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11. 发明授权

US5198579A Catalyst for oxidizing methacrolein and method for preparing methacrylic acid 失效
标题翻译：用于氧化异丁烯醛的催化剂和制备甲基丙烯酸的方法
公开(公告)号：US5198579A
公开(公告)日：1993-03-30
申请号：US789926
申请日：1991-11-12
申请人： Tadatoshi Honda , Nobuhiko Horiuchi , Jun Kitagawa , Masami Murakami , Kazunori Kawahara , Hirofumi Io
发明人： Tadatoshi Honda , Nobuhiko Horiuchi , Jun Kitagawa , Masami Murakami , Kazunori Kawahara , Hirofumi Io
IPC分类号： B01J27/199 , B01J27/24 , C07C51/25 , F16G5/16
CPC分类号： B01J23/002 , B01J27/199 , B01J27/24 , C07C51/252 , B01J2523/00
摘要： A composite oxide catalyst represented by the general formula: Mo-V-P-X-Y (wherein X represents at least one element selected from the group consisting of Sb, Cu, Co, Bi and As; Y represents at least one element selected from the group consisting of K, Rb, Cs and Tl) and a method for preparing methacrylic acid through gas phase catalytic oxidation of methacrolein with molecular oxygen in the presence of the foregoing catalyst are herein disclosed. The catalyst exhibits excellent catalytic activity, selectivity to methacrylic acid, catalytic stability and lifetime.
摘要翻译：由通式Mo-VPXY表示的复合氧化物催化剂（其中X表示选自Sb，Cu，Co，Bi和As中的至少一种元素; Y表示选自K ，Rb，Cs和Tl）以及在上述催化剂存在下通过气相催化氧化甲基丙烯醛与分子氧制备甲基丙烯酸的方法。该催化剂表现出优异的催化活性，对甲基丙烯酸的选择性，催化稳定性和寿命。

12. 发明授权

US4032572A Method for concentrating an acrylamide aqueous solution 失效
标题翻译：浓缩丙烯酰胺水溶液的方法
公开(公告)号：US4032572A
公开(公告)日：1977-06-28
申请号：US637416
申请日：1975-12-03
申请人： Shiro Asano , Kiyotaka Yoshimura , Ryoji Tsuchiya , Tadatoshi Honda
发明人： Shiro Asano , Kiyotaka Yoshimura , Ryoji Tsuchiya , Tadatoshi Honda
IPC分类号： C07C233/09 , C07C103/08
CPC分类号： C07C233/09 , Y10S159/10
摘要： A method for economically concentrating an acrylamide aqueous solution by catalytic hydration without substantial deterioration in the product. According to the method, an acrylamide aqueous solution obtained from catalytic hydration, is concentrated by distillation while maintaining the solution in good contact with at least 0.1 mole. or more of air per mole of water distilled from the acrylamide aqueous solution.

13. 发明授权

US5175308A Preparation process of indoles 失效
标题翻译：吲哚的制备方法
公开(公告)号：US5175308A
公开(公告)日：1992-12-29
申请号：US609641
申请日：1990-11-06
申请人： Tadatoshi Honda , Makoto Kotani
发明人： Tadatoshi Honda , Makoto Kotani
IPC分类号： C07D209/68 , B01J23/50 , B01J23/89 , C07B61/00 , C07D209/04
CPC分类号： B01J23/89 , B01J23/50 , C07D209/04
摘要： A process is provided for the preparation of an indole from aniline or a derivative thereof and a polyhydric alcohol. The reaction is carried out in the presence of a catalyst composed of a carrier having a specific surface area of at least 10 m.sup.2 /g and silver supported on the carrier. The catalyst also contains as an additional component a specific amount of at least one element selected from Co, Fe and Ni. Deterioration in catalytic performance of the catalyst during the reaction and its regeneration are therefore minimized.

14. 发明授权

US4345101A Process for purifying an aqueous solution of acrylamide 失效
标题翻译：纯化丙烯酰胺水溶液的方法
公开(公告)号：US4345101A
公开(公告)日：1982-08-17
申请号：US269602
申请日：1981-06-02
申请人： Shiro Asano , Kohei Shizuka , Yoshihiko Kambara , Junji Mikami , Hiroshi Kato , Tadatoshi Honda
发明人： Shiro Asano , Kohei Shizuka , Yoshihiko Kambara , Junji Mikami , Hiroshi Kato , Tadatoshi Honda
IPC分类号： C07C231/24 , B01J23/00 , C07C233/09 , C07C253/34 , C08F20/52 , C08F120/56 , C07C103/133
CPC分类号： C07C253/34 , C07C231/24
摘要： An aqueous solution of acrylamide obtained by catalytic hydration of acrylonitrile in the presence of a copper-based catalyst is purified by the steps, in sequence, of (a) removal of the unreacted acrylonitrile, (b) removal of copper, (c) treatment under basic conditions, (d) cation exchanging treatment and (e) weakly basic anion exchanging treatment. The acrylamide obtained by this process has good storage stability. An acrylamide polymer produced from this monomer is useful as a flocculant having a reduced content of the unreacted monomer, a high molecular weight and excellent solubility in water.
摘要翻译：通过在（a）去除未反应的丙烯腈，（b）去除铜，（c）处理（c）处理的步骤中，按照以下步骤来纯化在铜基催化剂存在下通过丙烯腈的催化水合获得的丙烯酰胺水溶液在碱性条件下，（d）阳离子交换处理和（e）弱碱性阴离子交换处理。通过该方法获得的丙烯酰胺具有良好的储存稳定性。由该单体制备的丙烯酰胺聚合物可用作具有降低的未反应单体含量，高分子量和优异的在水中的溶解度的絮凝剂。

15. 发明授权

US4668283A Magnetic powder and production process thereof 失效
标题翻译：磁粉及其制备方法
公开(公告)号：US4668283A
公开(公告)日：1987-05-26
申请号：US746884
申请日：1985-06-20
申请人： Tadatoshi Honda , Takeshi Tsuda
发明人： Tadatoshi Honda , Takeshi Tsuda
IPC分类号： H01F1/057 , C22C1/04
CPC分类号： H01F1/0572 , Y10T428/2991
摘要： Magnetic powder protected from subsequent oxidation and deterioration can be obtained by effecting contact of starting magnetic powder, which is formed of an intermetallic compound containing a rare-earth metal and an iron-group metal as principal components thereof, with a phosphorus compound containing at least one active proton having a pKa of 4 or smaller and exposure of the starting magnetic powder to an oxygen-containing atmosphere in an arbitrary order or simultaneously. Production of a plastic magnet with the magnetic powder of this invention allows to avoid danger and deterioration in magnetic characteristics of the resulting product due to oxidation of the magnetic powder even if exposed to elevated temperatures during its production or use.
摘要翻译：通过使包含稀土金属的金属间化合物和作为其主要成分的铁族金属形成的起始磁性粉末与至少含有磷化合物的磷化合物接触，可以获得保护免受后续氧化和劣化的磁性粉末一个pKa为4或更小的活性质子，并以起始磁性粉末以任意的顺序或同时暴露于含氧气氛。使用本发明的磁性粉末制造塑料磁体允许避免由于磁粉的氧化而导致的所得产品的磁特性的危险和劣化，即使在生产或使用过程中暴露于升高的温度下。

16. 发明授权

US4313001A Process for purifying aqueous acrylamide solutions 失效
标题翻译：净化丙烯酰胺水溶液的方法
公开(公告)号：US4313001A
公开(公告)日：1982-01-26
申请号：US186057
申请日：1980-09-11
申请人： Hiroshi Itoh , Tadatoshi Honda , Jun Saitoh , Takatoshi Mitsuishi
发明人： Hiroshi Itoh , Tadatoshi Honda , Jun Saitoh , Takatoshi Mitsuishi
IPC分类号： C07C20060101 , C08F8/12 , C08F120/56 , G01N11/00 , C07C103/133
CPC分类号： C07C1/00 , C08F120/56 , C08F8/12 , G01N11/00
摘要： A process for purifying an aqueous acrylamide solution which has been obtained through catalytic hydration of acrylonitrile in the presence of a copper-containing catalyst, by the steps of passing said solution through a OH-form strongly basic anion exchange resin layer and then, through a H-form cation exchange resin layer, is disclosed.
摘要翻译：一种纯化丙烯酰胺溶液的方法，其通过在含铜催化剂存在下通过丙烯腈的催化水合获得，通过使所述溶液通过OH-型强碱性阴离子交换树脂层，然后通过公开了H型阳离子交换树脂层。

17. 发明授权

US3962333A Process for the production of acrylamide and methacrylamide 失效
标题翻译：制备丙烯酰胺和甲基丙烯酰胺的方法
公开(公告)号：US3962333A
公开(公告)日：1976-06-08
申请号：US617973
申请日：1975-09-25
申请人： Kiyotaka Yoshimura , Shiro Asano , Tadatoshi Honda
发明人： Kiyotaka Yoshimura , Shiro Asano , Tadatoshi Honda
IPC分类号： C07C233/09 , C07C103/08
CPC分类号： C07C233/09
摘要： An improved process for preparing acrylamide or methacrylamide which process comprises the step of reacting acrylonitrile or methacrylonitrile with water in the presence of a catalyst system consisting of a metallic copper containing catalyst and a copper salt promoter, said copper salt being copper sulfate, copper nitrate, copper halide, or a copper salt of a lower fatty acid.
摘要翻译：一种制备丙烯酰胺或甲基丙烯酰胺的改进方法，该方法包括在由含金属铜催化剂和铜盐促进剂组成的催化剂体系存在下使丙烯腈或甲基丙烯腈与水反应的步骤，所述铜盐是硫酸铜，硝酸铜，卤化铜或低级脂肪酸的铜盐。

18. 发明授权

US3951600A Acrylamide aqueous solution handling method 失效
标题翻译：丙烯酰胺水溶液处理方法
公开(公告)号：US3951600A
公开(公告)日：1976-04-20
申请号：US311900
申请日：1972-12-04
申请人： Shiro Asano , Kiyotaka Yoshimura , Ryoji Tsuchiya , Tadatoshi Honda
发明人： Shiro Asano , Kiyotaka Yoshimura , Ryoji Tsuchiya , Tadatoshi Honda
IPC分类号： C07C231/22 , C07C67/00 , C07C231/00 , C07C231/06 , C07C233/09 , A61L13/00 , C07C103/08
CPC分类号： C07C233/09
摘要： There is disclosed a method for handling acrylamide aqueous solutions with safety wherein acrylamide aqueous solutions obtained through catalytic hydration reaction of acrylonitrile are handled using utensils made from phenol resin, polyethylene, polypropylene, polyvinylchloride resin or fluorine-containing resin or glass or using such utensils that are provided with linings formed by these materials.
摘要翻译：公开了一种安全处理丙烯酰胺水溶液的方法，其中通过丙烯腈的催化水合反应获得的丙烯酰胺水溶液是使用由酚醛树脂，聚乙烯，聚丙烯，聚氯乙烯树脂或含氟树脂或玻璃制成的器具处理的，或者使用这样的器具设置有由这些材料形成的衬里。

19. 发明授权

US5144090A Method for preparing acrolein or methacrolein 失效
标题翻译：制备丙烯酸或甲基纤维素的方法
公开(公告)号：US5144090A
公开(公告)日：1992-09-01
申请号：US711032
申请日：1991-06-06
申请人： Tadatoshi Honda , Tokio Nagayama , Nobuhiko Horiuchi , Jun Kitagawa , Kazunori Kawahara , Masami Murakami
发明人： Tadatoshi Honda , Tokio Nagayama , Nobuhiko Horiuchi , Jun Kitagawa , Kazunori Kawahara , Masami Murakami
IPC分类号： B01J23/88 , C07C45/35 , C07C45/37 , C07C45/39
CPC分类号： B01J23/887 , B01J23/002 , C07C45/35 , C07C45/37 , C07C45/39 , B01J2523/00
摘要： A method for preparing acrolein or methacrolein comprises subjecting propylene, secondary propanol, isobutylene or tertiary butanol to gas phase catalytic oxidation with molecular oxygen in the presence of a catalyst represented by the following general formula (I):Mo.sub.a Bi.sub.b Fe.sub.c X.sub.d Y.sub.O Z.sub.f O.sub.g (I)wherein X represents at least one element selected from the group consisting of Ni and Co; Y represents at least one element selected from the group consisting of K, Rb, Cs and Tl; and Z represents at least one element selected from the group consisting of Be, Mg, Ca, Sr, Ba, Ce, Ti, Zr, Nb, Cr, W, Mn, Cu, Ag, Zn, Cd, B, Al, Si, Ge, Sn, Pb, P, As, Sb, S, Se and Te; a, b, c, d, e, f and g each represents an atomic ratio of the corresponding element and when a is assumed to be 12, b=0.1.about.10, c=0.1.about.20, d=2.about.20, e=0.01.about.2, f=0.about.4 and g represents the number of oxygen atoms required for satisfying the valency requirement of the constituent elements, wherein the catalyst used is prepared by separately preparing solutions each of which contains the starting compound for the foregoing catalyst components, mixing these solutions within a short period of time, spray-drying the resulting mixture immediately after the mixing and then calcining the dried powder. A catalyst which further comprises 5 to 15% by weight of silica in addition to the foregoing composition is also used in the method. End products can be obtained in high conversion and selectivity through the use of the foregoing catalyst. Moreover, the catalyst is excellent in stability and has good reproducibility.

20. 发明授权

US4404063A Method for the separation of indole 失效
标题翻译：吲哚分离方法
公开(公告)号：US4404063A
公开(公告)日：1983-09-13
申请号：US423094
申请日：1982-09-24
申请人： Tadatoshi Honda
发明人： Tadatoshi Honda
IPC分类号： C07D209/08 , C07C209/04 , C07D209/04 , B01D3/34
CPC分类号： C07D209/04
摘要： A method for the separation of indole by distilling an indole-containing reaction fluid obtained by the reaction of aniline with ethylene glycol or by the reaction of N-(.beta.-hydroxyethyl)aniline, which comprises bringing the reaction fluid into contact with a basic substance prior to and/or during the distillation. This method can prevent the deterioration of indole during the distillation procedure.
摘要翻译：通过蒸馏通过苯胺与乙二醇反应获得的含吲哚反应流体或通过N-（β-羟乙基）苯胺的反应来分离吲哚的方法，其包括使反应流体与碱性物质接触在蒸馏之前和/或期间。该方法可以防止在蒸馏过程中吲哚的劣化。

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