's and (4-n) A2's is independently —R3 or —OR3 where R3 is a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, n is 1, 2, or 3. General Formula wherein R2, A1 and A2 are the same as defined above, R4 is a substituted or unsubstituted divalent hydrocarbon group havimg 1 to 20 carbon atoms.
摘要翻译： [问题]提供了具有良好的固化性和粘合性的固化性组合物。 [解决方案]一种可固化组合物，其包含（A）含反应性硅基的有机聚合物，（B）由通式（1）或（2）表示的钛螯合物，（C）具有数均分子量为1000〜15000：通式（1）：其中n R 1各自独立地为取代或未取代的碳原子数1〜20的烃基，（4 -n）R 2独立地为氢原子或取代或未取代的碳原子数1〜20的烃基，（4-n）A 1〜和（4-n）A 2独立地为-R 3或-OR 3，其中R 3为是具有1至20个碳原子的取代或未取代的烃基，n为1,2或3.其中R 2，A 1和A 2的通式为 2 与上述定义相同，R 4是取代或未取代的2至20碳a的二价烃基手铐

12. 发明申请

US20080076878A1 Curable Composition Having Improved Curability and Adhesion 有权
标题翻译：具有改善固化性和粘合性的可固化组合物
公开(公告)号：US20080076878A1
公开(公告)日：2008-03-27
申请号：US11579551
申请日：2005-04-25
申请人： Masayuki Wakioka , Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
发明人： Masayuki Wakioka , Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
IPC分类号： C08L43/04 , C08L31/02
CPC分类号： C08G65/336 , C08K3/014 , C08K5/0091 , C08K5/544 , C09D171/02 , C09J171/02 , C09K3/10 , C08L101/10 , C08L71/02
摘要： [Problems] There is provided a curable composition having good curability and adhesion by using a non-organotin catalyst.[Means to Solve Problems] The curable composition comprising (A) an organic polymer having a reactive silicon group as a silicon-containing group being capable of crosslinking by forming siloxane bonds, (B) one or more kinds selected from a titanium catalyst, an aluminum catalyst and a zirconium catalyst, and (C) a low molecular weight compound containing a hydrolyzable silicon group and having a molecular weight of 100 to 1,000, characterized in that a ratio (a/b) of the total mole (a) of titanium atoms, aluminum atoms and zirconium atoms of the component (B) to the total mole (b) of silicon atoms of the component (c) is larger than 0.08.
摘要翻译： [问题]提供了通过使用非有机锡催化剂具有良好的固化性和粘合性的固化性组合物。 [解决问题的方法]可固化组合物包含（A）具有通过形成硅氧烷键而能够交联的具有反应性硅基团的含硅基团的有机聚合物，（B）选自钛催化剂，铝催化剂和锆催化剂，和（C）含有可水解硅基并且分子量为100〜1000的低分子量化合物，其特征在于钛的总摩尔（a）的比（a / b）组分（B）的原子，铝原子和锆原子与组分（c）的硅原子的总摩尔数（b）大于0.08。

13. 发明申请

US20080033087A1 Curable Composition 有权
标题翻译：可固化成分
公开(公告)号：US20080033087A1
公开(公告)日：2008-02-07
申请号：US11579405
申请日：2005-04-25
申请人： Toshihiko Okamoto , Masato Kusakabe
发明人： Toshihiko Okamoto , Masato Kusakabe
IPC分类号： C08J3/24
CPC分类号： C08G65/336 , C08K3/014 , C08K5/0091 , C08K5/544 , C09D171/02 , C09J171/02 , C09K3/10 , C08L101/10 , C08L71/02
摘要： [Problem] There is provided a curable composition having high thixotropy and satisfactory curability by use of a non-organotin catalyst. [Means to Solve] A curable composition comprising (A) a polyoxyalkylene polymer having a silicon-containing group being capable of crosslinking by forming siloxane bonds and/or a (meth)acrylate polymer having a silicon-containing group being capable of crosslinking by forming siloxane bonds, (B) a titanium chelate, and (C) an amide wax type thixotropy-imparting agent.
摘要翻译： [问题]提供了通过使用非有机锡催化剂具有高触变性和令人满意的固化性的可固化组合物。 [解决方案]一种可固化组合物，其包含（A）具有能够通过形成硅氧烷键交联的含硅基团的聚氧化烯聚合物和/或具有含硅基团的（甲基）丙烯酸酯聚合物，其可以通过形成硅氧烷键，（B）钛螯合物和（C）酰胺蜡型触变性赋予剂。

14. 发明申请

US20070203297A1 Curable Composition 审中-公开
标题翻译：可固化成分
公开(公告)号：US20070203297A1
公开(公告)日：2007-08-30
申请号：US11547028
申请日：2005-03-18
申请人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
发明人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
IPC分类号： C08L71/02
CPC分类号： C08F293/005 , C08K5/09 , C08L43/04 , C08L53/00 , C08L71/02 , C09D153/00 , C08L83/12 , C08L2666/22 , C08L2666/02
摘要： The present invention has its object to provide a curable composition which has good curability and adhesiveness while containing an organotin-free catalyst. The present invention provides a one package curable composition which comprises (A) a polyoxyalkylene polymer having a silicon-containing group capable of crosslinking by forming a siloxane bond, (B) a (meth)acrylic ester polymer having a silicon-containing group capable of crosslinking by forming a siloxane bond and compatible with the component (A), and (C) (c1) a carboxylic acid of which the carbon atom adjacent to a carbonyl group is a quaternary carbon, and/or (c2) a metal carboxylate of which the carbon atom adjacent to a carbonyl group is a quaternary carbon.
摘要翻译：本发明的目的是提供一种含有无机锡催化剂的固化性和粘合性优异的固化性组合物。本发明提供一种包装可固化组合物，其包含（A）具有能够通过形成硅氧烷键交联的含硅基团的聚氧化烯聚合物，（B）具有含硅基团的（甲基）丙烯酸酯聚合物，通过形成硅氧烷键并与组分（A）相容的交联，和（C）（c1）与羰基相邻的碳原子为季碳的羧酸和/或（c2）羧酸金属的其中与羰基相邻的碳原子是季碳。

15. 发明授权

US06441101B1 Processes for preparing (METH) acrylic polymers having functional groups at the chain ends 失效
标题翻译：在链末端制备具有官能团的（METH）丙烯酸聚合物的方法
公开(公告)号：US06441101B1
公开(公告)日：2002-08-27
申请号：US09583106
申请日：1999-09-15
申请人： Masato Kusakabe , Kenichi Kitano
发明人： Masato Kusakabe , Kenichi Kitano
IPC分类号： C08F842
CPC分类号： C08F8/26 , C08F8/42 , C08F20/00
摘要： (Meth)acrylic polymers having alkenyl or curable silyl groups at the chain ends in high functionality ratios are prepared by a process which comprises (i) preparing a (meth)acrylic polymer having halogen atoms at the chain ends, using an organohalogenated compound or a halosulfonyl compound as an initiator and a metal complex catalyst wherein the central metal atom is selected from the group consisting of the elements of Groups 8, 9, 10 and 11 of the periodic table; and (ii) transforming the halogen atom into an alkenyl group- or a curable silyl group-containing substituent. The obtained (meth)acrylic polymers form homogeneous curing materials.
摘要翻译：通过包括（i）使用有机卤化化合物或其制备具有卤素原子的（甲基）丙烯酸聚合物的方法制备具有高官能度比的链末端具有烯基或可固化甲硅烷基的（甲基）丙烯酸聚合物卤代磺酰基化合物作为引发剂和金属配合物催化剂，其中中心金属原子选自周期表第8,9,10和11族的元素; 和（ii）将卤素原子转化为烯基或含可固化的含甲硅烷基的取代基。所得的（甲基）丙烯酸聚合物形成均匀的固化材料。

16. 发明授权

US08030427B2 Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：US08030427B2
公开(公告)日：2011-10-04
申请号：US11628893
申请日：2005-05-26
申请人： Katsuyu Wakabayashi , Masato Kusakabe
发明人： Katsuyu Wakabayashi , Masato Kusakabe
IPC分类号： C08G77/06
CPC分类号： C08L101/10 , C08G65/336 , C08K5/098 , C08K5/541 , C08L71/02 , C09D143/04 , C08L83/04 , C08L43/04
摘要： Provision of a curable composition having good curability and adhesiveness by the use of a non-organotin catalyst.A curable composition containing an organic polymer (A) having a silicon-containing group crosslinkable by forming a siloxane bond, metal carboxylate (B), a silane coupling agent (C) free of an amino group, and an amino group-containing compound (D) in an amount corresponding to a weight ratio relative to (B) of 0-0.05, which contains, as the silicon-containing group of component (A), a silicon-containing group, wherein three hydrolyzable groups or hydroxyl groups are bonded to a silicon atom, as an essential component.
摘要翻译：提供通过使用非有机锡催化剂具有良好固化性和粘合性的可固化组合物。含有具有通过形成硅氧烷键可交联的含硅基团的有机聚合物（A）的可固化组合物，金属羧酸盐（B），不含氨基的硅烷偶联剂（C）和含氨基化合物（ D）相当于相对于（B）为0〜0.05的重量比，其含有作为组分（A）的含硅基团的含硅基团，其中三个可水解基团或羟基键合作为必须成分的硅原子。

17. 发明授权

US07763673B2 Curable composition containing a silicon-containing group polymer, a titanium chelate and an amide wax 有权
标题翻译：包含含硅基聚合物，钛螯合物和酰胺蜡的可固化组合物
公开(公告)号：US07763673B2
公开(公告)日：2010-07-27
申请号：US11579405
申请日：2005-04-25
申请人： Toshihiko Okamoto , Masato Kusakabe
发明人： Toshihiko Okamoto , Masato Kusakabe
IPC分类号： B60C1/00 , C08K5/36 , C08K5/48 , C08L91/06
CPC分类号： C08G65/336 , C08K3/014 , C08K5/0091 , C08K5/544 , C09D171/02 , C09J171/02 , C09K3/10 , C08L101/10 , C08L71/02
摘要： [Problem] There is provided a curable composition having high thixotropy and satisfactory curability by use of a non-organotin catalyst.[Means to Solve] A curable composition comprising (A) a polyoxyalkylene polymer having a silicon-containing group being capable of crosslinking by forming siloxane bonds and/or a (meth)acrylate polymer having a silicon-containing group being capable of crosslinking by forming siloxane bonds, (B) a titanium chelate, and (C) an amide wax type thixotropy-imparting agent.
摘要翻译： [问题]提供了通过使用非有机锡催化剂具有高触变性和令人满意的固化性的可固化组合物。 [解决方案]一种可固化组合物，其包含（A）具有能够通过形成硅氧烷键交联的含硅基团的聚氧化烯聚合物和/或具有含硅基团的（甲基）丙烯酸酯聚合物，其可以通过形成硅氧烷键，（B）钛螯合物和（C）酰胺蜡型触变性赋予剂。

18. 发明申请

US20080051547A1 Curable Composition 有权
标题翻译：可固化成分
公开(公告)号：US20080051547A1
公开(公告)日：2008-02-28
申请号：US11628893
申请日：2005-05-26
申请人： Katsuyu Wakabayashi , Masato Kusakabe
发明人： Katsuyu Wakabayashi , Masato Kusakabe
IPC分类号： C08G77/08
CPC分类号： C08L101/10 , C08G65/336 , C08K5/098 , C08K5/541 , C08L71/02 , C09D143/04 , C08L83/04 , C08L43/04
摘要： [Problem] Provision of a curable composition having good curability and adhesiveness by the use of a non-organotin catalyst. [Solving means] A curable composition containing an organic polymer (A) having a silicon-containing group crosslinkable by forming a siloxane bond, metal carboxylate (B), a silane coupling agent (C) free of an amino group, and an amino group-containing compound (D) in an amount corresponding to a weight ratio relative to (B) of 0-0.05, which contains, as the silicon-containing group of component (A), a silicon-containing group, wherein three hydrolyzable groups or hydroxyl groups are bonded to a silicon atom, as an essential component.
摘要翻译： [问题]通过使用非有机锡催化剂提供具有良好固化性和粘合性的可固化组合物。 [解决方案]含有通过形成硅氧烷键可交联的含硅基团的有机聚合物（A）的可固化组合物，金属羧酸盐（B），不含氨基的硅烷偶联剂（C）和氨基（D），其含量相对于（B）为0〜0.05的重量比，其含有作为组分（A）的含硅基团的含硅基团，其中三个可水解基团或羟基作为必需成分键合到硅原子上。

19. 发明申请

US20070208108A1 Single-Component Curable Composition 审中-公开
标题翻译：单组分可固化组合物
公开(公告)号：US20070208108A1
公开(公告)日：2007-09-06
申请号：US11547026
申请日：2005-03-18
申请人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
发明人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
IPC分类号： C08K3/26 , C08K9/00
CPC分类号： C08K5/09 , C08L71/02
摘要： The present invention has its object to provide a one package curable composition which contains an organotin-free catalyst and therefore has good curability and adhesiveness. The present invention provides a one package curable composition which comprises (A) an organic polymer having a silicon-containing group capable of crosslinking by forming a siloxane bond, (B)(b1) a carboxylic acid of which the carbon atom adjacent to a carbonyl group is a quaternary carbon, and/or (b2) a metal carboxylate of which the carbon atom adjacent to a carbonyl group is a quaternary carbon, and (C) a surface-treated ground calcium carbonate.
摘要翻译：本发明的目的是提供一种含有机锡催化剂的一包装固化组合物，因此具有良好的固化性和粘合性。本发明提供一种包装可固化组合物，其包含（A）具有能够通过形成硅氧烷键交联的含硅基团的有机聚合物，（B）（b1）与羰基相邻的碳原子的羧酸和/或（b2）与羰基相邻的碳原子为季碳的金属羧酸盐，和（C）表面处理的研磨碳酸钙。

20. 发明授权

US06737482B1 Curable resin composition 失效
标题翻译：可固化树脂组合物
公开(公告)号：US06737482B1
公开(公告)日：2004-05-18
申请号：US09889587
申请日：2001-11-20
申请人： Katsuhiro Ando , Toru Inaya , Masato Kusakabe , Hiroshi Iwakiri
发明人： Katsuhiro Ando , Toru Inaya , Masato Kusakabe , Hiroshi Iwakiri
IPC分类号： C08L8312
CPC分类号： C08L71/02 , C08G65/336 , C08L63/00 , C08L71/00
摘要： The present invention is to provide a curable resin composition comprising (I) a reactive silicon group-containing polyoxyalkylene polymer wherein a introduction rate of a reactive silicon group into molecular chain terminus is not less than 85% as analyzed by 1H-NMR spectrometry and (II) an epoxy resin. The curable resin obtained from this composition reflects improvements in tensile strength and tensile shear bond strength and in adhesion to various substrates.
摘要翻译：本发明提供一种固化性树脂组合物，其包含（I）含有反应性硅基的聚氧化烯聚合物，其中通过1 H-NMR分析，反应性硅基团在分子链末端的引入速率不低于85％光谱测定法和（II）环氧树脂。由该组合物获得的可固化树脂反映了拉伸强度和拉伸剪切粘合强度以及对各种基材的粘附性的改善。

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