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11. 发明申请

US20070142665A1 Method of making a synthetic petroleum sulfonate 有权
标题翻译：制造合成石油磺酸盐的方法
公开(公告)号：US20070142665A1
公开(公告)日：2007-06-21
申请号：US11316106
申请日：2005-12-21
申请人： Curt B. Campbell , Thomas V. Harris , Gilles Sinquin
发明人： Curt B. Campbell , Thomas V. Harris , Gilles Sinquin
IPC分类号： C07C303/06
CPC分类号： C07C303/06 , C07C309/31
摘要： A process for preparing a synthetic petroleum sulfonate comprising (a) reacting at least one aromatic compound with a mixture of olefins selected from olefins having from about 8 to about 100 carbon atoms, in the presence of an acidic ionic liquid catalyst, wherein the resulting product comprises at least about 50 weight percent of a 1,2,4 tri-substituted aromatic compound or a 1,2,3 tri-substituted aromatic compound or mixtures thereof; (b) reacting the product of (a) with sulfur trioxide, which has been diluted with air; and (c) neutralizing the product of (b) with an alkali or alkaline earth metal hydroxide.
摘要翻译：一种制备合成石油磺酸盐的方法，包括（a）在酸性离子液体催化剂存在下使至少一种芳族化合物与选自约8至约100个碳原子的烯烃的烯烃混合物反应，其中所得产物包含至少约50重量％的1,2,4-三取代芳族化合物或1,2,3-三取代芳族化合物或其混合物; （b）使（a）的产物与已经用空气稀释的三氧化硫反应; 和（c）用碱金属或碱土金属氢氧化物中和（b）的产物。

12. 发明授权

US08148591B2 Method of making a synthetic alkylaryl compound 有权
标题翻译：制备合成烷基芳基化合物的方法
公开(公告)号：US08148591B2
公开(公告)日：2012-04-03
申请号：US11963340
申请日：2007-12-21
申请人： Gilles P. Sinquin , Curt B. Campbell
发明人： Gilles P. Sinquin , Curt B. Campbell
IPC分类号： C07C2/68 , C07C2/70
CPC分类号： C07C2/70 , C07C2527/03 , C07C2527/054 , C07C2527/11 , C07C2527/1206 , C07C2531/025 , C07C15/107
摘要： A process for alkylating an aromatic compound comprising reacting at least one aromatic compound with a mixture of olefins having from about 8 to about 100 carbon atoms, in the presence of a strong acid catalyst wherein the resulting product comprises at least about 60 weight percent of a 1,2,4 tri-alkylsubstituted aromatic compound.
摘要翻译：一种用于烷基化芳族化合物的方法，包括在强酸催化剂存在下使至少一种芳族化合物与具有约8至约100个碳原子的烯烃的混合物反应，其中所得产物包含至少约60重量％的 1,2,4-三烷基取代芳香族化合物。

13. 发明申请

US20100160703A1 Method of making an alkylated aromatic using compound using an acidic ionic liquid catalyst 审中-公开
标题翻译：使用酸性离子液体催化剂制备烷基化芳族化合物的方法
公开(公告)号：US20100160703A1
公开(公告)日：2010-06-24
申请号：US12660083
申请日：2010-02-19
申请人： Michael Driver , Curt B. Campbell , Thomas V. Harris
发明人： Michael Driver , Curt B. Campbell , Thomas V. Harris
IPC分类号： C07C2/66 , C07C2/70 , C07C2/68
CPC分类号： C07C2/66 , C07C2/22 , C07C2531/14 , C07C15/107 , C07C11/02
摘要： A process for alkylating an aromatic compound containing no hydroxyl groups comprising reacting at least one non-hydroxyl containing aromatic compound with at least one olefinic oligomer in the presence of an acidic ionic liquid catalyst, wherein the olefinic oligomer has a carbon range of from about C12 to about C70 and is synthesized by oligomerizing at least one monoolefin monomer in the presence of an acidic ionic liquid catalyst.
摘要翻译：一种用于烷基化不含羟基的芳族化合物的方法，包括在酸性离子液体催化剂存在下使至少一种含非芳族化合物与至少一种烯属低聚物反应，其中烯属低聚物的碳含量为约C12 至约C70，并通过在酸性离子液体催化剂存在下使至少一种单烯烃单体低聚来合成。

14. 发明授权

US07071370B2 Mordenite zeolite alkylation catalyst 有权
标题翻译：丝光沸石烷基化催化剂
公开(公告)号：US07071370B2
公开(公告)日：2006-07-04
申请号：US11186155
申请日：2005-07-20
申请人： Thomas V. Harris , Curt B. Campbell , Pierre Tequi , Jean-Louis Le Coent
发明人： Thomas V. Harris , Curt B. Campbell , Pierre Tequi , Jean-Louis Le Coent
IPC分类号： C07C2/66
CPC分类号： B01J29/18 , B01J37/0009 , B01J2229/37 , B01J2229/42 , C07C2/66
摘要： The present invention is directed to a mordenite zeolite catalyst having a controlled macropore structure. The present invention is also directed to a mordenite zeolite catalyst composite and a process for preparing the catalyst composite. The catalyst composite exhibits reduced deactivation rates during the alkylation process, thereby increasing the life of the catalyst.
摘要翻译：本发明涉及具有受控大孔结构的丝光沸石催化剂。本发明还涉及丝光沸石催化剂复合材料及其制备方法。催化剂复合物在烷基化过程中表现出降低的失活速率，从而增加催化剂的寿命。

15. 发明授权

US5922922A Process for producing an alkylated, non-oxygen-containing aromatic hydrocarbon 失效
标题翻译：用于制备烷基化的，非含氧芳族烃的方法
公开(公告)号：US5922922A
公开(公告)日：1999-07-13
申请号：US895540
申请日：1997-07-17
申请人： Thomas V. Harris , Curt B. Campbell , Mohammed M. Habib
发明人： Thomas V. Harris , Curt B. Campbell , Mohammed M. Habib
IPC分类号： B01J29/04 , B01J29/08 , C07B61/00 , C07C2/66 , C07C5/27 , C07C15/02 , C07C15/107 , C07C2/68 , C07C2/64 , C07C5/22
CPC分类号： C07C15/107 , C07C15/02 , C07C5/2775 , C07C2521/16 , C07C2529/06 , C07C2529/08
摘要： An alkylated aromatic hydrocarbon is produced having the following properties: (a) less than 40 wt. % of the alkylated aromatic hydrocarbon is 2-aryl; and (b) at least 20 wt. % of the alkylated aromatic hydrocarbon is a monoalkylate. That alkylated aromatic hydrocarbon is produced by isomerizing a normal alpha-olefin having from 20 to 28 carbon atoms in the presence of a first acidic catalyst to produce a partially-branched, isomerized olefin, then either benzene or toluene is alkylated with the partially-branched, isomerized olefin in the presence of a second solid, acidic catalyst. The first acidic catalyst can be a molecular sieve with a one-dimensional pore system. The second acidic catalyst can be a zeolite Y having a silica to alumina ratio of at least 40:1.
摘要翻译：制备具有以下特性的烷基化芳烃：（a）小于40wt。％的烷基化芳烃为2-芳基; 和（b）至少20wt。％的烷基化芳烃是单烷基化物。该烷基化芳烃通过在第一酸性催化剂存在下异构化具有20至28个碳原子的正常α-烯烃来制备，以产生部分支化的异构化烯烃，然后将苯或甲苯用部分支化的异构化的烯烃，在第二固体酸性催化剂的存在下。第一种酸性催化剂可以是具有一维孔隙体系的分子筛。第二酸性催化剂可以是二氧化硅与氧化铝之比至少为40:1的沸石Y。

16. 发明授权

US07563937B2 Zeolite Y alkylation catalysts 有权
标题翻译：沸石Y烷基化催化剂
公开(公告)号：US07563937B2
公开(公告)日：2009-07-21
申请号：US11355754
申请日：2006-02-15
申请人： Thomas V. Harris , Curt B. Campbell , Paul J. Marcatntonio , Pierre Tequi , Jean-Louis Le Coent
发明人： Thomas V. Harris , Curt B. Campbell , Paul J. Marcatntonio , Pierre Tequi , Jean-Louis Le Coent
IPC分类号： C07C13/00 , C10M127/00
CPC分类号： B01J37/0009 , B01J29/084 , B01J35/1038 , B01J35/1066 , B01J2229/42 , C07C2/66 , C07C303/06 , C07C309/31 , C07C309/58 , C07C2529/06 , C10M159/24 , C10M2219/046 , C07C15/107 , C10N2210/02
摘要： The present invention is directed to a zeolite Y catalyst having a controlled macropore structure. The present invention is also directed to a zeolite Y catalyst composite and a process for preparing the catalyst composite. The catalyst composite exhibits reduced deactivation rates during the alkylation process, thereby increasing the life of the catalyst. The present invention is also directed to processes for the preparation of carbonated, overbased aromatic sulfonates, which processes comprise alkylation, carbonation of aromatic hydrocarbons with one or more olefins.
摘要翻译：本发明涉及具有受控大孔结构的沸石Y催化剂。本发明还涉及沸石Y催化剂复合材料和制备催化剂复合材料的方法。催化剂复合物在烷基化过程中表现出降低的失活速率，从而增加催化剂的寿命。本发明还涉及制备碳酸化的高碱性芳族磺酸盐的方法，该方法包括芳族烃与一种或多种烯烃的烷基化，碳酸化。

17. 发明申请

US20090163669A1 METHOD OF MAKING A SYNTHETIC ALKYLARYL SULFONATE 审中-公开
标题翻译：制备合成烷基磺酸钠的方法
公开(公告)号：US20090163669A1
公开(公告)日：2009-06-25
申请号：US11963240
申请日：2007-12-21
申请人： Gilles P. Sinquin , Curt B. Campbell
发明人： Gilles P. Sinquin , Curt B. Campbell
IPC分类号： C07C309/63 , C08F8/36
CPC分类号： C07C303/32 , C07C2/70 , C07C303/06 , C07C309/31 , C07C2527/03 , C07C2527/054 , C07C2527/11 , C07C2527/1206 , C07C2531/025 , C09K8/584 , C07C15/107
摘要： A process for preparing a synthetic petroleum sulfonate comprising (a) reacting a first amount of at least one aromatic compound with a first amount of a mixture of olefins having from about 8 to about 100 carbon atoms, in the presence of a strong acid catalyst, wherein the resulting product comprises at least about 60 weight percent of a 1,2,4-trialkylsubstituted aromatic compound; (b) sulfonating the product of (a); and (c) neutralizing the product of (b) with an alkali or alkaline earth metal hydroxide or ammonia.
摘要翻译：一种制备合成石油磺酸盐的方法，包括（a）在强酸催化剂存在下使第一量的至少一种芳族化合物与第一量的具有约8至约100个碳原子的烯烃的混合物反应，其中所得产物包含至少约60重量％的1,2,4-三烷基取代的芳族化合物; （b）将（a）的产物磺化; 和（c）用碱金属或碱土金属氢氧化物或氨中和（b）的产物。

18. 发明授权

US06348438B1 Production of high BN alkaline earth metal single-aromatic ring hydrocarbyl salicylate-carboxylate 失效
标题翻译：生产高碱性碱土金属单芳香环烃基水杨酸酯 - 羧酸盐
公开(公告)号：US06348438B1
公开(公告)日：2002-02-19
申请号：US09325209
申请日：1999-06-03
申请人： Jean-Louis Marie Le Coent , Curt B. Campbell , Thierry Triconnet
发明人： Jean-Louis Marie Le Coent , Curt B. Campbell , Thierry Triconnet
IPC分类号： C10M15920
CPC分类号： C10M159/20
摘要： An overbased alkaline earth metal single-aromatic ring hydrocarbyl salicylate-carboxylate is produced by overbasing a mixture of a single-aromatic ring hydrocarbyl salicylate, at least one solvent, a metal hydroxide, and an alkyl polyhydric alcohol alkaline earth metal hydroxide, by contacting that mixture with carbon dioxide under overbasing reaction conditions. The alkyl group of the alkyl polyhydric alcohol has from one to five carbon atoms. The overbased metal single-aromatic ring hydrocarbyl salicylate is treated, before, during, or subsequent to overbasing, with a long-chain carboxylic acid to form a single-aromatic ring hydrocarbyl salicylate-carboxylate.
摘要翻译：高碱性碱土金属单芳香环烃酸水杨酸酯 - 羧酸盐通过使单芳族环烃基水杨酸酯，至少一种溶剂，金属氢氧化物和烷基多元醇碱土金属氢氧化物的混合物过量制备，在高碱性反应条件下与二氧化碳混合。烷基多元醇的烷基具有1至5个碳原子。高碱性金属单芳香环烃基水杨酸酯在高碱性化之前，之中或之后用长链羧酸处理以形成水杨酸单羧酸酯的单芳香环。

19. 发明授权

US5942476A Low-viscosity highly overbased phenate-carboxylate 失效
标题翻译：低粘度高度高碱性酚盐 - 羧酸盐
公开(公告)号：US5942476A
公开(公告)日：1999-08-24
申请号：US089527
申请日：1998-06-03
申请人： Curt B. Campbell
发明人： Curt B. Campbell
IPC分类号： C10M159/22 , C10M169/04 , C10N30/02
CPC分类号： C10M159/22
摘要： A low-viscosity overbased hydrocarbyl phenate-carboxylate is produced by contacting a mixture of a hydrocarbyl phenate, at least one solvent, metal hydroxide, aqueous metal chloride, and an alkyl polyhydric alcohol containing from one to five carbon atoms with carbon dioxide under overbasing reaction conditions. The hydrocarbyl phenate is treated with a long-chain carboxylic acid, anhydride or salt thereof to form the hydrocarbyl phenate-carboxylate before, during, or subsequent to overbasing. The hydrocarbyl phenate can be sulfurized or unsulfurized.
摘要翻译：通过使酚基酚盐，至少一种溶剂，金属氢氧化物，含水金属氯化物和含有1至5个碳原子的烷基多元醇与二氧化碳在高碱性反应下的混合物接触来制备低粘度高碱性烃基酚盐 - 羧酸盐条件。在高碱性化之前，期间或之后，用长链羧酸，酸酐或其盐处理烃基酚盐以形成酚盐 - 羧酸烃基酯。烃基酚盐可以被硫化或未硫化。

20. 发明授权

US5728657A Production of low fine sediment high TBN phenate stearate 失效
标题翻译：生产低细小沉积物高TBN酚盐硬脂酸酯
公开(公告)号：US5728657A
公开(公告)日：1998-03-17
申请号：US869514
申请日：1997-06-05
申请人： Curt B. Campbell , Christopher S. Fridia
发明人： Curt B. Campbell , Christopher S. Fridia
IPC分类号： C10M159/20 , C10M159/22
CPC分类号： C10M159/20 , C10M159/22
摘要： An overbased phenate stearate is produced by overbasing a mixture that comprises sulfurized phenate, metal stearate (such as calcium stearate), at least one solvent, calcium hydroxide, and water, by contacting the mixture with carbon dioxide in the presence of an alkyl polyhydric alcohol, such as ethylene glycol. The level of agitation is maintained at a level sufficiently high so that all solids are suspended over the length of the overbasing step. The polyhydric alcohol to water ratio is maintained sufficiently high so that the ratio is at least 4:1 at the end of the overbasing step. The overbased mixture is stripped to produce an overbased phenate stearate having less than 0.10 vol. % fine sediments.
摘要翻译：通过使含有硫化酚盐，硬脂酸金属盐（例如硬脂酸钙），至少一种溶剂，氢氧化钙和水的混合物过饱和，通过使该混合物与二氧化碳在烷基多元醇的存在下接触来制备高碱性酚盐硬脂酸盐，如乙二醇。搅拌水平保持在足够高的水平，使得所有固体悬浮在高碱性步骤的长度上。多元醇与水的比率保持足够高，使得在高碱性步骤结束时该比例至少为4:1。剥去高碱性混合物以制备具有小于0.10体积％的高碱性酚酸酯硬脂酸酯。％细小的沉积物。

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