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11. 发明授权

US09315626B2 Process for preparing polyamides 有权
标题翻译：制备聚酰胺的方法
公开(公告)号：US09315626B2
公开(公告)日：2016-04-19
申请号：US13514364
申请日：2010-12-03
申请人： Faissal-Ali El-Toufaili , Philippe Desbois , Andreas Wollny , Sven Lawrenz , Christian Schmidt
发明人： Faissal-Ali El-Toufaili , Philippe Desbois , Andreas Wollny , Sven Lawrenz , Christian Schmidt
IPC分类号： C08G69/24 , C08G69/26 , C08G69/28
CPC分类号： C08G69/265 , C08G69/28
摘要： The present invention relates to a process for preparing a polyamide based on dicarboxylic acids and diamines, comprising the following stages: A) providing an aqueous monomer mixture composed of dicarboxylic acids and diamines, where the molar ratio of dicarboxylic acids to diamines is adjusted such that, at the outlet of stage C), there is a molar deficiency of dicarboxylic acids or diamines of 1 to 10 mol %, based on the respective other component, B) transferring the aqueous mixture from stage A) into a continuous evaporator reactor in which diamines and dicarboxylic acids are converted at a temperature in the range from 100 to 370° C. and a pressure in the range from 1 to 50 bar, C) transferring the mixture from stage B) into a separator which is operated at a temperature in the range from 100 to 370° C. and a pressure in the range from 1 to 50 bar with removal of gaseous components, D) transferring the mixture from stage C) together with diamine or dicarboxylic acid in an amount suitable for compensation for the molar deficiency into a tubular reactor which is operated at a temperature in the range from 100 to 370° C. and a pressure in the range from 1 to 50 bar, for a residence time in the range from 10 seconds to 30 minutes, E) transferring the mixture from stage D) into an extruder which is operated at a temperature in the range from 150 to 400° C. for a residence time in the range from 10 seconds to 30 minutes with removal of gaseous components through venting orifices.
摘要翻译：本发明涉及一种制备基于二羧酸和二胺的聚酰胺的方法，其包括以下步骤：A）提供由二羧酸和二胺组成的含水单体混合物，其中二羧酸与二胺的摩尔比被调整为使得，在阶段C）的出口处，基于各自的其它组分，存在摩尔不足的二羧酸或二胺的1至10摩尔％，B）将水性混合物从阶段A）转移到连续的蒸发器反应器中，其中二胺和二羧酸在100至370℃的温度和1至50巴的压力范围内转化，C）将混合物从阶段B）转移到分离器中，该分离器在范围为100至370℃，压力范围为1至50巴，除去气态组分，D）将混合物从阶段C）与二胺或二羧酸一起转移 t适用于将摩尔不足补偿为在100至370℃的温度和1至50巴的压力范围内操作的管式反应器中，停留时间为10秒至30分钟，E）将混合物从阶段D）转移到挤出机中，该挤出机在150-400℃的温度下操作，停留时间为10秒至30分钟，同时除去气体组分通过通风口。

12. 发明授权

US08957133B2 Polyamide moldings comprising microencapsulated latent-heat-accumulator material 有权
标题翻译：聚酰胺模制品包括微胶囊潜热蓄热材料
公开(公告)号：US08957133B2
公开(公告)日：2015-02-17
申请号：US13184863
申请日：2011-07-18
申请人： Philippe Desbois , Tina Schröder-Grimonpont , Stephan Altmann , Marco Schmidt
发明人： Philippe Desbois , Tina Schröder-Grimonpont , Stephan Altmann , Marco Schmidt
IPC分类号： C08K9/10 , C08L77/02 , C08L1/00 , C08G69/18 , C08G69/24
CPC分类号： C08L1/00 , C08G69/18 , C08G69/24 , C08K5/01 , C08L33/06 , C08L77/02
摘要： The present invention relates to polyamide moldings obtainable via anionic polymerization of a lactam comprising microcapsules with a capsule core made of latent-heat-accumulator material and a polymer as capsule wall, to a process for producing the same, and also to the use of the same in motor-vehicle construction, as battery housing, as housing for small electronic devices, and for heat-retention systems for foods.
摘要翻译：本发明涉及通过由包含由潜热蓄热材料制成的胶囊芯的微胶囊和具有胶囊壁的聚合物的内酰胺的阴离子聚合得到的聚酰胺成型品，其制造方法，以及使用机动车辆结构相同，电池外壳，小型电子设备的外壳以及食品的保温系统。

13. 发明授权

US08759476B2 Method for producing polyamides 有权
标题翻译：生产聚酰胺的方法
公开(公告)号：US08759476B2
公开(公告)日：2014-06-24
申请号：US12665564
申请日：2008-06-12
申请人： Philippe Desbois , Hagen Stawitzki , Ralf Neuhaus , Hans-Joachim Weis , Jurgen Weichmann , Racquel Fernandez Rodiles , Gunter Vogel
发明人： Philippe Desbois , Hagen Stawitzki , Ralf Neuhaus , Hans-Joachim Weis , Jurgen Weichmann , Racquel Fernandez Rodiles , Gunter Vogel
IPC分类号： C08G69/26
CPC分类号： C08G69/26 , C08G69/265 , C08G69/28
摘要： The process for preparing a polyamide based on dicarboxylic acids and diamines has the following stages: 1) providing an aqueous monomer mixture of dicarboxylic acids and diamines, the molar ratio of dicarboxylic acids to diamines being adjusted such that a molar deficiency of dicarboxylic acids or diamines of from 1 to 10 mol % is present at the outlet of stage 3), based on the other component in each case, 2) transferring the aqueous mixture from stage 1) to a continuous evaporator reactor in which diamines and dicarboxylic acids are reacted at a temperature in the range from 100 to 370° C. and a pressure in the range from 1 to 50 bar, 3) transferring the mixture from stage 2) to a separator which is operated at a temperature in the range from 100 to 370° C. with removal of gaseous components, 4) transferring the mixture from stage 3) together with diamine or dicarboxylic acid in an amount suitable to balance out the molar deficiency into an extruder which is operated at a temperature in the range from 150 to 400° C. for a residence time in the range from 10 seconds to 30 minutes to remove gaseous components through devolatilizing orifices.
摘要翻译：基于二羧酸和二胺制备聚酰胺的方法具有以下阶段：1）提供二羧酸和二胺的单体混合物，二羧酸与二胺的摩尔比被调节，使得二羧酸或二胺的摩尔不足在阶段3）的出口处存在1至10摩尔％，基于每种情况下的其它组分，2）将水性混合物从阶段1）转移到连续的蒸发器反应器中，其中二胺和二羧酸在温度范围为100至370℃，压力范围为1至50巴，3）将混合物从阶段2转移至分离器，该分离器的运行温度范围为100至370℃ C.去除气体组分，4）将来自级3）的混合物与二胺或二羧酸一起转移，其量适合于将摩尔不足量平衡到在温度下操作的挤出机在150至400℃的范围内，停留时间在10秒至30分钟的范围内，以通过脱挥发泡孔除去气体组分。

14. 发明申请

US20140142274A1 SOLID PARTICLES, CONTAINING LACTAM, ACTIVATOR, AND CATALYST, METHOD FOR PRODUCING SAID SOLID PARTICLES, AND USE OF SAID SOLID PARTICLES 审中-公开
标题翻译：固体颗粒，含乳胶，活化剂和催化剂，生产固体颗粒的方法和使用固体颗粒
公开(公告)号：US20140142274A1
公开(公告)日：2014-05-22
申请号：US14131088
申请日：2012-07-02
申请人： Philippe Desbois , Silke Biedasek , Andreas Wollny
发明人： Philippe Desbois , Silke Biedasek , Andreas Wollny
IPC分类号： C08G69/20
CPC分类号： C08G69/20 , C08G69/18 , C08G69/24
摘要： The present invention relates to solid particles which comprise at least one lactam, and also at least one activator, and at least one catalyst, to a process for the production of these, and also to the use of these for the production of polyamide, and to a process for the production of polyamide.
摘要翻译：本发明涉及包含至少一种内酰胺，以及至少一种活化剂和至少一种催化剂的固体颗粒，涉及制备这些催化剂的方法，以及这些用于生产聚酰胺的方法，以及涉及生产聚酰胺的方法。

15. 发明申请

US20130065466A1 USE OF POLYETHYLENEIMINES IN THE PREPARATION OF POLYAMIDES 有权
标题翻译：聚乙烯在制备聚氨酯中的应用
公开(公告)号：US20130065466A1
公开(公告)日：2013-03-14
申请号：US13612382
申请日：2012-09-12
申请人： Philippe Desbois , Andreas Wollny , Andreas Radtke , Bernd Bruchmann , Anna Karina Möller
发明人： Philippe Desbois , Andreas Wollny , Andreas Radtke , Bernd Bruchmann , Anna Karina Möller
IPC分类号： B32B27/34 , B32B27/04 , B29C45/14 , B32B5/02 , C09K3/00 , C08G69/04
CPC分类号： B32B5/024 , B32B5/028 , B32B5/12 , B32B5/26 , B32B5/28 , B32B2250/05 , B32B2250/20 , B32B2260/023 , B32B2260/046 , B32B2262/0269 , B32B2262/101 , B32B2262/106 , C08G69/16 , C08G69/18 , C08L39/04 , Y10T442/184 , Y10T442/191 , Y10T442/20 , Y10T442/30 , Y10T442/40 , Y10T442/60 , Y10T442/697
摘要： The present invention relates to a process for preparing a composition comprising (A) at least one lactam, (B) at least one catalyst, (C) an activator from the group consisting of isocyanates, acid anhydrides, acyl halides, reaction products thereof with (A) and mixtures thereof, (D) at least one polyethyleneimine. The invention likewise relates to a composition comprising (i) 0.01 to 10 wt %, based on the sum total of components (A) and (D), of at least one polyethyleneimine, and (ii) 90 to 99.99 wt %, based on the sum total of components (A) and (D), of at least one lactam (A) and/or polyamide obtainable from (A).
摘要翻译：本发明涉及一种制备组合物的方法，该组合物包含（A）至少一种内酰胺，（B）至少一种催化剂，（C）来自异氰酸酯，酸酐，酰基卤的活化剂，其反应产物与（A）及其混合物，（D）至少一种聚乙烯亚胺。本发明同样涉及一种组合物，其包含（i）基于组分（A）和（D）的总和为至少一种聚乙烯亚胺的0.01至10重量％，和（ii）90至99.99重量％，基于由（A）得到的至少一种内酰胺（A）和/或聚酰胺的组分（A）和（D）的总和。

16. 发明申请

US20120245283A1 SEMI-AROMATIC, SEMI-CRYSTALLINE COPOLYAMIDES 有权
标题翻译：半自动，半结晶共聚酰胺
公开(公告)号：US20120245283A1
公开(公告)日：2012-09-27
申请号：US13514445
申请日：2010-12-07
申请人： Philippe Desbois , Andreas Wollny
发明人： Philippe Desbois , Andreas Wollny
IPC分类号： C08L77/10
CPC分类号： C08G69/265 , C08G69/26 , C08L77/06
摘要： Semiaromatic, semicrystalline copolyamide molding compositions, comprisingA) from 35 to 100% by weight of a copolyamide composed of a1) from 35 to 69% by weight of units which derive from hexamethylenediamine and from an aromatic dicarboxylic acid having from 8 to 16 carbon atoms, a2) from 31 to 65% by weight of units which derive from 3,3′-dimethyl-4,4′-diaminodicyclohexylmethane and from terephthalic acid, a3) from 0 to 30% by weight of units of a semicrystalline polyamide different from a1) and a2), B) from 0 to 65% by weight of further additives, where the total of the percentages by weight of A) and B) is 100%.
摘要翻译：半芳族半结晶共聚酰胺模塑组合物，其包含A）35-100％重量的共聚酰胺，该共聚酰胺由a1- 35-69％（重量）衍生自六亚甲基二胺的单元和具有8至16个碳原子的芳族二羧酸组成，a2）31至65重量％的衍生自3,3'-二甲基-4,4'-二氨基二环己基甲烷和来自对苯二甲酸的单元，a3）0至30重量％的半结晶聚酰胺单元不同于 a1）和a2），B）0至65重量％的其它添加剂，其中A）和B）的重量百分比的总和为100％。

17. 发明申请

US20120225995A1 USE OF VINYLAROMATIC-DIENE COPOLYMERS IN LACTAM COMPOSITIONS 有权
标题翻译：在LACTAM组合物中使用乙烯基二烯共聚物
公开(公告)号：US20120225995A1
公开(公告)日：2012-09-06
申请号：US13408298
申请日：2012-02-29
申请人： Philippe Desbois , Konrad Knoll , Anna Karina Möller
发明人： Philippe Desbois , Konrad Knoll , Anna Karina Möller
IPC分类号： C08L53/02
CPC分类号： C08L77/02 , C08G69/18 , C08L53/02
摘要： A lactam composition which comprises the following components: from 3 to 25% by weight of a random vinylaromatic-diene copolymer (A), where the random vinylaromatic-diene copolymer is composed of at least one block (S) which forms a hard phase and which is composed of vinylaromatic monomers, and of at least one random block (S/B) which forms a soft phase and which has vinylaromatic monomers and diene monomers, from 75 to 97% by weight of at least one lactam component (B), and also optionally reinforcing materials and/or additives has improved viscosity in the melt and can be used for producing polyamide moldings.
摘要翻译：一种内酰胺组合物，其包含以下组分：3至25重量％的无规乙烯基芳族二烯共聚物（A），其中无规乙烯基芳族二烯共聚物由至少一个形成硬相的嵌段（S）和由乙烯基芳族单体和形成软相的至少一种无规嵌段（S / B）组成，并且具有乙烯基芳族单体和二烯单体，75至97重量％的至少一种内酰胺组分（B），并且还可选地，增强材料和/或添加剂在熔体中具有改善的粘度，并且可用于生产聚酰胺模制品。

18. 发明申请

US20120088048A1 Process for producing fiber-reinforced composite materials 审中-公开
标题翻译：生产纤维增强复合材料的工艺
公开(公告)号：US20120088048A1
公开(公告)日：2012-04-12
申请号：US13267628
申请日：2011-10-06
申请人： Dietrich Scherzer , Philippe Desbois , Uwe Gleiter , Martin Weber , Michael Gall
发明人： Dietrich Scherzer , Philippe Desbois , Uwe Gleiter , Martin Weber , Michael Gall
IPC分类号： B32B5/02 , B32B1/00 , C09D177/02 , C08G69/26 , C09D177/06 , B29C70/30 , C08G69/14
CPC分类号： C08J5/04 , B29B15/12 , B29B15/127 , B29C70/48 , B29K2077/00 , B32B2262/101 , B32B2377/00 , B32B2437/04 , C08G69/14 , C08G69/26 , C08J2377/00 , C08L2205/02 , C09D177/02 , C09D177/06 , Y10T428/1362 , Y10T442/20 , C08L77/00 , C08L77/06
摘要： The present invention relates to binders for the preforming process to which textile structures are subjected when structural materials are produced by the RIM or RTM method, where the binder composed of an amorphous polyimide is spray applied in a solvent onto the textile structure or onto the textile, and is used as binder for the preforming process. The present invention further relates to a process for producing moldings made of fiber-reinforced composite materials.
摘要翻译：本发明涉及当通过RIM或RTM方法制造结构材料时织物结构受到的预成型方法的粘合剂，其中将由无定形聚酰亚胺组成的粘合剂在溶剂中喷涂到织物结构上或织物上，并用作预成型工艺的粘合剂。本发明还涉及由纤维增强复合材料制成的模制品的制造方法。

19. 发明申请

US20080015303A1 Flowable Polyamides With Hyperbranched Polyesters/Polycarbonates 审中-公开
标题翻译：具有超支化聚酯/聚碳酸酯的可流动聚酰胺
公开(公告)号：US20080015303A1
公开(公告)日：2008-01-17
申请号：US11577590
申请日：2005-10-14
申请人： Peter Eibeck , Bernd Bruchmann , Andreas Eipper , Jean-Francois Stumbe , Ralf Neuhaus , Michael Fischer , Jochen Engelmann , Philippe Desbois
发明人： Peter Eibeck , Bernd Bruchmann , Andreas Eipper , Jean-Francois Stumbe , Ralf Neuhaus , Michael Fischer , Jochen Engelmann , Philippe Desbois
IPC分类号： C08L69/00
CPC分类号： C08L67/00 , C08L69/00 , C08L77/00 , C08L77/02 , C08L77/06 , C08L2666/20 , C08L2666/18
摘要： Thermoplastic molding compositions, comprising A) from 10 to 99% by weight of at least one thermoplastic polyamide, B) from 0.01 to 50% by weight of B1) at least one highly branched or hyperbranched polycarbonate with an OH number of from 1 to 600 mg KOH/g of polycarbonate (to DIN 53240, Part 2), or B2) at least one highly branched or hyperbranched polyester of AxBy type, where x is at least 1.1 and y is at least 2.1, or a mixture of these, C) from 0 to 60% by weight of other additives, where the total of the percentages by weight of components A) to C) is 100%.
摘要翻译：热塑性模塑组合物，其包含A）10至99重量％的至少一种热塑性聚酰胺，B）0.01至50重量％的B1）至少一种高度支化或超支化聚碳酸酯，OH数为1至600 mg KOH / g聚碳酸酯（根据DIN 53240第2部分）或B2）至少一种高度支化或超支化的A x B B y Y y型聚酯，其中x为至少1.1，y为至少2.1，或这些的混合物，C）0至60重量％的其它添加剂，其中组分A）至C）的重量百分比的总和为100％。

20. 发明申请

US20060058177A1 Initiator composition and method for anionic polymerisation 失效
标题翻译：用于阴离子聚合的引发剂组合物和方法
公开(公告)号：US20060058177A1
公开(公告)日：2006-03-16
申请号：US10512444
申请日：2003-04-15
申请人： Philippe Desbois , Christian Schade , Alain Deffieux , Stephane Menoret , Jurgen Demeter
发明人： Philippe Desbois , Christian Schade , Alain Deffieux , Stephane Menoret , Jurgen Demeter
IPC分类号： C08F4/46 , C08F36/00 , B01J31/00
CPC分类号： C08F297/04 , C07F5/062 , C08F4/54 , C08F36/04 , C08L53/02 , C08F4/52 , C08F4/48 , C08L2666/02
摘要： The invention relates to an initiator composition for anionic polymerization, comprising at least one alkali metal hydride selected from LiH, NaH, and KH, and at least one organylaluminum compound, and to a process for the anionic polymerization of styrene monomers or of diene monomers using the initiator composition.
摘要翻译：本发明涉及用于阴离子聚合的引发剂组合物，其包含至少一种选自LiH，NaH和KH的碱金属氢化物和至少一种有机铝化合物，以及使用苯乙烯单体或二烯单体进行阴离子聚合的方法，该方法使用引发剂组合物。

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