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11. 发明授权

US4291167A Preparation of tetramethyldisilane from 1,2-tetramethyldichlorodisilane 失效
标题翻译：从1,2-四甲基二氯二硅烷制备四甲基硅烷
公开(公告)号：US4291167A
公开(公告)日：1981-09-22
申请号：US172611
申请日：1980-07-28
申请人： Ronald J. Allain , Joseph P. Maniscalco
发明人： Ronald J. Allain , Joseph P. Maniscalco
IPC分类号： C07F7/08
CPC分类号： C07F7/0896
摘要： A process of producing tetramethyldisilane by reacting tetramethyldichlorodisilane with a reducing mixture of NaH and NaBH.sub.4 in the presence of a complexing ether such as the diethyl ether of tetraethylene glycol.
摘要翻译：通过四甲基二氯二硅烷与NaH和NaBH 4的还原性混合物在络合醚例如四乙二醇的乙醚存在下反应生产四甲基二硅烷的方法。

12. 发明授权

US4201758A Boron removal from ethylene glycol-magnesium chloride solutions 失效
标题翻译：从乙二醇 - 氯化镁溶液中除去硼
公开(公告)号：US4201758A
公开(公告)日：1980-05-06
申请号：US22666
申请日：1979-03-22
申请人： Ronald J. Allain , David G. Braithwaite , Ansell L. Reid
发明人： Ronald J. Allain , David G. Braithwaite , Ansell L. Reid
IPC分类号： C01F5/30 , C01F5/34
CPC分类号： C01F5/34 , C01F5/30
摘要： A method for removing boric acid and salts therefrom from ethylene glycol-magnesium chloride solutions which contain at least 100 ppm of boron which comprises reducing the pH of such solutions below 7 and then adding thereto at least 3 moles of methanol based on the amount of boric acid or salt thereof present in said solution and then subjecting the thus-treated ethylene glycol-magnesium chloride solution to distillation at a temperature sufficient to remove trimethyl borate-methanol therefrom, thereby reducing the level of boron in the starting solution to not more than 35 ppm.
摘要翻译：一种从含有至少100ppm硼的乙二醇 - 氯化镁溶液中除去硼酸及其盐的方法，其包括将该溶液的pH降低到7以下，然后加入至少3摩尔甲醇，基于硼的量酸或其盐，然后在足以从其中除去三甲基硼酸盐 - 甲醇的温度下将经过处理的乙二醇 - 氯化镁溶液进行蒸馏，从而将起始溶液中的硼水平降低至不超过35 ppm。

13. 发明授权

US4195070A Preparation of a MgCl.sub.2 solution for Nalco's MgCl.sub.2 process from MgSO.sub.4 and other MgSO.sub.4 salts 失效
标题翻译：从MgSO 4和其他MgSO 4盐制备用于Nalco MgCl 2工艺的MgCl 2溶液
公开(公告)号：US4195070A
公开(公告)日：1980-03-25
申请号：US22397
申请日：1979-03-21
申请人： Ronald J. Allain , David G. Braithwaite , Joseph P. Maniscalco
发明人： Ronald J. Allain , David G. Braithwaite , Joseph P. Maniscalco
IPC分类号： C01D5/00 , C01F5/34 , C01D5/10 , C01D5/18
CPC分类号： C01D5/00 , C01F5/34
摘要： A method of beneficiating a mixed salt mineral ore containing potassium and magnesium sulfates and/or their hydrates which allows the recovery of anhydrous magnesium chloride and the simultaneous recovery of commercially acceptable potassium sulfate.
摘要翻译：一种优选含有硫酸钾和镁和/或其水合物的混合矿物矿石的方法，其允许回收无水氯化镁并同时回收商业上可接受的硫酸钾。

14. 发明授权

US4140491A Gasoline additive comprising a blend of methylcyclopentadienyl manganese tricarbonyl and certain methylcyclopentadiene dimer compounds 失效
标题翻译：含有甲基环戊二烯基三羰基锰与某些甲基环戊二烯二聚体化合物的混合物的汽油添加剂
公开(公告)号：US4140491A
公开(公告)日：1979-02-20
申请号：US853615
申请日：1977-11-21
申请人： Ronald J. Allain , Ansell L. Reid
发明人： Ronald J. Allain , Ansell L. Reid
IPC分类号： C10L1/14 , C10L1/18 , C10L1/30
CPC分类号： C10L10/10 , C10L1/14 , C10L1/182 , C10L1/1822 , C10L1/305
摘要： Gasoline containing an additive comprising about 70% by weight of methylcyclopentadienyl manganese tricarbonyl and about 30% of a composition selected from the group consisting of methylcyclopentadiene dimer compounds, hydrogenated methylcyclopentadiene dimer compounds, and the alcohols of methylcyclopentadiene dimer compounds, said additive being present in the gasoline in an amount sufficient to increase its anti-knock effectiveness.
摘要翻译：含有约70重量％甲基环戊二烯基三羰基锰和约30％选自甲基环戊二烯二聚体化合物，氢化甲基环戊二烯二聚体化合物和甲基环戊二烯二聚体化合物的醇的组合物的汽油的汽油，所述添加剂存在于汽油的量足以提高其抗爆击效能。

15. 发明授权

US3966888A Anhydrous magnesium chloride using ethylene glycol and ammonia 失效
标题翻译：使用乙二醇和氨的无水氯化镁
公开(公告)号：US3966888A
公开(公告)日：1976-06-29
申请号：US626813
申请日：1975-10-29
申请人： David G. Braithwaite , Ronald J. Allain
发明人： David G. Braithwaite , Ronald J. Allain
IPC分类号： C01F5/34
CPC分类号： C01F5/34
摘要： Anhydrous magnesium chloride may be prepared from magnesium chloride hydrates by the following sequence of processing steps:1. Dissolving the magnesium chloride hydrate in ethylene glycol to form a magnesium chloride hydrate solution.2. Heating the thus-formed solution to remove all the water therefrom thereby forming a ethylene glycol anhydrous magnesium chloride solution.3. Treating the water-free magnesium chloride-ethylene glycol solution with ammonia to form a magnesium chloride ammonia complex which precipitates from the ethylene glycol.4. Removing the precipitate from the ethylene glycol and washing it with a low boiling solvent for ethylene glycol to remove any ethylene glycol entrained in the precipitate.5. Heating the magnesium chloride ammonia complex to drive off the ammonia which leaves as a finished product completely anhydrous magnesium chloride.
摘要翻译：无水氯化镁可以通过以下顺序的加工步骤由氯化镁水合物制备：

16. 发明授权

US06372882B1 Method for producing substantially dry water-insoluble polymers for improved flocculation in the bayer process 失效
标题翻译：用于生产基本上干的水不溶性聚合物的方法，用于改进拜耳法中的絮凝
公开(公告)号：US06372882B1
公开(公告)日：2002-04-16
申请号：US09542074
申请日：2000-04-03
申请人： Everett C. Phillips , Ronald J. Allain
发明人： Everett C. Phillips , Ronald J. Allain
IPC分类号： C08F614
CPC分类号： C08J3/122 , C01F7/0653 , C08J2333/06
摘要： The present invention is a method of producing substantially dry water insoluble polymers from poly alkyl esters of vinylic monomers for use in a method for the clarification of red mud-containing liquors generated in the Bayer process for the recovery of alumina from bauxite ore. The polymers can be either homopolymers, copolymers or terpolymers. Preferably, the dried emulsion polymers are high molecular weight polymers of poly(methyl acrylate), poly(methyl acrylate/acrylic acid), poly(vinyl acetate/acrylic acid/methyl acrylate), poly(t-butyl methacrylate/acrylic acid/methyl acrylate) and poly(t-butyl acrylate/acrylic acid/methyl acrylate).
摘要翻译：本发明是一种从乙烯基单体的聚烷基酯生产基本上干燥的水不溶性聚合物的方法，用于澄清在拜耳法中产生的用于从铝土矿矿石回收氧化铝的含红泥的液体的方法。聚合物可以是均聚物，共聚物或三元共聚物。优选地，干燥的乳液聚合物是聚（丙烯酸甲酯），聚（丙烯酸甲酯/丙烯酸），聚（乙酸乙烯酯/丙烯酸/丙烯酸甲酯），聚（甲基丙烯酸叔丁酯/丙烯酸/甲基）丙烯酸酯）和聚（丙烯酸叔丁酯/丙烯酸/丙烯酸甲酯）。

17. 发明授权

US4309556A Preparation of hexamethyldisilane (HMDS) from chloromethyldisilanes using special solvents 失效
标题翻译：使用特殊溶剂由氯甲基二硅烷制备六甲基二硅烷（HMDS）
公开(公告)号：US4309556A
公开(公告)日：1982-01-05
申请号：US171768
申请日：1980-07-24
申请人： Ronald J. Allain , Joseph P. Maniscalco
发明人： Ronald J. Allain , Joseph P. Maniscalco
IPC分类号： C07F7/08 , C07F7/12
CPC分类号： C07F7/0821 , C07F7/122
摘要： An improved process for producing hexamethyldisilane by reacting ether solutions of methyl Grignard with a crude mixture of chloromethyl disilanes, the improvement which comprises obtaining higher yields and simplified purification of HMDS by the use of a mixed solvent system composed of tetrahydrofuran and the diethyl ether of tetraethylene glycol.
摘要翻译：通过使格列尼尔甲醚的醚溶液与氯甲基二硅烷的粗混合物反应制备六甲基二硅烷的改进方法，其改进包括通过使用由四氢呋喃和四乙烯的乙醚组成的混合溶剂系统获得更高的产率和简化的HMDS的纯化乙二醇

18. 发明授权

US4248838A Preparation of useful MgCl.sub.2. solution with subsequent recovery of KCl from carnallite 失效
标题翻译：制备有用的MgCl2。溶液随后从光卤石回收KCl
公开(公告)号：US4248838A
公开(公告)日：1981-02-03
申请号：US22396
申请日：1979-03-21
申请人： Ronald J. Allain , David G. Braithwaite , Joseph P. Maniscalco
发明人： Ronald J. Allain , David G. Braithwaite , Joseph P. Maniscalco
IPC分类号： C01F5/30 , C01D3/08 , C01D5/00 , C01F5/34
CPC分类号： C01D5/00 , C01D3/08 , C01F5/34
摘要： This invention outlines a process to beneficiate carnallite ores in such a way as to obtain anhydrous MgCl.sub.2 of sufficient purity to be used as feed for an electrolysis cell producing magnesium metal. Commercially acceptable potassium chloride as also recovered. The organic solvents and the anhydrous ammonia used to obtain the beneficiation of these carnallite materials are recovered for recycle in the process.
摘要翻译：本发明概述了以获得足够纯度的无水MgCl 2作为生产镁金属电解池的进料的方法来选择光卤石矿石的方法。也可回收市售的氯化钾。用于获得这些光卤石材料的选矿的有机溶剂和无水氨回收再循环。

19. 发明授权

US4195071A Polyethers to obtain anhydrous magnesium chloride 失效
标题翻译：聚醚获得无水氯化镁
公开(公告)号：US4195071A
公开(公告)日：1980-03-25
申请号：US016710
申请日：1979-03-01
申请人： Ronald J. Allain , David G. Braithwaite , Joseph P. Maniscalco
发明人： Ronald J. Allain , David G. Braithwaite , Joseph P. Maniscalco
IPC分类号： C01F5/34
CPC分类号： C01F5/34
摘要： In a process of producing anhydrous magnesium chloride of the type comprising:A. Mixing together a magnesium chloride hydrate, said hydrate containing minor amounts of water-soluble sulfate and boron compounds as impurities with diethyl ether of tetraethylene glycol to prepare 0.1-6.0% by weight slurry of MgCl.sub.2 in the diethyl ether of tetraethylene glycol and an azeotropic agent having a boiling point less than the diethyl ether of tetraethylene glycol in a quantity sufficient to remove water from said slurry;the improvement which comprises substituting dibutyl ether of tetraethylene glycol for the diethyl ether of tetraethylene glycol.
摘要翻译：在制备以下类型的无水氯化镁的方法中：A.将氯化镁水合物，所述水合物与少量的水溶性硫酸盐和硼化合物混合在一起作为杂质与四乙二醇的乙醚混合，制备0.1-6.0％的在四乙二醇的二乙醚中的MgCl 2重量浆料和沸点低于四甘醇二乙醚的共沸剂，其量足以从所述浆料中除去水; 其改进包括用四乙二醇的二丁基醚代替四乙二醇的乙醚。

20. 发明授权

US3983224A Anhydrous magnesium chloride process 失效
标题翻译：无水氯化镁工艺
公开(公告)号：US3983224A
公开(公告)日：1976-09-28
申请号：US680403
申请日：1976-04-26
申请人： Ronald J. Allain , David G. Braithwaite
发明人： Ronald J. Allain , David G. Braithwaite
IPC分类号： C01F5/30 , C01F5/34
CPC分类号： C01F5/34
摘要： Anhydrous magnesium chloride may be prepared for magnesium chloride hydrate by the following sequence of process steps:A. mixing together a magnesium chloride hydrate said hydrate containing minor amounts of water soluble sulfate and boron compounds as impurities with diethyl ether of tetraethylene glycol to prepare 0.1 - 6.0% by weight slurry of MgCl.sub.2 in the diethyl ether of tetraethylene glycol and an azeotropic agent having a boiling point less than the diethyl ether of tetraethylene glycol in a quantity sufficient to remove water from said slurry;B. distilling water from said slurry wherein an anhydrous solution of MgCl.sub.2 in diethyl ether of tetraethylene glycol containing the water soluble sulfate and boron compounds as insoluble impurities is formed;C. separating said MgCl.sub.2 solution from the insoluble impurities;D. adding to the MgCl.sub.2 solution about 3.0 moles of ethylene glycol per mole of MgCl.sub.2 present so as to prepare a MgCl.sub.2.3 moles ethylene glycol complex precipitate;E. separating precipitate pecipitate from the diethyl ether of tetraethylene glycol and recovering the precipitate;F. dissolving said precipitate in ethylene glycol to prepare a solution of the precipitate in ethylene glycol said ethylene glycol being used in a quantity so as to prepare an ethylene glycol solution containing from 1 to 20% by weight MgCl.sub.2 ;G. treating the ethylene glycol magnesium chloride solution with ammonia to form a magnesium chloride-ammonia complex which is insoluble in the ethylene glycol with the temperature of the ethylene glycol magnesium chloride solution being within the range of between -15.degree. to 50.degree.C;H. separating the magnesium chloride-ammonia complex from the ethylene glycol;I. washing the magnesium chloride-ammonia complex with a polar solvent having a lower boiling point than ethylene glycol to remove any ethlene glycol entrained in the magnesium chloride-ammonia complex;J. heating the magnesium chloride-ammonia complex to a temperature sufficient to drive off the ammonia for a sufficient period of time to remove the ammonia, thereby forming anhydrous magnesium chloride; and then,K. recovering anhydrous magnesium chloride which has a magnesium oxide content of less than 0.8% by weight and which is substantially free of impurities.
摘要翻译：可以通过以下顺序的步骤制备氯化镁水合物的无水氯化镁：

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