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11. 发明授权

US08049027B2 Organosilicon compound having amino group and its production method 有权
标题翻译：具有氨基的有机硅化合物及其制备方法
公开(公告)号：US08049027B2
公开(公告)日：2011-11-01
申请号：US12582026
申请日：2009-10-20
申请人： Takayuki Honma , Tohru Kubota , Ayumu Kiyomori
发明人： Takayuki Honma , Tohru Kubota , Ayumu Kiyomori
IPC分类号： C07F7/04 , C07F7/07 , C07F7/08
CPC分类号： C07F7/1804
摘要： An organosilicon compound having an amino group is provided. This compound is represented by the following general formula (1): wherein R1 and R2 respectively represent an unsubstituted or substituted aliphatic monovalent hydrocarbon group containing 1 to 10 carbon atoms with the proviso that the R1 and R2 may together form a ring with the nitrogen atom to which they are bonded, and that R1 and R2 may contain a heteroatom; R3 and R4 independently represent an unsubstituted or substituted monovalent hydrocarbon group containing 1 to 10 carbon atoms; and n represents an integer of 0 to 2. Use of this compound enables production of a polymer product having excellent mechanical properties, high heat resistance, and high transparency. The solution of this compound is stable, and can be stored for a long time, and when used for a polymer modifying agent, it facilitates introduction of amino group and hydroxy group.
摘要翻译：提供具有氨基的有机硅化合物。该化合物由以下通式（1）表示：其中R 1和R 2分别表示含有1至10个碳原子的未取代或取代的脂族一价烃基，条件是R 1和R 2可以与氮原子一起形成环它们与它们键合，并且R 1和R 2可以含有杂原子; R3和R4独立地表示含有1至10个碳原子的未取代或取代的一价烃基; n表示0〜2的整数。该化合物的使用能够制造具有优异的机械性能，高耐热性和高透明性的聚合物制品。该化合物的溶液是稳定的，可以长时间储存，当用于聚合物改性剂时，有利于氨基和羟基的引入。

12. 发明授权

US07307178B2 Processes of making γ,δ-unsaturated carboxylic acid and silyl ester thereof, carboxyl group-containing organosilicon compound and process of making 有权
标题翻译：制备γ，δ-不饱和羧酸及其甲硅烷基酯的方法，含羧基的有机硅化合物及其制备方法
公开(公告)号：US07307178B2
公开(公告)日：2007-12-11
申请号：US10947129
申请日：2004-09-23
申请人： Ayumu Kiyomori , Tohru Kubota
发明人： Ayumu Kiyomori , Tohru Kubota
IPC分类号： C07F7/08
CPC分类号： C07F7/1896 , C07F7/081
摘要： A γ,δ-unsaturated carboxylic acid silyl ester is prepared by reacting an α,β-unsaturated carboxylic acid ester with a hydrosilane or hydrosiloxane in the presence of tris(pentafluorophenyl)borane. γ,δ-Unsaturated carboxylic acid derivatives are readily prepared through fewer steps and in high yields.
摘要翻译：在三（五氟苯基）硼烷的存在下，使α，β-不饱和羧酸酯与氢硅烷或氢硅氧烷反应制备γ，δ-不饱和羧酸甲硅烷基酯。 γ，δ-不饱和羧酸衍生物通过较少的步骤和高产率容易地制备。

13. 发明申请

US20050070729A1 Processes of making gamma,delta-unsaturated carboxylic acid and silyl ester thereof, carboxyl group-containing organosilicon compound and process of making 有权
标题翻译：制备γ，δ-不饱和羧酸及其甲硅烷基酯的方法，含羧基的有机硅化合物及其制备方法
公开(公告)号：US20050070729A1
公开(公告)日：2005-03-31
申请号：US10947129
申请日：2004-09-23
申请人： Ayumu Kiyomori , Tohru Kubota
发明人： Ayumu Kiyomori , Tohru Kubota
IPC分类号： C07C51/09 , C07C57/03 , C07F7/08 , C07F7/18
CPC分类号： C07F7/1896 , C07F7/081
摘要： A γ,δ-unsaturated carboxylic acid silyl ester is prepared by reacting an α,β-unsaturated carboxylic acid ester with a hydrosilane or hydrosiloxane in the presence of tris(pentafluorophenyl)borane. γ,δ-Unsaturated carboxylic acid derivatives are readily prepared through fewer steps and in high yields.
摘要翻译：在三（五氟苯基）硼烷的存在下，使α，β-不饱和羧酸酯与氢硅烷或氢硅氧烷反应制备γ，δ-不饱和羧酸甲硅烷基酯。 γ，δ-不饱和羧酸衍生物通过较少的步骤和高产率容易地制备。

14. 发明申请

US20110160464A1 SURFACE TREATMENT METHOD FOR SOLID MATERIAL 有权
标题翻译：固体表面处理方法
公开(公告)号：US20110160464A1
公开(公告)日：2011-06-30
申请号：US12975931
申请日：2010-12-22
申请人： Ayumu Kiyomori , Yusuke Itoh , Tohru Kubota
发明人： Ayumu Kiyomori , Yusuke Itoh , Tohru Kubota
IPC分类号： C07F7/28 , C07F7/08
CPC分类号： H01L21/306 , C09D4/00
摘要： A solid material is subjected to surface treatment by chemically bonding onto a surface of the solid material a stabilized monofunctional silanol represented by R1R2R3SiOH. R1, R2 and R3 may be the same or different, and each represent a substituent group independently selected from a substituted or unsubstituted, monovalent hydrocarbon group having from 1 to 40 carbon atoms or a substituted or unsubstituted, monovalent heterocyclic group having from 1 to 100 carbon atoms. The monofunctional silanol has a dehydrative self-condensation rate lower than triethylsilanol.
摘要翻译：通过在固体材料的表面上化学键合由R1R2R3SiOH表示的稳定的单官能硅烷醇，对固体材料进行表面处理。 R 1，R 2和R 3可以相同或不同，各自表示独立地选自具有1至40个碳原子的取代或未取代的一价烃基或具有1至100个取代或未取代的1价杂环基的取代基碳原子。单官能硅烷醇具有低于三乙基硅烷醇的脱水自缩缩速率。

15. 发明授权

US07576231B2 Method for producing isocyanate group-containing siloxane compound 有权
标题翻译：含异氰酸酯基的硅氧烷化合物的制造方法
公开(公告)号：US07576231B2
公开(公告)日：2009-08-18
申请号：US11882335
申请日：2007-08-01
申请人： Takanobu Tsudera , Tohru Kubota , Ayumu Kiyomori
发明人： Takanobu Tsudera , Tohru Kubota , Ayumu Kiyomori
IPC分类号： C07F7/10
CPC分类号： C07F7/0889
摘要： A method for producing an isocyanate group-containing siloxane compound is provided. In this method, a halogenated siloxane compound represented by the following general formula (1): or the following general formula (2) wherein R1, R2, R3, and R4 are independently hydrogen atom, a monovalent hydrocarbon group containing 1 to 8 carbon atoms, or a siloxy group represented by OSiR5R6R7 wherein R8, R6, and R7 are a monovalent hydrocarbon group containing 1 to 8 carbon atoms, X is a halogen atom, n is an integer of 1 to 10, a is 0, 1, or 2, and b is an integer of 2 to 9; is reacted with a cyanate salt represented by the following general formula (3): Mm+(OCN)m (3) wherein M represents an alkali metal or an alkaline earth metal, and m is 1 or 2. The isocyanate group-containing siloxane compound produced is represented by the following general formula (4): or the following general formula (5): wherein R1, R2, R3, R4, n, q, and a are as defined above.
摘要翻译：提供含异氰酸酯基的硅氧烷化合物的制造方法。在该方法中，由以下通式（1）表示的卤代硅氧烷化合物或其中R 1，R 2，R 3和R 4独立地为氢原子，含有1至8个碳原子的一价烃基的通式（2）或由OSiR 5 R 6 R 7表示的甲硅烷氧基，其中R 8，R 6和R 7为含有1至8个碳原子的一价烃基，X为卤素原子，n为1至10的整数，a为0,1或2 ，b为2〜9的整数。与由以下通式（3）表示的氰酸盐反应：<？in-line-formula description =“In-line formula”end =“lead”？> Mm +（OCN）m（3） line-formula description =“In-line Formulas”end =“tail”？>其中M表示碱金属或碱土金属，m为1或2.含异氰酸酯基的硅氧烷化合物由以下通式（4）：或以下通式（5）：其中R1，R2，R3，R4，n，q和a如上定义。

16. 发明申请

US20050256329A1 Preparation of silyl ketene acetal and disilyl ketene acetal 有权
公开(公告)号：US20050256329A1
公开(公告)日：2005-11-17
申请号：US11186845
申请日：2005-07-22
申请人： Ayumu Kiyomori , Tohru Kubota
发明人： Ayumu Kiyomori , Tohru Kubota
IPC分类号： C07F7/18 , C07F7/04
CPC分类号： C07F7/188
摘要： By reacting α,β-unsaturated carboxylic esters with hydrosilanes or hydrosiloxanes in the presence of a catalytic amount of tris(pentafluorophenyl)borane, silyl ketene acetals or disilyl ketene acetals with high purity are produced in high yields.

17. 发明授权

US06291696B1 Preparation of tris (trimethylsilyl) silylethyl esters 有权
公开(公告)号：US06291696B1
公开(公告)日：2001-09-18
申请号：US09754320
申请日：2001-01-05
申请人： Takeshi Kinsho , Koji Hasegawa , Takeru Watanabe , Tohru Kubota , Ayumu Kiyomori
发明人： Takeshi Kinsho , Koji Hasegawa , Takeru Watanabe , Tohru Kubota , Ayumu Kiyomori
IPC分类号： C07F708
摘要： An industrially acceptable process for preparing 2-[tris(trimethylsilyl)silyl]ethyl (meth)acrylate in high yields involves reacting 2-[tris(trimethylsilyl)silyl]ethyl acetate with an alcohol in the presence of a catalyst to form 2-[tris(trimethylsilyl)silyl]ethanol, then reacting it with a (meth)acrylate ester.

18. 发明授权

US06337415B1 Process for preparing tetrakis (trimethylsily) silane and tris (trimethysilyl) silane 有权
标题翻译：制备四（三甲基甲硅烷基）硅烷和三（三甲基甲硅烷基）硅烷的方法
公开(公告)号：US06337415B1
公开(公告)日：2002-01-08
申请号：US09704557
申请日：2000-11-03
申请人： Ayumu Kiyomori , Tohru Kubota , Takeshi Kinsho , Koji Hasegawa , Takeru Watanabe
发明人： Ayumu Kiyomori , Tohru Kubota , Takeshi Kinsho , Koji Hasegawa , Takeru Watanabe
IPC分类号： C07F704
CPC分类号： C07F7/0803
摘要： Tetrakis(trimethylsilyl)silane is prepared by reacting tetrachlorosilane with chlorotrimethylsilane in the presence of lithium metal, adding a compound with active proton(s) to the reaction mixture for treating the residual lithium metal therewith while maintaining the mixture neutral or acidic, and separating tetrakis(trimethylsilyl)silane from the organic layer. The residual lithium metal is treated in a safe and simple manner. Reaction of the tetrakis(trimethylsilyl)silane with an alkyl lithium or alkali metal alkoxide, followed by acid hydrolysis, affords tris(trimethylsilyl)silane. The desired compounds are prepared in high yields and on an industrial scale.
摘要翻译：通过四氯硅烷与氯代三甲基硅烷在锂金属的存在下反应制备四（三甲基甲硅烷基）硅烷，在反应混合物中加入具有活性质子的化合物，用于处理残留的锂金属同时保持混合物中性或酸性，并分离四（三甲基甲硅烷基）硅烷。剩余的锂金属以安全和简单的方式进行处理。四（三甲基甲硅烷基）硅烷与烷基锂或碱金属醇盐的反应，然后进行酸水解，得到三（三甲基甲硅烷基）硅烷。所需化合物以高产率和工业规模制备。

19. 发明授权

US08541631B2 Surface treatment method for solid material 有权
标题翻译：固体材料的表面处理方法
公开(公告)号：US08541631B2
公开(公告)日：2013-09-24
申请号：US12975931
申请日：2010-12-22
申请人： Ayumu Kiyomori , Yusuke Itoh , Tohru Kubota
发明人： Ayumu Kiyomori , Yusuke Itoh , Tohru Kubota
IPC分类号： C07C41/09
CPC分类号： H01L21/306 , C09D4/00
摘要： A solid material is subjected to surface treatment by chemically bonding onto a surface of the solid material a stabilized monofunctional silanol represented by R1R2R3SiOH. R1, R2 and R3 may be the same or different, and each represent a substituent group independently selected from a substituted or unsubstituted, monovalent hydrocarbon group having from 1 to 40 carbon atoms or a substituted or unsubstituted, monovalent heterocyclic group having from 1 to 100 carbon atoms. The monofunctional silanol has a dehydrative self-condensation rate lower than triethylsilanol.
摘要翻译：通过在固体材料的表面上化学键合由R1R2R3SiOH表示的稳定的单官能硅烷醇，对固体材料进行表面处理。 R 1，R 2和R 3可以相同或不同，各自表示独立地选自具有1至40个碳原子的取代或未取代的一价烃基或具有1至100个取代或未取代的1价杂环基的取代基碳原子。单官能硅烷醇具有低于三乙基硅烷醇的脱水自缩缩速率。

20. 发明授权

US06960679B2 Preparation of silyl ketene acetal and disilyl ketene acetal 有权
标题翻译：制备甲硅烷基乙烯酮乙缩醛和二甲硅烷基乙烯酮缩醛
公开(公告)号：US06960679B2
公开(公告)日：2005-11-01
申请号：US10829193
申请日：2004-04-22
申请人： Ayumu Kiyomori , Tohru Kubota
发明人： Ayumu Kiyomori , Tohru Kubota
IPC分类号： C07F7/18
CPC分类号： C07F7/188
摘要： By reacting α,β-unsaturated carboxylic esters with hydrosilanes or hydrosiloxanes in the presence of a catalytic amount of tris(pentafluorophenyl)borane, silyl ketene acetals or disilyl ketene acetals with high purity are produced in high yields.
摘要翻译：通过使α，β-不饱和羧酸酯与氢硅烷或氢硅氧烷在催化量的三（五氟苯基）硼烷存在下反应，以高产率生产出高纯度的甲硅烷基乙烯酮缩醛或二甲硅烷基乙烯酮缩醛。

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