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11. 发明授权

US07279137B2 Burners and combustion apparatus for carbon nanomaterial production 有权
标题翻译：燃烧器和碳纳米材料生产的燃烧装置
公开(公告)号：US07279137B2
公开(公告)日：2007-10-09
申请号：US10098829
申请日：2002-03-15
申请人： J. Michael Alford , Michael D. Diener , James Nabity , Michael Karpuk
发明人： J. Michael Alford , Michael D. Diener , James Nabity , Michael Karpuk
IPC分类号： B01J12/00 , F23D3/40 , F23D14/12
CPC分类号： D01F9/133 , B82Y30/00 , B82Y40/00 , C01B32/15 , C01B32/152 , D01F9/127 , F23D14/02 , F23D99/00 , F23D2203/105 , F23D2900/21007
摘要： The invention provides improved burners, combustion apparatus, and methods for carbon nanomaterial production. The burners of the invention provide sooting flames of fuel and oxidizing gases. The condensable products of combustion produced by the burners of this invention produce carbon nanomaterials including without limitation, soot, fullerenic soot, and fullerenes. The burners of the invention do not require premixing of the fuel and oxidizing gases and are suitable for use with low vapor pressure fuels such as those containing substantial amounts of polyaromatic hydrocarbons. The burners of the invention can operate with a hot (e.g., uncooled) burner surface and require little, if any, cooling or other forms of heat sinking. The burners of the invention comprise one or more refractory elements forming the outlet of the burner at which a flame can be established. The burners of the invention provide for improved flame stability, can be employed with a wider range of fuel/oxidizer (e.g., air) ratios and a wider range of gas velocities, and are generally more efficient than burners using water-cooled metal burner plates. The burners of the invention can also be operated to reduce the formation of undesirable soot deposits on the burner and on surfaces downstream of the burner.
摘要翻译：本发明提供了改进的燃烧器，燃烧装置和用于碳纳米材料生产的方法。本发明的燃烧器提供燃料和氧化气体的燃烧火焰。由本发明的燃烧器产生的燃烧的可冷凝产物产生碳纳米材料，包括但不限于烟灰，富勒烯烟和富勒烯。本发明的燃烧器不需要燃料和氧化气体的预混合，并且适用于低蒸气压燃料，例如含有大量多芳族烃的燃料。本发明的燃烧器可以用热（例如非冷却）的燃烧器表面操作，并且需要很少的任何冷却或其它形式的散热。本发明的燃烧器包括形成燃烧器出口的一个或多个耐火元件，在该燃烧器的出口可建立火焰。本发明的燃烧器提供了改进的火焰稳定性，可以用于更宽范围的燃料/氧化剂（例如空气）比和更宽范围的气体速度，并且通常比使用水冷金属燃烧器板的燃烧器更有效。本发明的燃烧器也可以被操作以减少燃烧器和燃烧器下游表面上不期望的烟灰沉积物的形成。

12. 发明授权

US07157066B2 Combustion process for synthesis of carbon nanomaterials from liquid hydrocarbon 有权
标题翻译：用于从液态碳氢化合物合成碳纳米材料的燃烧过程
公开(公告)号：US07157066B2
公开(公告)日：2007-01-02
申请号：US10306615
申请日：2002-11-27
申请人： Michael D. Diener , J. Michael Alford , James Nabity , Bradley D. Hitch
发明人： Michael D. Diener , J. Michael Alford , James Nabity , Bradley D. Hitch
IPC分类号： B01J19/26 , C01B31/02
CPC分类号： B82Y30/00 , B01J19/26 , B01J2219/00094 , B01J2219/00119 , B01J2219/00157 , B82Y40/00 , C01B32/152 , C01B32/162 , F23D2900/21007 , Y10S977/842
摘要： The present invention provides a combustion apparatus for the production of carbon nanomaterials including fullerenes and fullerenic soot. Most generally the combustion apparatus comprises one or more inlets for introducing an oxygen-containing gas and a hydrocarbon fuel gas in the combustion system such that a flame can be established from the mixed gases, a droplet delivery apparatus for introducing droplets of a liquid hydrocarbon feedstock into the flame, and a collector apparatus for collecting condensable products containing carbon nanomaterials that are generated in the combustion system. The combustion system optionally has a reaction zone downstream of the flame. If this reaction zone is present the hydrocarbon feedstock can be introduced into the flame, the reaction zone or both.
摘要翻译：本发明提供一种用于生产包括富勒烯和富勒烯烟灰的碳纳米材料的燃烧装置。最通常地，燃烧装置包括用于在燃烧系统中引入含氧气体和烃燃料气体的一个或多个入口，使得可以从混合气体建立火焰，用于引入液体烃原料液滴的液滴输送装置和用于收集在燃烧系统中产生的含有碳纳米材料的可冷凝产品的收集器装置。燃烧系统任选地在火焰下游具有反应区。如果存在该反应区，可将烃原料引入火焰，反应区或两者。

13. 发明授权

US07090788B2 Nanoporous composites of polymerized lyotropic liquid-crystalline monomers, and hydrophobic polymers 失效
标题翻译：聚合溶致液晶单体的纳米复合材料和疏水性聚合物
公开(公告)号：US07090788B2
公开(公告)日：2006-08-15
申请号：US10422604
申请日：2003-04-24
申请人： Brian Elliott
发明人： Brian Elliott
IPC分类号： C09K19/38 , C09K19/54 , B32B3/26 , B32B27/24 , B32B9/04
CPC分类号： C09K19/38 , C09K19/52 , Y10S428/91 , Y10S977/897 , Y10T428/249978 , Y10T428/25 , Y10T428/31504 , Y10T428/31855
摘要： This invention provides composite materials that combine the material properties of hydrophobic polymers with internal structure and order provided by polymerization of lyotropic liquid crystals (LLCs). Composites, particularly nanocomposites, are made by forming a LLC assembly that has hydrophobic regions and hydrophilic regions, combining hydrophobic polymer in the assembly and polymerizing the polymerizable LLC monomers in the assembly. The hydrophobic polymer, polymerized LLC assembly or both can be crosslinked in the composite. Nanoporous composites, particularly those with uniform-sized pores and/or with uniform pores distribution can be prepared in this way. In addition, complex polymers in which a second polymeric material, which may be organic or inorganic, can be introduced into the pores or other structural features of the composite can be prepared. Adding flexible hydrophobic polymers to the LLC assembly increases the flexibility and toughness of the resultant polymerized composite material to provide improved composite materials for use as membranes and in other applications. Hydrophobic polymer addition can also increase the diffusion resistance in the organic phase of the composite. Of particular interest are composites in which the hydrophobic polymer is butyl rubber or related synthetic rubber.
摘要翻译：本发明提供了将疏水性聚合物的材料性质与内部结构和通过溶致液晶（LLCs）聚合提供的顺序组合的复合材料。复合材料，特别是纳米复合材料，通过形成具有疏水区域和亲水区域的LLC组件，组合中的疏水性聚合物并在组合中聚合可聚合的LLC单体来制备。疏水性聚合物，聚合的LLC组件或两者都可以在复合材料中交联。可以以这种方式制备纳米多孔复合材料，特别是具有均匀孔隙和/或均匀孔分布的纳米复合材料。此外，可以制备其中可以将有机或无机的第二聚合物材料引入复合材料的孔或其它结构特征的复合聚合物。向LLC组件中加入柔性疏水聚合物增加了所得聚合复合材料的柔韧性和韧性，以提供用作膜和其它应用的改进的复合材料。疏水性聚合物添加也可以增加复合材料的有机相中的扩散阻力。特别令人感兴趣的是其中疏水性聚合物是丁基橡胶或相关合成橡胶的复合材料。

14. 发明授权

US07060233B1 Process for the simultaneous removal of sulfur and mercury 失效
标题翻译：同时去除硫和汞的方法
公开(公告)号：US07060233B1
公开(公告)日：2006-06-13
申请号：US10717299
申请日：2003-11-19
申请人： Girish Srinivas , Robert J. Copeland
发明人： Girish Srinivas , Robert J. Copeland
IPC分类号： B01D53/64 , B01D53/48 , B01D53/52 , C01B17/04 , C01G13/00
CPC分类号： B01D53/8612 , B01D53/64 , B01D2257/602 , C01B17/0404 , C01B17/0434 , C01B17/0447
摘要： A process for removing hydrogen sulfide, other sulfur-containing compounds and/or sulfur and mercury from a gas stream contaminated with mercury, hydrogen sulfide or both. The method comprises the step of selective oxidation of hydrogen sulfide (H2S) in a gas stream containing one or more oxidizable components other than H2S to generate elemental sulfur (S) or a mixture of sulfur and sulfur dioxide (SO2). The sulfur generated in the gas stream reacts with mercury in the gas stream to generate mercuric sulfide and sulfur and mercuric sulfide are removed from the gas stream by co-condensation.
摘要翻译：从被汞，硫化氢或两者污染的气流中除去硫化氢，其他含硫化合物和/或硫和汞的方法。该方法包括在含有除了H 2 S之外的一种或多种可氧化组分的气流中选择性氧化硫化氢（H 2 S 2 S）以产生元素硫的步骤（H 2 S 2 S） S）或硫和二氧化硫（SO 2 H 2）的混合物。在气流中产生的硫与气流中的汞反应产生硫化汞，硫和硫化汞通过共缩合从气流中除去。

15. 发明授权

US06986943B1 Surface modified particles by multi-step addition and process for the preparation thereof 失效
标题翻译：通过多步添加的表面改性颗粒及其制备方法
公开(公告)号：US06986943B1
公开(公告)日：2006-01-17
申请号：US10171402
申请日：2002-06-12
申请人： Ronald Lee Cook , Brian John Elliott , Silvia DeVito Luebben , Andrew William Myers , Bryan Matthew Smith
发明人： Ronald Lee Cook , Brian John Elliott , Silvia DeVito Luebben , Andrew William Myers , Bryan Matthew Smith
IPC分类号： B05D1/36 , B32B1/00
CPC分类号： C09C1/407 , B01J2/30 , B82Y30/00 , C01P2002/82 , C01P2004/64 , C09C1/24 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993
摘要： The present invention relates to a new class of surface modified particles and to a multi-step surface modification process for the preparation of the same. The multi-step surface functionalization process involves two or more reactions to produce particles that are compatible with various host systems and/or to provide the particles with particular chemical reactivities. The initial step comprises the attachment of a small organic compound to the surface of the inorganic particle. The subsequent steps attach additional compounds to the previously attached organic compounds through organic linking groups.
摘要翻译：本发明涉及一类新的表面改性颗粒和一种多步表面改性方法的制备方法。多步骤表面官能化过程涉及两个或更多个反应以产生与各种主体体系相容的颗粒和/或提供具有特定化学反应性的颗粒。初始步骤包括将小的有机化合物附着到无机颗粒的表面。随后的步骤通过有机连接基团将附加的化合物连接到先前连接的有机化合物上。

16. 发明授权

US5271907A High temperature regenerable hydrogen sulfide removal agents 失效
标题翻译：高温可再生硫化氢去除剂
公开(公告)号：US5271907A
公开(公告)日：1993-12-21
申请号：US844829
申请日：1992-03-03
申请人： Robert J. Copeland
发明人： Robert J. Copeland
IPC分类号： B01D53/04 , B01D53/08 , B01D53/52 , B01J20/06 , C01B17/04 , B01D53/02
CPC分类号： B01D53/12 , B01D53/08 , B01D53/523 , B01J20/06 , C01B17/04 , B01D2253/112 , B01D2257/302 , B01D2259/401 , B01D2259/402 , B01D2259/4143
摘要： A system for high temperature desulfurization of coal-derived gases using regenerable sorbents. One sorbent is stannic oxide (tin oxide, SnO.sub.2), the other sorbent is a metal oxide or mixed metal oxide such as zinc ferrite (ZnFe.sub.2 O.sub.4). Certain otherwise undesirable by-products, including hydrogen sulfide (H.sub.2 S) and sulfur dioxide (SO.sub.2) are reused by the system, and elemental sulfur is produced in the regeneration reaction. A system for refabricating the sorbent pellets is also described.
摘要翻译：使用可再生吸附剂对煤源气体进行高温脱硫的系统。一种吸附剂是氧化锡（氧化锡，SnO 2），另一种吸附剂是金属氧化物或混合金属氧化物如锌铁氧体（ZnFe2O4）。某些其他不合需要的副产物，包括硫化氢（H2S）和二氧化硫（SO2）都被系统重复利用，而再生反应中产生元素硫。还描述了用于重新制备吸附剂颗粒的系统。

17. 发明申请

US20220080072A1 MATERIALS AND METHODS FOR DECONTAMINATING ANIMAL INTEGUMENT 有权
公开(公告)号：US20220080072A1
公开(公告)日：2022-03-17
申请号：US17385359
申请日：2021-07-26
申请人： TDA Research, Inc.
发明人： Christopher Brian France
IPC分类号： A61L2/26 , A61L2/16
摘要： A method for decontaminating the outer integument of an animal without transferring contamination to the inner integument of the animal where the hazard can interact with the skin and harm the animal further. The animal has either fur, hair, or feathers and the inner integument is the skin and a skin-hazard material is present on the outer integument (the fur, hair, or feathers). The method uses a first porous dry wipe to sequester the skin-hazard material away from the contaminated animal by either wiping, blotting or rubbing the outer integument of the contaminated animal. The method avoids using free-flowing liquid in contact with the inner integument of the contaminated animal, and does not promote a liquid-phase transfer of the skin-hazard material from the outer integument to the inner integument.

18. 发明申请

US20210309778A1 HYDROLYSIS-TOLERANT CROSSLINKED POLYMERS FROM REVERSE-ACRYLATE MULTIFUNCTIONAL MONOMERS 有权
公开(公告)号：US20210309778A1
公开(公告)日：2021-10-07
申请号：US17203648
申请日：2021-03-16
申请人： TDA Research, Inc.
发明人： Robert Donald Bolskar , James William Raebiger , Rhia M. Martin , Sylvia DeVito Luebben
IPC分类号： C08F222/10
摘要： Crosslink-forming monomers, comprising reverse-acrylate groups, and crosslinked polymer networks formed by the polymerization of monomers that comprise said reverse-acrylate crosslink-forming monomers. Crosslink-forming monomers, comprising reverse-acrylate groups, comprising an alkyl, an aryl, an alkoxyl, and an alkylamino group bridging one or more reverse-acrylate groups. Crosslink-forming monomers, comprising reverse-acrylate groups, comprising an alkyl, an aryl, an alkoxyl, and an alkylamino ester groups. Crosslink-forming monomers, comprising reverse-acrylate groups, comprising alkyl groups where the group is selected from the group consisting of a methyl, an ethyl, a propyl, an n-butyl and a t-butyl. Reverse-acrylate crosslink-forming monomers comprise a chemical structure where the two or more polymerizable carbon-carbon double bonds are connected by a crosslinking group on the opposite side of the hydrolysable ester groups relative to normal crosslinking acrylate monomers. The crosslink-forming monomers herein form crosslinked polymer networks that do not lose their crosslinking upon hydrolysis of the ester linkages.

19. 发明申请

US20210300876A1 DIENE GEMINI POLYMERIZABLE SURFACTANTS WITH MIXED CIS AND TRANS ISOMERS THAT FORM BICONTINUOUS CUBIC PHASES 有权
公开(公告)号：US20210300876A1
公开(公告)日：2021-09-30
申请号：US17259467
申请日：2019-07-09
申请人： TDA Research, Inc
发明人： Rhia M Martin , Douglas L. Gin , Richard D Noble , Vinh The Nguyen , Brian J Elliott
IPC分类号： C07D233/58 , C09K19/52
摘要： A polymerizable Gemini surfactant based on tail groups with mixed isomer dienes. The Gemini surfactants may be produced having imidazolium head groups and diene tail groups with a near-equal abundance of the “E” and “Z” isomers. These compounds are lyotropic liquid crystals that can form bicontinuous cubic phases by self-assembly.

20. 发明申请

US20210041065A1 RAPID FILL COMPRESSED GAS STORAGE TANK 有权
公开(公告)号：US20210041065A1
公开(公告)日：2021-02-11
申请号：US16989815
申请日：2020-08-10
申请人： TDA Research, Inc
发明人： Ambalavanan Jayaraman , Michael Travis Bonnema
IPC分类号： F17C5/06 , F17C13/02
摘要： A method for rapidly filling a compressed gas storage tank with a moderated temperature rise using a Coanda nozzle to inject the feed gas into the tank and using the Coanda nozzle to direct the feed gas along the inner surface of the storage tank; entraining the stored gas with the feed gas that is flowing under the influence of the Coanda effect to flow along the inner surface of the gas storage tank; and transferring heat from the flowing gas to the external walls of the tank. Also, a compressed gas storage tank for rapid filling with a moderated temperature rise comprising: a gas storage tank and a Coanda nozzle capable of directing feed gas that is injected into the gas storage tank along the inner surface of the gas storage tank.

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