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11. 发明授权

US07125922B2 Alkoxysilane dryer for crosslinkable polymer compounds 有权
标题翻译：用于可交联聚合物化合物的烷氧基硅烷干燥器
公开(公告)号：US07125922B2
公开(公告)日：2006-10-24
申请号：US10649722
申请日：2003-08-28
申请人： Dieter Barfurth , Helmut Mack
发明人： Dieter Barfurth , Helmut Mack
IPC分类号： B60C1/00
CPC分类号： C08G77/18 , C08K5/54 , C08K5/5419
摘要： A composition containing an alkoxysiloxane including a catenate alkoxysilane of formula I and/or a cyclic siloxane of formula II, and a crosslinkable polymer compound and the use thereof as a water scavenger, dryer or precuring retarder R3Si—O—[SiR2—O—]mSiR3 (I)
摘要翻译：含有式I的链状烷氧基硅烷和/或式II的环状硅氧烷的烷氧基硅氧烷和交联性高分子化合物的组合物及其作为除水剂，干燥剂或预固化缓凝剂的用途< 在线公式“end =”lead“？> R 3 Si-O- [SiR 2 -O - ] m SiR _{3 （I）<？in-line-formula description =“In-line Formulas”end =“tail”？>}

12. 发明授权

US06784272B2 Metal-free silane-terminated polyurethanes, a process for their preparation and their use 有权
标题翻译：无金属硅烷封端的聚氨酯，其制备方法及其用途
公开(公告)号：US06784272B2
公开(公告)日：2004-08-31
申请号：US10108502
申请日：2002-03-29
申请人： Helmut Mack , Dieter Barfurth
发明人： Helmut Mack , Dieter Barfurth
IPC分类号： C08G7726
CPC分类号： C09K3/1021 , C08G18/10 , C09J175/04 , C08G18/289
摘要： A metal-free, in particular tin-free, silane-terminated polyurethane which is useful in adhesives or sealant compositions is obtained by reacting at least one aliphatic secondary aminoalkylalkoxysilane of formula (Ia) R—NH—(CH2)3Si(R1)x(OR2)(3-X) (Ia) or at least one aliphatic secondary aminoalkylalkoxysilane of formula (Ib) R—NH—CH2—CH(R1)—CH2—Si(R1)x(OR2)(3-X) (Ib) wherein in the formulae (Ia) and (Ib), R is a linear or branched alkyl group having 1 to 18 C atoms, R1 is a methyl group, R2 is a methyl or ethyl group and x is 0 or 1, with a polyurethane prepolymer having at least one terminal isocyanate group in the absence of a metal catalyst.
摘要翻译：通过使至少一种式（Ia）的脂肪族仲氨基烷基烷氧基硅烷或至少一种式（Ib）的脂族仲氨基烷基烷氧基硅烷与式（Ia）的脂族仲氨基烷基烷氧基硅烷反应，得到不含金属的，特别是无锡的硅烷封端的聚氨酯，其中在式（Ia）和（Ib）中，R是具有1至18个C原子的直链或支链烷基，R 1是甲基，R 2是甲基或乙基，x是0 或1，在不存在金属催化剂的情况下，聚氨酯预聚物具有至少一个末端异氰酸酯基团。

13. 发明授权

US06780955B2 Mixture of catenate and cyclic siloxane oligomers, its preparation and use 失效
标题翻译：联苯胺和环状硅氧烷低聚物的混合物，其制备和用途
公开(公告)号：US06780955B2
公开(公告)日：2004-08-24
申请号：US10348959
申请日：2003-01-23
申请人： Dieter Barfurth , Helmut Mack
发明人： Dieter Barfurth , Helmut Mack
IPC分类号： C08G7708
CPC分类号： C08G77/20 , C08G77/045 , C08G77/06 , C09D183/04
摘要： The present invention provides a process for preparing a mixture, which mixture includes catenate and cyclic siloxanes of formula I R3Si—O—(SiR2—O—)mSiR3 (I) and cyclic siloxanes of formula II wherein m is an integer from 0 to 40 and n is an integer from 2 to 40, wherein R2 and R3 are each independently an organic functional group selected from the group including alkyl, aryl, vinyl, and alkoxy groups, and wherein there is not more than one vinyl group or aryl group per silicon atom, said process including a controlled hydrolysis, condensation or cocondensation reaction of at least one monomeric silane in alcoholic solution in the presence of an acidic catalyst, which reaction includes contacting alcohol, water, and at least one chlorosilane component selected from the group including (i), (ii), (iii): (i) at least one arylchlorosilane; (ii) at least one admixture selected from the group including alkylchlorosilane and arylchlorosilane, arylchlorosilane and vinylchlorosilane, alkylchlorosilane and vinylchlorosilane, and arylchlorosilane and vinylchlorosilane and alkylchlorosilane; (iii) at least one selected from the group including chlorosilane, alkylchlorosilane, arylchlorosilane, and vinylchlorosilane in two or more separate batches to obtain two or more separate mixtures and thereafter combining the mixtures; to form the mixture of the catenate and cyclic siloxanes. The present invention also provides the mixtures and the use of such mixtures.
摘要翻译：本发明提供一种制备混合物的方法，该混合物包括式I的链环和环状硅氧烷和式II的环状硅氧烷，其中m为0至40的整数，n为2至40的整数，其中R 2和R 3各自为独立地是选自包括烷基，芳基，乙烯基和烷氧基的有机官能团，并且其中每个硅原子不超过一个乙烯基或芳基，所述方法包括受控的水解，缩合或共缩聚反应在酸性催化剂存在下，醇溶液中的至少一种单体硅烷，该反应包括使醇，水和至少一种选自（i），（ii），（iii）：（i）中的氯硅烷组分与至少一种芳基氯硅烷;（ii）至少一种选自烷基氯硅烷和芳基氯硅烷，芳基氯硅烷和乙烯基氯硅烷，烷基氯硅烷和乙烯基氯硅烷的混合物， nd芳基氯硅烷和乙烯基氯硅烷和烷基氯硅烷;（iii）选自包括氯硅烷，烷基氯硅烷，芳基氯硅烷和乙烯基氯硅烷的组中的至少一种，分两批以上分批，以获得两种或更多种分离的混合物，然后混合该混合物; 链状和环状硅氧烷。本发明还提供了这些混合物的混合物和用途。

14. 发明授权

US07939616B2 Organofunctional siloxane mixtures 有权
标题翻译：有机官能硅氧烷混合物
公开(公告)号：US07939616B2
公开(公告)日：2011-05-10
申请号：US10555984
申请日：2004-03-18
申请人： Dieter Barfurth , Helmut Mack
发明人： Dieter Barfurth , Helmut Mack
IPC分类号： C08G77/22
CPC分类号： C08G77/26 , C07F7/21 , C08G77/04
摘要： The present Invention relates to a mixture comprising catenary, branched and for cyclic siloxanes of the general formula (I) where x is 1, 2 or 3, the substituents R are (i) organofunctional groups selected from —CH2—SH, —CH2—S—(CO)—R′, —CH2—(O—C2H4)a—OH with a=1 to 10, —CH2(O—C2H4)b—OR′ with b=1 to 40, —(CH2)—NH2, —(CH2)—NHR′, —(CH2)—NR′2, —(CH2)—NH(CH2)2—NH2, —(CH2)—N[(CH2)2—NH2]2 and —(CH2)—NH(CH2)2—NH(CH2)2—NH2, In which R′ is a linear, branched or cyclic alkyl group having 1 to 18 carbon atoms or an aryl group having 6 to 12 carbon atoms, (ii) hydroxyl, methoxy, ethoxy, 2-methoxyethoxy, isopropoxy, n-propoxy, isobutoxy and for n-butoxy groupe, and (iii) where appropriate, alkyl, alkenyl, isoalkyl, cycloalkyl or fluorcalkyl groups having 1 to 18 carbon atoms or aryl groups having 6 to 12 carbon atoms, whit the proviso that not more than one organofunctional group (i) is attached per silicon atom, the quotient of the molar ratio of the moiety (ii) to silicon le from I to 2, and the degree of oligornerization for compounds of the general formula I is in the range from 2 to 50. The present invention also relates to a specific process for preparing said siloxane mixtures and also to their use.
摘要翻译：本发明涉及包含通式（I）的链状，支链和环状硅氧烷的混合物，其中x为1,2或3，取代基R为（i）选自-CH 2 -SH，-CH 2 - 具有a = 1-10的S-（CO）-R'，-CH 2 - （O-C 2 H 4）a -OH，b = 1至40的-CH 2（O-C 2 H 4）b-OR'， - （CH 2） NH 2， - （CH 2）-NHR'， - （CH 2）-NR'2， - （CH 2）-NH（CH 2）2 -NH 2， - （CH 2）-N [（CH 2）2 -NH 2] 2和 - CH 2）-NH（CH 2）2 -NH（CH 2）2 -NH 2，其中R'是具有1至18个碳原子的直链，支链或环状烷基或具有6至12个碳原子的芳基，（ii）羟基，甲氧基，乙氧基，2-甲氧基乙氧基，异丙氧基，正丙氧基，异丁氧基和正丁氧基，和（iii）适当的是具有1至18个碳原子的烷基，烯基，异烷基，环烷基或氟烷基或芳基具有6至12个碳原子，条件是每个硅原子连接不超过一个有机官能团（i），其中th （ii）与硅的摩尔比为1至2，并且通式I化合物的低聚化程度在2至50的范围内。本发明还涉及制备所述硅氧烷混合物以及它们的用途。

15. 发明申请

US20070032622A1 Organofunctional siloxane mixtures 有权
标题翻译：有机官能硅氧烷混合物
公开(公告)号：US20070032622A1
公开(公告)日：2007-02-08
申请号：US10555984
申请日：2004-03-18
申请人： Dieter Barfurth , Helmut Mack
发明人： Dieter Barfurth , Helmut Mack
IPC分类号： C08G77/04
CPC分类号： C08G77/26 , C07F7/21 , C08G77/04
摘要： The present Invention relates to a mixture comprising catenary, branched andfor cyclic siloxanes of the general formula (I) where x is 1, 2 or 3, the substituents R are (i) organofunctional groups selected from —CH2—SH, —CH2—S—(CO)—R′, —CH2(O—C2H4)a—OH with a =1 to 10, —CH2(O—C2H4)b—OR′ with b =1 to 40, —(CH2)—NH2, —(CH2)—NHR′, —(CH2)—NR′2, —(CH2)—NH(CH2)2—NH2, —(CH2)—N[(CH2)2—NH2]2 and —(CH2) —NH(CH2)2—NH(CH2)2—NH2, In which R′ is a linear, branched or cyclic alkyl group having 1 to 18 carbon atoms or an aryl group having 6 to 12 carbon atoms, (ii) hydroxyl, methoxy, ethoxy, 2-methoxyethoxy, isopropoxy, n-propoxy, isobutoxy andfor n-butoxy groupe, and (iii) where appropriate, alkyl, alkenyl, isoalkyl, cycloalkyl or fluorcalkyl groups having 1 to 18 carbon atoms or aryl groups having 6 to 12 carbon atoms, whit the proviso that not more than one organofunctional group (i) is attached per silicon atom, the quotient of the molar ratio of the moiety (ii) to silicon le from I to 2, and the degree of oligornerization for compounds of the general formula I is in the range from 2 to 50. The present invention also relates to a specific process for preparing said siloxane mixtures and also to their use.
摘要翻译：本发明涉及包含通式（I）的链状，支链和环状硅氧烷的混合物，其中x为1,2或3，取代基R为（i）选自-CH 2的有机官能团 > -SH，-CH 2 -S-（CO）-R'，-CH 2（OC 2 H 4）其中a = 1至10，-CH 2（OC 2 H 4））b = 1至40， - （CH 2）2 NH 2 - ， - （CH 2）） - NHR'， - （CH 2） - NR'2， - （CH 2） - NH（CH

16. 发明授权

US06444315B1 Surface-modified flame retardants containing an organic silicon composition, their use, and process for their preparation 有权
标题翻译：表面改性阻燃剂，其用途及其制备方法
公开(公告)号：US06444315B1
公开(公告)日：2002-09-03
申请号：US09347534
申请日：1999-07-06
申请人： Dieter Barfurth , Helmut Mack , Karl Goetzmann , Vincente Mans , Hans-Dieter Naegerl , Klaus Sommer
发明人： Dieter Barfurth , Helmut Mack , Karl Goetzmann , Vincente Mans , Hans-Dieter Naegerl , Klaus Sommer
IPC分类号： B32B516
CPC分类号： C08K9/06 , C09K21/00 , Y10S428/92 , Y10T428/2991 , Y10T428/2998
摘要： An encapsulated flame retardant is made by a process including applying an organic silicon composition to a powder flame retardant. The organic silicon composition is an organofunctional-silane or a mixture of organofunctional silanes, an oligomeric organosiloxane or a mixture of oligomeric organosiloxanes, or a solvent-containing preparation based on monomeric organosilanes and/or on oligomeric organosiloxanes, or a preparation based on water-soluble organopolysiloxanes, or mixtures of any or all of these. These surface-modified flame retardants are used in particular in polymers and polymer compounds, for rendering naturally occurring materials flame retardant, and also for the intumescent coating of combustible materials.
摘要翻译：包封的阻燃剂通过包括将有机硅组合物施用于粉末阻燃剂的方法制备。有机硅组合物是有机官能硅烷或有机官能硅烷，低聚有机硅氧烷或低聚有机硅氧烷的混合物或基于单体有机硅烷和/或低聚有机硅氧烷的含溶剂的制剂的混合物，或基于水溶性有机硅烷的制剂，可溶性有机聚硅氧烷，或其中任何一种或全部的混合物。这些表面改性阻燃剂特别用于聚合物和聚合物化合物中，用于使天然存在的材料阻燃，也用于可燃材料的膨胀涂层。

17. 发明授权

US4931094A Titanium(IV)-chelates and their use in printing inks 失效
标题翻译：钛（IV） - 它们在印刷油墨中的应用
公开(公告)号：US4931094A
公开(公告)日：1990-06-05
申请号：US252700
申请日：1988-10-03
申请人： Dieter Barfurth , Claus Lindzus , Heinz Nestler
发明人： Dieter Barfurth , Claus Lindzus , Heinz Nestler
IPC分类号： C07F7/28 , C07F7/00 , C09D11/02 , C09D11/14
CPC分类号： C07F7/006 , C09D11/14
摘要： Novel alkoxy titanium(IV)-chelates are used to modify printing inks based on nitrocellulose or other cellulose ester derivatives. The novel chelates comprise citric acid alkyl esters as chelate formers. They delay, as other titanium chelates do, the well-known catalytic effect of the titanium component in cross-linking reactions. When used in printing inks, the novel titanium chelates and their alcoholic solutions have the advantage that they have an insignificant color of their own, so that they practically do not discolor the printing inks. A further advantage of the novel chelates resides in that they do not enter into alteration effects with antioxidants based on phenol, so that they can also be used for printing inks which are to be applied to polymeric substrates containing such antioxidants without the occurence of discoloration.
摘要翻译：新型烷氧基钛（IV） - 螯合物用于改性基于硝化纤维素或其它纤维素酯衍生物的印刷油墨。新型螯合物包括柠檬酸烷基酯作为螯合物。与其他钛螯合物一样，它们延迟钛组分在交联反应中的众所周知的催化作用。当用于印刷油墨时，新型钛螯合物及其醇溶液的优点在于它们本身具有无色的颜色，因此它们实际上不会使印刷油墨变色。新型螯合物的另一个优点在于它们不会以基于苯酚的抗氧化剂引起改变效果，因此它们也可以用于印刷油墨，这些油墨应用于含有这种抗氧化剂的聚合物基材上，而不发生变色。

18. 发明授权

US5021596A Zirconium chelates, their preparation, and their use in printing inks 失效
标题翻译：锆螯合物，它们的制备及其在印刷油墨中的应用
公开(公告)号：US5021596A
公开(公告)日：1991-06-04
申请号：US314816
申请日：1989-02-23
申请人： Dieter Barfurth , Claus Lindzus , Heinz Nestler
发明人： Dieter Barfurth , Claus Lindzus , Heinz Nestler
IPC分类号： C07C69/704 , C07F7/00 , C09D11/03 , C09K3/00
CPC分类号： C09D11/03 , C07F7/003
摘要： Zirconium(IV) chelates with citric acid ester radicals and optionally with alkoxy groups are prepared from tetraalkoxy zirconate and a citric acid ester; they are useful as components of printing inks.
摘要翻译：柠檬酸酯基和任选具有烷氧基的锆（IV）螯合物由四烷氧基锆酸酯和柠檬酸酯制备; 它们可用作印刷油墨的组分。

19. 发明授权

US4924016A Condensed acetoacetic acid ester titanium chelates and process for their preparation 失效
标题翻译：浓缩乙酰乙酸酯钛螯合物及其制备方法
公开(公告)号：US4924016A
公开(公告)日：1990-05-08
申请号：US268897
申请日：1988-11-08
申请人： Dieter Barfurth , Heinz Nestler
发明人： Dieter Barfurth , Heinz Nestler
IPC分类号： C08L83/04 , B01J31/22 , C07B61/00 , C07C51/41 , C07F7/00 , C07F7/28 , C08K5/05
CPC分类号： C07F7/006 , C07C51/418
摘要： Titanium chelates with 1 to 2 acetoacetic acid ester ligands and one to two alkoxy groups per titanium atom the sum of these ligands and the alkoxy groups being three as well as Ti-O-Ti bridge between two titanium atoms are formed by release of alcohol and condensation of mono- or bis-acetoacetic acid ester-Ti-(IV)-chelates which have up to 4 alkoxy groups per titanium atom.
摘要翻译：钛螯合物与1至2个乙酰乙酸酯配体和每个钛原子一至两个烷氧基，这些配体和烷氧基之和为三个以及两个钛原子之间的Ti-O-Ti桥的总和通过释放醇形成，每个钛原子具有最多4个烷氧基的单 - 或双 - 乙酰乙酸酯-Ti-（IV） - 螯合物的缩合。

20. 发明授权

US4909846A Compositions based on titanium chelates of diols and titanium acylates 失效
标题翻译：基于二醇和钛酰化物钛螯合物的组合物
公开(公告)号：US4909846A
公开(公告)日：1990-03-20
申请号：US264697
申请日：1988-10-31
申请人： Dieter Barfurth , Heinz Nestler
发明人： Dieter Barfurth , Heinz Nestler
IPC分类号： C08K5/00 , C09D11/03
CPC分类号： C09D11/03 , C08K5/0091
摘要： Titanium chelate - based compositions are used as additives for liquid or pasty coating agents, especially printing inks; they consist of a mixture of titanium chelates of saturated diols and titanium acylates of saturated monocarboxylic acids.
摘要翻译：钛螯合物组合物用作液体或糊状包衣剂，特别是印刷油墨的添加剂; 它们由饱和二醇的钛螯合物和饱和一元羧酸的酰化物钛的混合物组成。

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