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11. 发明授权

US06417263B1 Heat curable silicone rubber composition with improved resistance to engine oils and coolants 失效
标题翻译：可热固化的硅橡胶组合物具有改善的耐发动机油和冷却剂的性能
公开(公告)号：US06417263B1
公开(公告)日：2002-07-09
申请号：US09415240
申请日：1999-10-12
申请人： Jonathan Vierling DeGroot, Jr. , Lawrence Dale Fielder , William James Schulz, Jr. , Antony Pope Wright
发明人： Jonathan Vierling DeGroot, Jr. , Lawrence Dale Fielder , William James Schulz, Jr. , Antony Pope Wright
IPC分类号： C08J510
CPC分类号： C08K3/32 , C08G77/20 , C08K3/26 , C08K3/30 , C08K5/098 , C08L83/04 , C08L83/00 , C08L2666/54
摘要： A heat curable silicone rubber composition, having improved resistance to engine coolants and oils, including long-life coolants and synthetic motor oils, comprises: (A) 100 parts by weight of an organosiloxane polymer base comprising an organosiloxane polymer containing at least 2 silicon-bonded alkenyl groups in each molecule and 1 to 65 weight percent reinforcing silica filler, (B) curing component sufficient to cure the composition when heated, and (C) an effective amount of at least one metal salt additive selected from the group consisting of monobasic alkali metal phosphates, alkali metal oxalates, alkali metal tartrates, alkali metal tetraborates, alkali metal phthalates, alkali metal citrates; dibasic metal phosphates where the metal is selected from the group consisting of sodium, potassium, calcium and magnesium; metal acetates, where the metal is selected from the group consisting of sodium, potassium, calcium, magnesium; metal sulfates where the metal is selected from the group consisting of sodium, potassium, calcium, magnesium, aluminum, and zinc; and metal carbonates where the metal is selected from the group consisting of sodium, potassium, calcium, magnesium, aluminum and zinc.
摘要翻译：具有改进的耐发动机冷却剂和油的耐热性硅橡胶组合物，包括长寿命的冷却剂和合成机油，包括：（A）100重量份的有机硅氧烷聚合物基质，其包含含有至少2个硅 - 每个分子中的键合的烯基和1至65重量％的增强二氧化硅填料，（B）加热时足以固化组合物的固化组分，和（C）有效量的至少一种金属盐添加剂，其选自单碱碱金属磷酸盐，碱金属草酸盐，碱金属酒石酸盐，碱金属四硼酸盐，碱金属邻苯二甲酸盐，碱金属柠檬酸盐; 二价金属磷酸盐，其中金属选自钠，钾，钙和镁; 金属乙酸盐，其中金属选自钠，钾，钙，镁; 金属硫酸盐，其中金属选自钠，钾，钙，镁，铝和锌; 和金属碳酸盐，其中金属选自钠，钾，钙，镁，铝和锌。

12. 发明授权

US06294634B1 Organosilicon compositions from cyclosiloxanes 有权
标题翻译：来自环硅氧烷的有机硅组合物
公开(公告)号：US06294634B1
公开(公告)日：2001-09-25
申请号：US09536141
申请日：2000-03-28
申请人： Michael Salvatore Ferritto , William James Schulz, Jr.
发明人： Michael Salvatore Ferritto , William James Schulz, Jr.
IPC分类号： C08G7708
CPC分类号： C08G77/46 , A61K8/585 , A61K8/891 , A61Q19/00 , C08G77/06
摘要： A method of preparing organosilicon compositions by heating various mixtures of (i) dimethylcyclosiloxanes or methylhydrogencyclosiloxanes, (ii) homopolymeric and copolymeric cyclosiloxanes containing a C5 or more carbon atom containing group, and (iii) homopolymeric and copolymeric cyclosiloxanes containing an oxyalkylene segment, in the presence of a catalyst, at a temperature and for a time sufficient to cause polymerization of cyclosiloxanes (i) to (iii) to the desired organosilicon composition.
摘要翻译：通过加热（i）二甲基环硅氧烷或甲基氢化硅氧烷的各种混合物制备有机硅组合物的方法，（ii）含有C5或更多含碳原子的基团的均聚和共聚环硅氧烷，和（iii）含有氧化烯链段的均聚和共聚的环硅氧烷，在足以使环硅氧烷（i）至（iii）聚合到期望的有机硅组合物的温度和时间下存在催化剂。

13. 发明授权

US06221979B1 Mixtures of silicone elastomers 有权
标题翻译：有机硅弹性体的混合物
公开(公告)号：US06221979B1
公开(公告)日：2001-04-24
申请号：US09435044
申请日：1999-11-08
申请人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
发明人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
IPC分类号： C08G7746
CPC分类号： C08L83/04 , A61K8/06 , A61K8/064 , A61K8/891 , A61K8/894 , A61K8/92 , A61K8/922 , A61Q5/00 , A61Q19/00 , C08G77/12 , C08G77/14 , C08G77/46 , C08G77/70 , C08L83/12 , Y10S516/903 , Y10S516/906 , C08L83/00
摘要： A new composition of matter is a blend of (i) a crosslinked elastomeric silicone polyether and (ii) a crosslinked elastomeric silicone containing alkyl groups having 3-40 carbon atoms. The new composition can be used in preparing water-in-oil emulsions, and clear solutions containing an oil(s) or an oil-soluble active ingredient(s).
摘要翻译：新的物质组合物是（i）交联的弹性硅氧烷聚醚和（ii）含有3-40个碳原子的烷基的交联弹性体硅氧烷的共混物。新组合物可用于制备油包水乳液，以及清除含有油或油溶性活性成分的溶液。

14. 发明授权

US06887934B2 Resin modified elastomers 失效
标题翻译：树脂改性弹性体
公开(公告)号：US06887934B2
公开(公告)日：2005-05-03
申请号：US10227516
申请日：2002-08-26
申请人： Michael Salvatore Ferritto , Tina Marie Leaym , William James Schulz, Jr. , Janet Mary Smith
发明人： Michael Salvatore Ferritto , Tina Marie Leaym , William James Schulz, Jr. , Janet Mary Smith
IPC分类号： A61K8/72 , A61K8/89 , A61K8/895 , A61Q5/00 , A61Q19/00 , C08G77/50 , C08K5/00 , C08K5/01 , C08L83/04 , C08L83/05 , C08L83/07 , C08L83/14
CPC分类号： A61Q5/00 , A61K8/895 , A61Q19/00 , C08G77/12 , C08G77/20 , C08G77/50 , C08K5/01 , C08L83/04 , C08L83/14 , C08L83/00
摘要： Resin modified elastomers, methods of making them and their uses. The method for making the elastomers comprises reacting in a diluent an ≡SiH functional siloxane; a diene, diyne or ene-yne compound, a resin having the formula (R13SiO1/2)x(SiO4/2)y(R1SiO3/2)z where each R1 is independently a monovalent hydrocarbon group having 1 to 30 carbon atoms or an unsaturated hydrocarbon group having 2 to 30 carbon atoms x is ≧1, y≧0, z≧0 and y+z≧1.
摘要翻译：树脂改性弹性体，制造方法及其用途。制备弹性体的方法包括在稀释剂中使≡SiH官能化硅氧烷反应; 二烯烃，二炔烃或烯烃化合物，具有下式的树脂：（R 1）3 SiO 1/2，（SiO 2/2/2）y（R 1，O 3，3/2））z 其中每个R 1独立地为具有1至30个碳原子的一价烃基或具有2至30个碳原子的不饱和烃基，x = 1，y> = 0，z > = 0并且y + z> = 1。

15. 发明授权

US06803399B2 Silicone liquid crystals, vesicles, and gels 失效
标题翻译：硅胶液晶，囊泡和凝胶
公开(公告)号：US06803399B2
公开(公告)日：2004-10-12
申请号：US10465316
申请日：2003-06-19
申请人： Michael Salvatore Ferritto , Zuchen Lin , William James Schulz, Jr.
发明人： Michael Salvatore Ferritto , Zuchen Lin , William James Schulz, Jr.
IPC分类号： C08K554
CPC分类号： A61K8/893 , A61K8/0295 , A61K8/042 , A61K8/14 , A61K8/898 , A61K2800/594 , A61Q5/00 , A61Q13/00 , A61Q15/00 , A61Q17/04 , A61Q19/00 , C08G59/50 , C08G77/045 , C08G77/14 , C08G77/26 , C08G77/46 , C08G77/70 , C08J3/205 , C08J3/26 , C08J2383/04 , C08L83/04 , C08L83/08 , C08L2666/02
摘要： Silicone liquid crystals, silicone vesicles, and silicone gels are formed by combining (i) an amine functional silicone or an organic amine compound, (ii) an organic epoxide containing at least two epoxy groups or an epoxy functional silicone containing at least two epoxy groups, and (iii) a fluid such as water, a silicone fluid other than a silicone used in (i) and (ii), and a polar organic compound or nonpolar organic compound other than organic compounds used in (i) and (ii) in which the polar and nonpolar organic compound are present at a concentration to provide a level of solids less than 40 percent by weight based on the weight of (i)-(iii). These silicone liquid crystals, silicone vesicles, and silicone gels are useful in personal care for preparing various skin, hair, and underarm products.
摘要翻译：通过组合（i）胺官能硅氧烷或有机胺化合物，（ii）含有至少两个环氧基的有机环氧化物或含有至少两个环氧基的环氧官能硅氧烷，形成有机硅液体，有机硅泡沫和硅氧烷凝胶（i）和（ii）中使用的有机化合物以外的极性有机化合物或非极性有机化合物，以及（iii）除了（i）和（ii）中使用的硅酮以外的其它流体，其中极性和非极性有机化合物以浓度提供基于（i） - （iii）的重量提供小于40重量％的固体含量的浓度。这些有机硅液晶，有机硅泡沫和有机硅凝胶可用于个人护理，用于制备各种皮肤，头发和腋下产品。

16. 发明授权

US06168782A Elastomeric silicone containing an active ingredient 有权
标题翻译：弹性硅氧烷含有活性成分
公开(公告)号：US06168782A
公开(公告)日：2001-01-02
申请号：US09317459
申请日：1999-05-24
申请人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
发明人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
IPC分类号： A61K3174
CPC分类号： A61K8/894 , A61Q5/02 , A61Q19/00 , C08L83/12 , C08L83/14 , C08L2666/28
摘要： Elastomeric silicones, especially elastomeric silicone polyethers, are prepared by combining and reacting (A) an ≡Si—H containing polysiloxane, (B) a mono-alkenyl polyether, (C) an active ingredient such as a vitamin, antimicrobial agent, sunburn prevention agent, astringent, or sex hormone, (D) an &agr;,&ohgr;-unsaturated hydrocarbon, (E) a platinum catalyst, and (F) an oil. The reaction of components (A)-(F) is allowed to continue, forming a crosslinked three-dimensional gelled network of the elastomeric silicone polyether containing the active ingredient and the oil. The compositions are useful in personal and health care applications, personal hygiene, and household cleaning applications.
摘要翻译：弹性体硅酮，特别是弹性硅氧烷聚醚，是通过（A）a =含Si-H的聚硅氧烷，（B）单烯基聚醚，（C）活性成分如维生素，抗微生物剂，防晒剂药剂，收敛剂或性激素，（D）α，ω-不饱和烃，（E）铂催化剂和（F）油。允许组分（A） - （F）的反应继续，形成含有活性成分和油的弹性体硅氧烷聚醚的交联的三维胶凝网。该组合物可用于个人和医疗保健应用，个人卫生和家庭清洁应用。

17. 发明授权

US5777002A Method for preparing organopolysiloxane bases and compositions therefrom 失效
标题翻译：制备有机聚硅氧烷碱及其组合物的方法
公开(公告)号：US5777002A
公开(公告)日：1998-07-07
申请号：US748435
申请日：1996-11-13
申请人： Lori Jean Conway , Thomas Edward Gray , Phillip Joseph Griffith , William James Schulz, Jr.
发明人： Lori Jean Conway , Thomas Edward Gray , Phillip Joseph Griffith , William James Schulz, Jr.
IPC分类号： C08K9/06 , C08L83/04
CPC分类号： C08K9/06 , C08L83/04 , C08G77/045 , C08G77/16 , C08G77/20
摘要： A method for preparing organopolysiloxane bases with high levels of fillers. The present inventors have found that by mixing the components of the base at a temperature below about 60.degree. C. for a period of time sufficient to effect essentially a homogeneous blend, a base composition is formed which can be further blended with a platinum group metal-containing catalyst, an organohydrogensiloxane, and optionally an inhibitor to form a curable liquid silicone rubber (LSR) composition. The curable LSR composition has improved flow characteristics and improved shelf life when compared to similar materials where the base is prepared at temperatures above about 60.degree. C. The improved flow characteristics allows larger quantities of fillers to be incorporated into the curable LSR composition while still maintaining acceptable flow characteristics. Silicone elastomers prepared using the curable LSR compositions can have improved swell and degradation resistance to oils, lower compression set values, and improved tear, elongation, and tensile values and require no post cure. The present organopolysiloxane bases are particularly useful as a common base for forming a group of cured silicone elastomers with a range of durometers.
摘要翻译：一种制备高含量填料的有机聚硅氧烷基料的方法。本发明人已经发现，通过将碱的组分在低于约60℃的温度下混合足以实现基本均匀共混物的时间，形成基础组合物，其可以进一步与铂族金属的有机氢硅氧烷和任选的抑制剂以形成可固化液体硅橡胶（LSR）组合物。与基材在高于约60℃的温度下制备的类似材料相比，可固化的LSR组合物具有改善的流动特性和改善的保质期。改进的流动特性允许更大量的填料掺入可固化LSR组合物中同时仍保持可接受的流量特性。使用可固化的LSR组合物制备的硅氧烷弹性体可以具有改善的对油的溶胀和降解抗性，较低的压缩永久变形值和改进的撕裂，伸长率和拉伸值，并且不需要后固化。本发明的有机聚硅氧烷基料特别可用作形成具有一定范围的硬度的一组固化的硅氧烷弹性体的常用碱。

18. 发明授权

US5654362A Silicone oils and solvents thickened by silicone elastomers 失效
标题翻译：硅油和硅酮弹性体增稠的溶剂
公开(公告)号：US5654362A
公开(公告)日：1997-08-05
申请号：US618616
申请日：1996-03-20
申请人： William James Schulz, Jr. , Shizhong Zhahg
发明人： William James Schulz, Jr. , Shizhong Zhahg
IPC分类号： C08J3/09 , C08L83/04 , C08L83/05 , C08L83/14
CPC分类号： C08J3/09 , C08L83/04 , C08L83/14 , C08G77/12 , C08G77/20 , C08G77/70 , C08J2383/04
摘要： Silicone gels are made by reacting an .tbd.Si--H containing polysiloxane with an alpha, omega-diene. The reaction is conducted in the presence of a platinum catalyst and in the presence of a low molecular weight silicone oil. The reaction is continued until a gel is formed by crosslinking and addition of .tbd.Si--H across double bonds in the alpha, omega-diene. The silicone gel can then be crumbled into a silicone powder using mechanical force. When additional amounts of low molecular weight silicone oil are added to the gel, and the silicone oil and the gel are subjected to shear force, a silicone paste can be formed.
摘要翻译：硅氧烷凝胶通过使含有SiTHH的聚硅氧烷与α，ω-二烯反应而制成。该反应在铂催化剂存在下和在低分子量硅油存在下进行。反应继续进行，直到通过交联并通过在α，ω-二烯中双键加入3BOND Si-H形成凝胶。然后可以使用机械力将有机硅凝胶粉碎成硅酮粉末。当将另外量的低分子量硅油加入到凝胶中，并且硅油和凝胶受到剪切力时，可以形成硅胶。

19. 发明授权

US06207717B1 Entrapment of vitamins with an elastomeric silicone polyether 有权
标题翻译：用弹性硅氧烷聚醚包埋维生素
公开(公告)号：US06207717B1
公开(公告)日：2001-03-27
申请号：US09228301
申请日：1999-01-12
申请人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
发明人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
IPC分类号： A61K4730
CPC分类号： A61K8/894 , A61K8/671 , A61K8/678 , A61K9/107 , A61K47/34 , A61Q19/00 , C08G77/46 , C08L83/12
摘要： Oil-soluble vitamins such as vitamin A and vitamin E can be entrapped in the oil phase of an elastomeric silicone polyether. The vitamin entrapped oil phase can then be emulsified and stabilized without requiring the use of other surfactants. The vitamin entrapped oil phase and water-in-oil emulsions prepared from the vitamin entrapped oil phase are useful in water-based skin and cosmetic compositions.
摘要翻译：油溶性维生素如维生素A和维生素E可以包埋在弹性体硅氧烷聚醚的油相中。然后可以将维生素捕获的油相乳化并稳定，而不需要使用其它表面活性剂。由维生素截留的油相制备的维生素截留的油相和油包水乳液可用于水性皮肤和化妆品组合物。

20. 发明授权

US06200581B1 Elastomeric silicone terpolymer 有权
标题翻译：弹性硅胶三元共聚物
公开(公告)号：US06200581B1
公开(公告)日：2001-03-13
申请号：US09299864
申请日：1999-04-28
申请人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
发明人： Zuchen Lin , William James Schulz, Jr. , Janet Mary Smith
IPC分类号： A61K600
CPC分类号： A61K8/894 , A61K8/0208 , A61K8/04 , A61K8/042 , A61K8/066 , A61Q5/00 , A61Q19/00 , C08G77/46 , C08G77/50 , Y10S514/937 , Y10T442/20
摘要： Three-dimensional silicone elastomers having both polyether and higher alkyl functionality present in their molecules are in the form of networks of crosslinked linear siloxanes with polyether and olefin containing repeating units. Representative units are EO7 and EO12 for the polyether functionality, and C10, C12, and C18 alkyl functionality for the olefin. These gelled molecules are multipurpose type materials, and consequently they are capable of being useful in a variety of multiphased formulations in personal and health care applications.
摘要翻译：其分子中存在聚醚和高级烷基官能团的三维有机硅弹性体是具有聚醚和含烯烃的重复单元的交联线性硅氧烷网络的形式。代表性单元是用于聚醚官能团的EO 7和EO 12，以及烯烃的C 10，C 12和C 18烷基官能团。这些凝胶分子是多用途类型的材料，因此它们能够用于个人和医疗保健应用中的各种多相配方。

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