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11. 发明授权

US09169445B2 Process, method, and system for removing heavy metals from oily solids 有权
标题翻译：从油性固体中除去重金属的工艺，方法和系统
公开(公告)号：US09169445B2
公开(公告)日：2015-10-27
申请号：US13804662
申请日：2013-03-14
申请人： Russell Evan Cooper , Dennis John O'Rear , Seyi Abiodun Odueyungbo
发明人： Russell Evan Cooper , Dennis John O'Rear , Seyi Abiodun Odueyungbo
IPC分类号： C07C7/11 , C10G21/08 , C10G31/09 , C10G53/02 , C10G1/04
CPC分类号： C10G21/08 , C10G1/04 , C10G31/09 , C10G53/02 , C10G2300/202
摘要： Oil is recovered from a mercury containing oily solids by mixing the solids with at least a treating agent selected from selected from flocculants, sulfidic compounds, demulsifiers, and combinations thereof, and optionally a solvent, forming a mixture. The mixture is then separated to recover a first phase containing treated oil having less than 50% of the original amount of mercury in the oily solids, and a second phase containing treated solids having a reduced concentration of mercury. In one embodiment, the oily solids comprise filter aid materials, e.g., diatomaceous earth filter media, removed from a mercury removal filtration unit by backflushing the filter.
摘要翻译：通过将固体与至少一种选自絮凝剂，硫化合物，破乳剂及其组合的处理剂以及任选的溶剂混合形成混合物，从含汞油状固体中回收油。然后将混合物分离以回收含有少于油状固体中原始汞含量的50％的经处理的油的第一相，以及含有具有降低的汞浓度的经处理的固体的第二相。在一个实施方案中，油性固体包含过滤助剂材料，例如硅藻土过滤介质，通过反吹过滤器从除汞过滤单元中除去。

12. 发明授权

US08840691B2 Process, method, and system for removing mercury from fluids 有权
公开(公告)号：US08840691B2
公开(公告)日：2014-09-23
申请号：US14020293
申请日：2013-09-06
申请人： Russell Evan Cooper , Dennis John O'Rear , Feng-Ran Sheu , Jordan Taylor Belue
发明人： Russell Evan Cooper , Dennis John O'Rear , Feng-Ran Sheu , Jordan Taylor Belue
IPC分类号： C10L3/10
CPC分类号： C10L3/101 , B01D53/1462 , B01D53/1493 , B01D2252/2023 , B01D2252/20484 , B01D2252/20489 , B01D2252/602 , B01D2256/245 , B01D2257/602 , B01D2257/80 , C10G5/00 , C10L3/102 , C10L3/105 , C10L3/106
摘要： Trace levels of mercury in a natural gas are removed in a gas processing plant in an amine unit and/or a dehydrator. The mercury removal occurs concurrently with the removal of acid gases in an amine unit, e.g., an absorber or scrubber, with an amine solution containing a complexing agent. The mercury removal can also be carried out concurrently with the removal of water in a glycol dehydrator with the addition of a complexing agent to the glycol solution. Volatile mercury in the natural gas is removed by the complexing agent, forming non-volatile mercury species in the rich amine/glycol solution.

13. 发明申请

US20140275694A1 Process, Method, and System for Removing Heavy Metals from Oily Solids 有权
标题翻译：从油性固体中去除重金属的工艺，方法和系统
公开(公告)号：US20140275694A1
公开(公告)日：2014-09-18
申请号：US13804662
申请日：2013-03-14
申请人： Russell Evan Cooper , Dennis John O'Rear , Seyi Abiodun Odueyungbo
发明人： Russell Evan Cooper , Dennis John O'Rear , Seyi Abiodun Odueyungbo
IPC分类号： C10G21/08 , C07C7/11
CPC分类号： C10G21/08 , C10G1/04 , C10G31/09 , C10G53/02 , C10G2300/202
摘要： Oil is recovered from a mercury containing oily solids by mixing the solids with at least a treating agent selected from selected from flocculants, sulfidic compounds, demulsifiers, and combinations thereof, and optionally a solvent, forming a mixture. The mixture is then separated to recover a first phase containing treated oil having less than 50% of the original amount of mercury in the oily solids, and a second phase containing treated solids having a reduced concentration of mercury. In one embodiment, the oily solids comprise filter aid materials, e.g., diatomaceous earth filter media, removed from a mercury removal filtration unit by backflushing the filter.
摘要翻译：通过将固体与至少一种选自絮凝剂，硫化合物，破乳剂及其组合的处理剂以及任选的溶剂混合形成混合物，从含汞油状固体中回收油。然后将混合物分离以回收含有少于油状固体中原始汞含量的50％的经处理的油的第一相，以及含有具有降低的汞浓度的经处理的固体的第二相。在一个实施方案中，油性固体包含过滤助剂材料，例如硅藻土过滤介质，通过反吹过滤器从除汞过滤单元中除去。

14. 发明申请

US20140275665A1 Process, Method, and System for Removing Heavy Metals from Oily Solids 审中-公开
标题翻译：从油性固体中去除重金属的工艺，方法和系统
公开(公告)号：US20140275665A1
公开(公告)日：2014-09-18
申请号：US13804172
申请日：2013-03-14
申请人： Dennis John O'Rear , Russell Evan Cooper , Fan-Sheng Teddy Tao , Ronald Hobbs
发明人： Dennis John O'Rear , Russell Evan Cooper , Fan-Sheng Teddy Tao , Ronald Hobbs
IPC分类号： C10G1/00
CPC分类号： C10G1/002 , C10G1/045
摘要： Oil is recovered from a mercury containing oily solids by mixing the solids with at least a treating agent selected from selected from flocculants, sulfidic compounds, demulsifiers, and combinations thereof, and optionally a solvent, forming a mixture. The mixture is then separated to recover a first phase containing treated oil having less than 50% of the original amount of mercury in the oily solids, and a second phase containing treated solids having a reduced concentration of mercury. The oily solids are selected from drilling muds; oily sediments coating inside of pipelines; sediment deposits on crude oil tanks, vessels, and separators; surface coating on equipment; slop oil from upstream operations; oily solids from heavy oil processing operations; solids recovered from processes for removing mercury from hydrocarbon materials; spill clean-up materials; and mixtures thereof.
摘要翻译：通过将固体与至少一种选自絮凝剂，硫化合物，破乳剂及其组合的处理剂以及任选的溶剂混合形成混合物，从含汞油状固体中回收油。然后将混合物分离以回收含有少于油状固体中原始汞含量的50％的经处理的油的第一相，以及含有具有降低的汞浓度的经处理的固体的第二相。油状固体选自钻井泥浆; 管道内部含油沉积物; 原油罐，船舶和分离器上的沉积物沉积物; 设备表面涂层; 上游作业油; 重油加工作业的油性固体; 从烃类材料中除去汞的方法中回收的固体; 溢出清理材料; 及其混合物。

15. 发明申请

US20140206915A1 PARAFFINIC JET AND DIESEL FUELS AND BASE OILS FROM VEGETABLE OILS VIA A COMBINATION OF HYDROTREATING, PARAFFIN DISPROPORTIONATION AND HYDROISOMERIZATION 审中-公开
标题翻译：通过加氢，分离分解和水解的组合，来自植物油的PARAFFINIC喷射和柴油燃料和基础油
公开(公告)号：US20140206915A1
公开(公告)日：2014-07-24
申请号：US13841226
申请日：2013-03-15
申请人： Cong-Yan Chen , Dennis John O'Rear , Thomas Francis Finger , Stephen Joseph Miller , Alexander Kuperman
发明人： Cong-Yan Chen , Dennis John O'Rear , Thomas Francis Finger , Stephen Joseph Miller , Alexander Kuperman
IPC分类号： C10G3/00
CPC分类号： C07C6/04 , B01J23/30 , B01J23/58 , B01J23/6527 , B01J35/0006 , B01J37/0201 , C07C5/03 , C07C5/2775 , C07C5/333 , C07C6/00 , C07C6/02 , C07C6/08 , C07C2523/652 , C07C2529/85 , C10G3/42 , C10G3/44 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1011 , C10G2300/1014 , C10G2300/1018 , C10G2400/02 , C10G2400/04 , C10G2400/08 , C10G2400/10 , C10L1/04 , C10L1/08 , C10L2200/0469 , C10L2270/026 , C10L2270/04 , Y02E50/13 , Y02P30/20
摘要： The present invention relates to a new process which comprises the steps of hydrotreating, paraffin disproportionation and hydroisomerization to convert biological hydrocarbonaceous oxygenated oils comprising triglycerides into biologically-derived paraffinic jet/diesel fuels, solvents and base oils. A combination of conventional hydrogenation/dehydrogenation catalysts, such as Pt/Al2O3, and conventional olefin metathesis catalysts, such as WO3/SiO2, or inexpensive variations thereof, is generally employed in the paraffin disproportionation step.
摘要翻译：本发明涉及一种新方法，其包括加氢处理，石蜡歧化和加氢异构化以将包含甘油三酯的生物烃类含氧油转化为生物衍生的链烷烃喷射/柴油燃料，溶剂和基础油的步骤。常规的氢化/脱氢催化剂如Pt / Al 2 O 3和常规的烯烃复分解催化剂如WO 3 / SiO 2或其便宜的变体的组合通常用于石蜡歧化步骤。

16. 发明申请

US20130306311A1 PROCESS, METHOD, AND SYSTEM FOR REMOVING MERCURY FROM FLUIDS 有权
标题翻译：从流体中去除汞的方法，方法和系统
公开(公告)号：US20130306311A1
公开(公告)日：2013-11-21
申请号：US13895754
申请日：2013-05-16
申请人： Russell Evan Cooper , Dennis John O'Rear , Darrell Lynn Gallup , Lyman Arnold Young , Sujin Yean
发明人： Russell Evan Cooper , Dennis John O'Rear , Darrell Lynn Gallup , Lyman Arnold Young , Sujin Yean
IPC分类号： C10G21/08 , E21B43/40 , E21B43/34
CPC分类号： C10G21/08 , B01D53/64 , B01D2257/602 , C10G2300/201 , C10G2300/205 , E21B43/34 , E21B43/40
摘要： Trace amount levels of non-volatile mercury in crude oil are reduced by contacting the crude oil with a water stream containing at least a monatomic water-soluble sulfur species such as sulfides and hydrosulfides. The non-volatile mercury is extracted into the water phase forming a mercury rich wastewater, yielding a treated crude oil having at less than 50% of the original non-volatile mercury level. The wastewater can disposed or recycled by injection into a reservoir. In one embodiment, the water stream consists essentially of produced water.
摘要翻译：通过使原油与至少含有单原子水溶性硫物质如硫化物和氢硫化物的水流接触来降低原油中微量的非挥发性汞。非挥发性汞被提取到水相中，形成富含汞的废水，产生的处理原油的含量低于原始非挥发性汞含量的50％。废水可以通过注入设置或回收到储存器中。在一个实施方案中，水流基本上由生产的水组成。

17. 发明授权

US09234141B2 Process, method, and system for removing heavy metals from oily solids 有权
标题翻译：从油性固体中除去重金属的工艺，方法和系统
公开(公告)号：US09234141B2
公开(公告)日：2016-01-12
申请号：US13804430
申请日：2013-03-14
申请人： Dennis John O'Rear , Russell Evan Cooper , Kevin John Grice
发明人： Dennis John O'Rear , Russell Evan Cooper , Kevin John Grice
IPC分类号： C10G21/08
CPC分类号： C10G21/08 , C10G1/04 , C10G1/042 , C10G1/045
摘要： Oil is recovered from a mercury containing Hg-containing solids containing abradants by mixing the solids with a sulfidic compound in a molar ratio of sulfur compound to mercury from 5:1 to 5,000:1, and the sulfidic compound when dissolved in water, yields S2-, SH—, Sx2-, or SxH— anions, and optionally a solvent, forming a mixture. The mixture is then separated to recover a first phase containing treated oil in water, and a second phase containing treated abradants having a reduced concentration of mercury. In one embodiment, the treated abradants contain less than 100 ppmw mercury. The abradants are provided by removing at least a portion of a mercury-containing coating from a surface by abradant blasting, laser ablation, laser thermal desorption, and sponge jet blasting.
摘要翻译：通过将硫化合物与硫化合物与汞的摩尔比为5:1至5,000:1混合固体和溶解在水中的硫化合物，从含有汞的含汞固体含有研磨剂中回收油，得到S2 - ，SH-，Sx2-或SxH-阴离子，和任选的溶剂，形成混合物。然后分离混合物以回收含水中处理过的油的第一相，以及含有具有降低的汞浓度的经处理的研磨剂的第二相。在一个实施方案中，经处理的研磨剂含有小于100ppmw的汞。通过研磨喷砂，激光烧蚀，激光热解吸和海绵喷射喷砂，从表面除去至少一部分含汞涂层来提供研磨剂。

18. 发明授权

US09199898B2 Process, method, and system for removing heavy metals from fluids 有权
标题翻译：从流体中除去重金属的工艺，方法和系统
公开(公告)号：US09199898B2
公开(公告)日：2015-12-01
申请号：US14013843
申请日：2013-08-29
申请人： Dennis John O'Rear , Russell Evan Cooper , Feng-Ran Sheu , Jordan Taylor Belue
发明人： Dennis John O'Rear , Russell Evan Cooper , Feng-Ran Sheu , Jordan Taylor Belue
IPC分类号： C07C7/152 , C10G29/04 , C10G21/22 , C10L3/10
CPC分类号： C07C7/152 , C10G21/22 , C10L3/101 , C10L3/107
摘要： A method for concurrently transporting and removing trace amount levels of heavy metals such as mercury from produced fluids such as natural gas, with the injection of a complexing agent and a hydrate inhibitor into the pipeline for use in transporting the produced fluid. Volatile mercury in the natural gas is removed while the produced fluid is being transported in the pipeline, with the hydrate inhibitor suppressing or decreasing the formation of the hydrate that would cause plugging in the pipeline. The complexing agent reacts with the volatile mercury in the natural gas, forming precipitate or soluble mercury complexes in the aqueous phase. The aqueous phase containing the hydrate inhibitor, unreacted complexing agent, and mercury complexes is subsequently recovered and can be re-used in the pipeline.
摘要翻译：一种从生产的流体如天然气中同时输送和除去痕量的重金属如汞的方法，其中将络合剂和水合物抑制剂注入到用于输送所产生的流体的管道中。当生产的流体在管道中运输时，天然气中的挥发性汞被除去，水合物抑制剂抑制或减少将导致管道堵塞的水合物的形成。络合剂与天然气中的挥发性汞反应，在水相中形成沉淀物或可溶性汞络合物。随后回收含有水合物抑制剂，未反应的络合剂和汞络合物的水相，并可在管道中重新使用。

19. 发明申请

US20150266796A1 PARAFFINIC JET AND DIESEL FUELS AND BASE OILS FROM VEGETABLE OILS VIA A COMBINATION OF HYDROTREATING, PARAFFIN DISPROPORTIONATION AND HYDROISOMERIZATION 审中-公开
标题翻译：通过加氢，分离分解和水解的组合，来自植物油的PARAFFINIC喷射和柴油燃料和基础油
公开(公告)号：US20150266796A1
公开(公告)日：2015-09-24
申请号：US14729831
申请日：2015-06-03
申请人： Cong-Yan CHEN , Dennis John O'REAR , Thomas Francis FINGER , Stephen Joseph MILLER , Alexander KUPERMAN
发明人： Cong-Yan CHEN , Dennis John O'REAR , Thomas Francis FINGER , Stephen Joseph MILLER , Alexander KUPERMAN
IPC分类号： C07C6/04 , C07C5/27 , C10L1/08 , C07C5/03 , C10L1/04 , C10G3/00 , C07C5/333
CPC分类号： C07C6/04 , B01J23/30 , B01J23/58 , B01J23/6527 , B01J35/0006 , B01J37/0201 , C07C5/03 , C07C5/2775 , C07C5/333 , C07C6/00 , C07C6/02 , C07C6/08 , C07C2523/652 , C07C2529/85 , C10G3/42 , C10G3/44 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1011 , C10G2300/1014 , C10G2300/1018 , C10G2400/02 , C10G2400/04 , C10G2400/08 , C10G2400/10 , C10L1/04 , C10L1/08 , C10L2200/0469 , C10L2270/026 , C10L2270/04 , Y02P30/20
摘要： The present invention relates to a new process which comprises the steps of hydrotreating, paraffin disproportionation and hydroisomerization to convert biological hydrocarbonaceous oxygenated oils comprising triglycerides into biologically-derived paraffinic jet/diesel fuels, solvents and base oils. A combination of conventional hydrogenation/dehydrogenation catalysts, such as Pt/Al2O3, and conventional olefin metathesis catalysts, such as WO3/SiO2, or inexpensive variations thereof, is generally employed in the paraffin disproportionation step.
摘要翻译：本发明涉及一种新方法，其包括加氢处理，石蜡歧化和加氢异构化以将包含甘油三酯的生物烃类含氧油转化为生物衍生的链烷烃喷射/柴油燃料，溶剂和基础油的步骤。常规的氢化/脱氢催化剂如Pt / Al 2 O 3和常规的烯烃复分解催化剂如WO 3 / SiO 2或其便宜的变体的组合通常用于石蜡歧化步骤。

20. 发明授权

US09023196B2 Process, method, and system for removing heavy metals from fluids 有权
标题翻译：从流体中除去重金属的工艺，方法和系统
公开(公告)号：US09023196B2
公开(公告)日：2015-05-05
申请号：US13826213
申请日：2013-03-14
申请人： Russell Evan Cooper , Dennis John O'Rear , Sujin Yean , Seyi Abiodun Odueyungbo
发明人： Russell Evan Cooper , Dennis John O'Rear , Sujin Yean , Seyi Abiodun Odueyungbo
IPC分类号： C10G53/04 , C10G29/02 , C10G27/12
CPC分类号： C10G29/02 , C10G27/10 , C10G27/12 , C10G27/14 , C10G29/10 , C10G29/28 , C10G31/09 , C10G2300/1033 , C10G2300/205
摘要： Trace element levels of mercury in crude oil are reduced by first passing the crude oil through a filtration device to generate filtered crude having a reduced concentration of mercury and a reject stream having a concentrated mercury level. In one embodiment, the filtration device is back-flushed to generate the reject stream. In another embodiment, the reject stream comprises a portion of the retentate from a cross-flow filter device. The reject stream is treated with an extractive agent selected from tetrakis(hydroxymethyl)phosphonium sulfate; tetrakis(hydroxymethyl) phosphonium chloride; an oxidizing agent; an organic or inorganic sulfidic compound to extract a portion of the mercury into a water phase for subsequent removal. In one embodiment, the extractive agent is a reductant to convert non-volatile mercury into volatile mercury.
摘要翻译：通过首先使原油通过过滤装置来降低原油中微量元素汞的水平，以产生具有降低的汞浓度的过滤粗品和具有浓汞水平的废品流。在一个实施例中，过滤装置被反冲洗以产生废品流。在另一个实施方案中，废液流包含来自交叉流过滤装置的一部分滞留物。用选自四（羟甲基）硫酸鏻的萃取剂处理废料流; 氯化四（羟甲基）鏻; 氧化剂; 有机或无机硫化合物，将一部分汞提取到水相中以便随后除去。在一个实施方案中，萃取剂是将非挥发性汞转化成挥发性汞的还原剂。

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