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121. 发明授权

US4224236A Process for the manufacture of oxygen-containing carbon compounds from synthesis gas 失效
标题翻译：从合成气制造含氧碳化合物的方法
公开(公告)号：US4224236A
公开(公告)日：1980-09-23
申请号：US25032
申请日：1979-03-29
申请人： Friedrich Wunder , Hans-Jurgen Arpe , Ernst I. Leupold , Hans-Joachim Schmidt
发明人： Friedrich Wunder , Hans-Jurgen Arpe , Ernst I. Leupold , Hans-Joachim Schmidt
IPC分类号： C07C27/06 , B01J23/00 , C07C27/00 , C07C27/22 , C07C29/158 , C07C45/49 , C07C51/00 , C07C51/10 , C07C53/08 , C07C67/00
CPC分类号： C07C45/49 , C07C29/158 , C07C51/10
摘要： Acetic acid, ethanol, acetic aldehyde and possibly the secondary products thereof are prepared by the catalytic reaction of carbon monoxide and hydrogen. The catalyst contains applied onto a carrier, metallic rhodium, halide ions and magnesium salts or complex compounds of magnesium or compounds of magnesium with oxides of elements from groups III to VI of the Periodic Table.
摘要翻译：通过一氧化碳和氢气的催化反应制备乙酸，乙醇，乙醛及其可能的二次产物。该催化剂包含在载体，金属铑，卤离子和镁盐或镁的复合化合物或镁的化合物与周期表第III至VI族元素的氧化物之间。

122. 发明授权

US4177203A Process for the production of hydrocarbons and oxygen-containing compounds and catalysts therefor 失效
标题翻译：用于生产烃和含氧化合物及其催化剂的方法
公开(公告)号：US4177203A
公开(公告)日：1979-12-04
申请号：US840059
申请日：1977-10-06
申请人： Herbert Kolbel , Klaus D. Tillmetz
发明人： Herbert Kolbel , Klaus D. Tillmetz
IPC分类号： B01J23/889 , B01J37/16 , B01J37/18 , C07C1/04 , C07C29/156 , C07C45/49 , C07C27/06
CPC分类号： B01J23/8892 , C07C1/0445 , C07C29/156 , C07C45/49 , B01J37/16 , B01J37/18 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/10 , C07C2523/02 , C07C2523/04 , C07C2523/34 , C07C2523/745 , C07C2523/889
摘要： Processes for synthesizing unsaturated and saturated hydrocarbons and oxygen-containing compounds by catalytic hydrogenation of carbon monoxide at temperatures of 220 to 375 degrees C. and pressures from 1 to 60 bars. Specially activated catalysts for this purpose contain at least 50% manganese and less than 50% iron, by weight. The product distribution spectrum is shifted in the direction of C.sub.2 to C.sub.4 hydrocarbons, the chain length of the products extending only to about C.sub.6 and methane being formed only in traces.
摘要翻译：通过一氧化碳在220至375℃的温度和1至60巴的压力下催化氢化合成不饱和烃和饱和烃和含氧化合物的方法。用于此目的的特殊活化催化剂含有至少50％的锰和小于50重量％的铁。产物分布谱在C2至C4烃的方向上移动，产物的链长仅延伸至约C6，甲烷仅形成痕迹。

123. 发明授权

US4162262A Process for producing two-carbon atom compounds from synthesis gas with minimal production of methanol 失效
标题翻译：以最少的甲醇生产从合成气生产双碳原子化合物的方法
公开(公告)号：US4162262A
公开(公告)日：1979-07-24
申请号：US841054
申请日：1977-10-11
申请人： Paul C. Ellgen , Madan M. Bhasin
发明人： Paul C. Ellgen , Madan M. Bhasin
IPC分类号： B01J23/63 , C07C29/151 , C07C29/158 , C07C45/49 , C07C27/06
CPC分类号： C07C29/158 , B01J23/63 , C07C29/1512 , C07C45/49 , Y02P20/52
摘要： A process for selectively preparing a mixture of two-carbon atom oxygenated hydrocarbons while minimizing the co-production of methanol which comprises continuously contacting a gaseous reaction mixture containing hydrogen and carbon monoxide with a solid catalyst comprising rhodium in combination with thorium and/or uranium at reaction conditions correlated so as to favor the formation of a substantial proportion of such two-carbon atom products.
摘要翻译：一种用于选择性地制备双碳原子氧化烃的混合物的方法，同时最小化甲醇的共同生产，其包括使含有氢和一氧化碳的气态反应混合物与包含铑和钍和/或铀的组合的固体催化剂连续接触反应条件相关，从而有利于形成相当大比例的这种二碳原子产物。

124. 发明授权

US4151192A Promoting n-propyl alcohol formation with vanadium compounds 失效
标题翻译：促进用钒化合物形成正丙醇
公开(公告)号：US4151192A
公开(公告)日：1979-04-24
申请号：US906585
申请日：1978-05-16
申请人： Leonard Kaplan
发明人： Leonard Kaplan
IPC分类号： C07C29/151 , C07C29/158 , C07C29/159 , C07C27/06 , C07C31/02 , C07C31/20
CPC分类号： C07C29/159 , C07C29/1514 , C07C29/158
摘要： This invention relates to the manufacture of monohydric and polyhydric alcohols, specifically, n-propyl alcohol by reacting synthesis gas, i.e., hydrogen and oxides of carbon, in the presence of a rhodium carbonyl complex and vanadium compounds.
摘要翻译：本发明涉及在羰基铑络合物和钒化合物的存在下，使合成气，即氢和碳氧化物反应来制造一元醇和多元醇，特别是正丙醇。

125. 发明授权

US4131616A Methanation catalyst 失效
标题翻译：甲烷化催化剂
公开(公告)号：US4131616A
公开(公告)日：1978-12-26
申请号：US482574
申请日：1974-06-24
申请人： Alvin B. Stiles
发明人： Alvin B. Stiles
IPC分类号： B01J23/86 , B01J37/03 , C07B61/00 , C07C1/00 , C07C1/02 , C07C9/04 , C07C67/00 , C10K3/02 , C10K3/04 , C07C27/06
CPC分类号： C10K3/04 , B01J23/866 , B01J37/03 , C07C1/02 , C07C2523/26 , C07C2523/755 , C07C2523/86
摘要： An improved nickel chromite catalyst useful for methanation is prepared by pre-reducing the hexavalent chromium component thereof to trivalent form, while maintaining the nickel component in unreduced oxide form.
摘要翻译：通过将六价铬组分预还原成三价形式，同时保持镍组分为未还原氧化物形式，可制备用于甲烷化的改进的镍铬铁合金催化剂。

126. 发明授权

US4119656A Preparation of hydroxylated compounds from synthesis of gas with palladium catalysts 失效
标题翻译：用钯催化剂合成气体制备羟化化合物
公开(公告)号：US4119656A
公开(公告)日：1978-10-10
申请号：US797242
申请日：1977-05-16
申请人： Marvin Lloyd Poutsma , Jule Anthony Rabo , Alan Peter Risch
发明人： Marvin Lloyd Poutsma , Jule Anthony Rabo , Alan Peter Risch
IPC分类号： C07C29/15 , B01J23/00 , C07B61/00 , C07C27/00 , C07C29/151 , C07C29/157 , C07C31/04 , C07C67/00 , C07C27/06
CPC分类号： C07C29/157 , C07C29/1512 , Y02P20/52
摘要： A heterogeneous catalytic process for producing hydroxylated hydrocarbons containing from 1-2 carbon atoms which comprises: contacting a synthesis gas containing carbon monoxide and hydrogen with a catalyst consisting essentially of palladium at reaction conditions such that hydroxylated compounds are selectively produced while substantially avoiding the concomitant formation of methane or higher molecular weight hydrocarbons.
摘要翻译：用于生产含有1-2个碳原子的羟基化烃的非均相催化方法，其包括：在反应条件下使含有一氧化碳和氢气的合成气与基本上由钯组成的催化剂接触，使得羟基化化合物被选择性地生产，同时基本上避免了伴随形成的甲烷或更高分子量的烃。

127. 发明授权

US4115433A Catalyst and process for producing polyhydric alcohols and derivatives 失效
标题翻译：用于制备多元醇和衍生物的催化剂和方法
公开(公告)号：US4115433A
公开(公告)日：1978-09-19
申请号：US840866
申请日：1977-10-11
申请人： Lowell Alan Cosby , Rocco Anthony Fiato , Jose Luis Vidal
发明人： Lowell Alan Cosby , Rocco Anthony Fiato , Jose Luis Vidal
IPC分类号： C01G55/00 , B01J31/00 , B01J31/20 , C07B61/00 , C07C27/00 , C07C27/06 , C07C29/15 , C07C29/151 , C07C29/158 , C07C31/04 , C07C31/18 , C07C67/00 , C07C29/16
CPC分类号： B01J31/0239 , B01J31/0204 , B01J31/0237 , B01J31/0271 , B01J31/20 , C07C29/151 , C07C29/1514 , C07C29/158 , B01J2231/641 , B01J2531/0211 , B01J2531/822 , B01J31/226 , Y02P20/52
摘要： A novel catalyst and process for the manufacture of polyhydric alcohols from synthesis gas. This novel catalyst is a rhodium carbonyl sulfur cluster compound. In particular, the anion cluster of the rhodium carbonyl sulfur compound is of the following empirical formula:[Rh.sub.17 (S).sub.2 (CO).sub.32 ].sup.-3
摘要翻译：用于从合成气制造多元醇的新型催化剂和方法。这种新型催化剂是一种铑羰基硫簇化合物。特别地，羰基铑羰基化合物的阴离子簇具有以下经验式：

128. 发明授权

US4115428A Catalyst and process for producing polyhydric alcohols and derivatives 失效
标题翻译：催化剂和生产多元醇和衍生物的方法
公开(公告)号：US4115428A
公开(公告)日：1978-09-19
申请号：US838016
申请日：1977-09-29
申请人： Jose Luis Vidal , Zoltan Csaba Mester , Wellington Epler Walker
发明人： Jose Luis Vidal , Zoltan Csaba Mester , Wellington Epler Walker
IPC分类号： C07C27/06 , B01J31/00 , B01J31/20 , C07B61/00 , C07C27/00 , C07C29/15 , C07C29/151 , C07C29/158 , C07C29/159 , C07C31/18 , C07C67/00 , C07C29/16
CPC分类号： B01J31/0244 , B01J31/0204 , B01J31/0237 , B01J31/0271 , B01J31/20 , C07C29/1512 , C07C29/1514 , C07C29/158 , C07C29/159 , B01J2231/648 , B01J2531/0211 , B01J2531/822 , Y02P20/52
摘要： A novel catalyst and process for the manufacture of polyhydric alcohols from synthesis gas. This novel catalyst is a rhodium carbonyl carbido cluster compound. In particular the cluster compound is of the following empirical formula:Cs.sub.2 [Rh.sub.6 (CO).sub.15 C]

129. 发明授权

US4111975A Catalytic process for producing polyhydric alcohols and derivatives 失效
标题翻译：用于生产多元醇和衍生物的催化方法
公开(公告)号：US4111975A
公开(公告)日：1978-09-05
申请号：US782986
申请日：1977-03-30
申请人： James Norman Cawse , Jose Luis Vidal
发明人： James Norman Cawse , Jose Luis Vidal
IPC分类号： C07C27/06 , B01J31/00 , C07B61/00 , C07C27/00 , C07C29/15 , C07C29/151 , C07C29/158 , C07C31/04 , C07C31/18 , C07C67/00
CPC分类号： C07C29/158 , C07C29/1512 , C07C29/1514 , Y02P20/52
摘要： A process for producing polyhydric alcohols, their ether and ester derivatives, oligomers of such alcohols and monohydric alcohols and their ester derivatives by reacting hydrogen and oxides of carbon in the presence of a rhodium carbonyl complex, an alkali metal cation and a cryptand.
摘要翻译：在羰基铑络合物，碱金属阳离子和穴穴存在下，使氢和碳的氧化物反应，生成多元醇，它们的醚和酯衍生物，这些醇和一元醇的低聚物及其酯衍生物的方法。

130. 发明授权

US4012404A Process for producing high-methane gas 失效
标题翻译：生产高甲烷气的方法
公开(公告)号：US4012404A
公开(公告)日：1977-03-15
申请号：US521985
申请日：1974-11-07
申请人： Helmut Liebgott
发明人： Helmut Liebgott
IPC分类号： C10K1/12 , C10K1/14 , C10L3/00 , C10L3/08 , C07C27/06
CPC分类号： C10K1/14 , C10G11/00 , C10K1/122 , C10L3/00 , C10L3/08
摘要： High-methane gas which can be used in place of natural gas is made byA. catalytically cracking liquid hydrocarbons with water vapor at elevated temperatures and pressures to produce a rich gas containing less than 15% hydrogen by volume;B. cooling the rich gas to a temperature below 150.degree. C thereby reducing the water vapor content thereof by condensation;C. separating condensed water from the rich gas;D. thereafter hydrogenating the carbon oxides in the gas by dividing same into two streams, one of the streams being preheated to a temperature of at least 250.degree. C and then being introduced into the first catalyst layer of a hydrogenation zone containing two catalyst layers, the other of the streams being fed at the temperatures produced in cooling step (b) between the catalyst layers of the hydrogenation zone; andE. scrubbing the product gas leaving the hydrogenation zone to remove carbon dioxide.Preferably, the ratio of the two streams is adjusted such that the temperature rise in the second catalyst layer of the hydrogenation zone is less than 50.degree. C and the product gas leaving the hydrogenation zone contains less than 1% hydrogen by volume.
摘要翻译：可用于代替天然气的高甲烷气体由A.通过水蒸汽在高温下以液体的形式催化裂化液体碳氢化合物产生含有低于15％氢气的大量气体的压力; B.将大量气体冷却至低于150℃的温度，从而通过冷凝降低其水蒸汽含量; 从丰富的气体分离浓缩水; D.将气体中的碳氧化物加氢分解成两个流，其中一个流经至少250℃的温度，然后被引入含有两个催化剂层的氢化区的第一催化剂层中，在冷却步骤（b）中在氢化区的催化剂层之间产生的温度下进料另一个; 和E.将产品气体放出加氢区以移除二氧化碳。

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