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91. 发明申请

US20180282436A1 METHOD FOR PRODUCING HYDROXYALKYL ALKYL CELLULOSE 审中-公开
公开(公告)号：US20180282436A1
公开(公告)日：2018-10-04
申请号：US15921146
申请日：2018-03-14
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Akira KITAMURA , Mitsuo NARITA
IPC分类号： C08B11/02 , D21C9/00
摘要： Provided is a method for producing a hydroxyalkyl alkyl cellulose having high thermal gel strength while suppressing a reduction in thermal gelation temperature. More specifically, provided is a method for producing a hydroxyalkyl alkyl cellulose including steps of: mixing cellulose pulp with a first alkali metal hydroxide solution to obtain alkali cellulose, reacting the alkali cellulose with an alkylating agent and a hydroxyalkylating agent to obtain a first reaction product mixture, adding a second alkali metal hydroxide solution to the first reaction product mixture without further adding any of alkylating and hydroxyalkylating agents to obtain a second reaction product mixture, and subjecting the second reaction product mixture to purification to obtain a hydroxyalkyl alkyl cellulose.

92. 发明授权

US10058509B2 Alkyl cellulose for use in tableting and solid preparation comprising same 有权
公开(公告)号：US10058509B2
公开(公告)日：2018-08-28
申请号：US15622354
申请日：2017-06-14
申请人： Shin-Etsu Chemical Co., Ltd.
发明人： Takuya Yokosawa , Naosuke Maruyama
IPC分类号： C08B11/08 , A61K9/20 , C08B11/20 , A61K31/167 , C08B11/02
CPC分类号： A61K9/2054 , A61K9/2095 , A61K31/167 , C08B11/02 , C08B11/20
摘要： Provided are an alkyl cellulose excellent in formability when added even in a small amount and not causing marked delay in disintegration; a solid preparation comprising it; and a method for producing the solid preparation. More specifically, provided are an alkyl cellulose for use in tableting, the alkyl cellulose having a specific surface area of from 0.5 to 10.0 m2/g as measured by BET method and a solid preparation comprising the alkyl cellulose. Also provided is a method for producing the alkyl cellulose, comprising the steps of: bringing pulp into contact with an alkali metal hydroxide solution to obtain alkali cellulose, reacting the alkali cellulose with an etherifying agent to obtain a first alkyl cellulose, pulverizing the first alkyl cellulose, and depolymerizing the pulverized first alkyl cellulose through hydrolysis with an acid catalyst or through oxidative decomposition with an oxidant to obtain a second alkyl cellulose.

93. 发明申请

US20180022832A1 METHOD FOR PRODUCING POLYSACCHARIDE DERIVATIVE AND LIGNIN DERIVATIVE 审中-公开
公开(公告)号：US20180022832A1
公开(公告)日：2018-01-25
申请号：US15521200
申请日：2015-10-23
申请人： NATIONAL UNIVERSITY CORPORATION KANAZAWA UNIVERSITY , Kanazawa Institute of Technology
发明人： Ryohei KAKUCHI , Kazuaki NINOMIYA , Yoshiki SHIBATA , Kiyoshi UZAWA , Tomoki OGOSHI , Katsuhiro MAEDA , Tomoyuki IKAI , Kenji TAKAHASHI
IPC分类号： C08B3/06 , C08B11/02 , C08B3/18 , C07G1/00
CPC分类号： C08B3/06 , C07G1/00 , C08B3/00 , C08B3/18 , C08B11/00 , C08B11/02 , Y02P20/542
摘要： An object is to provide a method for producing a polysaccharide derivative without using a catalyst, a cocatalyst, or an active compound by esterification, etherification, or the like, from a polysaccharide such as cellulose as a source material, while maintaining a high molecular weight. Another object is to provide a method for producing a cellulose derivative in a separated condition directly from biomass containing lignocellulose. A method for producing a polysaccharide derivative of the present invention is characterized in that a reaction is carried out in a mixture comprising: a source material comprising a polysaccharide; an ionic liquid for which the pKa of a conjugate acid of an anion in DMSO is 12 to 19 and which is capable of producing a carbene; and a chain or cyclic ester compound or an epoxy compound. Preferably as a source material containing a polysaccharide, a biomass source material containing lignocellulose is used.

94. 发明授权

US09738621B2 Multifunctional materials and composites 有权
公开(公告)号：US09738621B2
公开(公告)日：2017-08-22
申请号：US14379021
申请日：2013-02-15
申请人： ARIZONA BOARD OF REGENTS, A BODY CORPORATE OF THE STATE OF ARIZONA ACTING FOR AND ON BEHALF OF ARIZONA STATE UNIVERSITY
发明人： Dong-Kyun Seo , Ki-Wan Jeon
IPC分类号： C07D331/02 , C01B19/00 , C01B31/02 , C01B31/04 , C08B11/02 , C08B11/20 , C08B15/05 , C08L1/08 , C08L1/28 , B82Y30/00 , B82Y40/00 , C07D345/00 , C08B15/00 , C08L101/06
CPC分类号： C07D331/02 , B82Y30/00 , B82Y40/00 , C01B19/00 , C01B32/17 , C01B32/194 , C07D345/00 , C08B11/02 , C08B11/20 , C08B15/00 , C08B15/05 , C08L1/08 , C08L1/28 , C08L101/06 , Y02P20/134
摘要： Forming multifunctional materials and composites thereof includes contacting a first material having a plurality of oxygen-containing functional groups with a chalcogenide compound, and initiating a chemical reaction between the first material and the chalcogenide compound, thereby replacing oxygen in some of the oxygen-containing functional groups with chalcogen from the chalcogen-containing compound to yield a second material having chalcogen-containing functional groups and oxygen-containing functional groups. The first material is a carbonaceous material or a macromolecular material. A product including the second material is collected and may be processed further to yield a modified product or a composite.

95. 发明授权

US09434787B2 Cellulose ethers having reactive anchor group, modified cellulose ethers obtainable therefrom and methods for the preparation thereof 有权
公开(公告)号：US09434787B2
公开(公告)日：2016-09-06
申请号：US14645700
申请日：2015-03-12
申请人： SE Tylose GmbH & Co. KG
发明人： Mike Kleinert
IPC分类号： C08B11/14 , C08B11/16 , C08B11/193 , C08L1/26 , C08B11/145 , C08B11/02 , C08B11/06 , C08B11/08 , C08L1/28
CPC分类号： C08B11/145 , C08B11/02 , C08B11/06 , C08B11/08 , C08B11/193 , C08L1/26 , C08L1/28 , C08L1/282 , C08L1/284 , C08L1/288
摘要： Non-ionic water-soluble cellulose ethers modified with 3-azido-2-hydroxypropyl groups bound via an ether link are provided having a molar degree of substitution MSAHP in the range from 0.001 to 0.50. Exemplary cellulose ethers are alkyl cell doses, including methyl, hydroxyalkyl (e.g. hydroxyethyl hydroxypropyl) or alkylhydroxyalkyl cellulose (e.g. methylhydroxyethyl). Reaction products with alkyne compounds are also provided, resulting in a terminal alkyne group. The reaction of azide with the alkyne proceeds as a 1,3-dipolar cycloaddition reaction, advantageously with Cu(I) or ruthenium catalysts. A multiplicity of cellulose ethers can be obtained from the conversion reaction. Variations in the macroscopic properties can be achieved by controlled modification, ranging from increased or reduced viscosity. The reaction, taking place within a few seconds, requires only minimal catalyst. Gel formation is reversible by adjustment of the pH such that a monophasic system (high-viscous fluid) arises again from a biphasic system (gel+low-viscous water phase).

96. 发明授权

US09243075B2 N-acylamino acid derivatives of cellulose or starch based polysaccharides and emulsified products containing the same 有权
标题翻译：纤维素或淀粉基多糖的N-酰基氨基酸衍生物和含有它们的乳化产物
公开(公告)号：US09243075B2
公开(公告)日：2016-01-26
申请号：US13599650
申请日：2012-08-30
申请人： Masayuki Kuramoto , Tatsuya Hattori , Masahiro Ino
发明人： Masayuki Kuramoto , Tatsuya Hattori , Masahiro Ino
IPC分类号： C08B31/02 , C08B15/06 , C08L3/06 , C08B31/04 , C08B15/00 , C08B31/00 , C08L1/08 , A61K8/06 , A61Q19/00 , A61K8/73 , C08B11/02 , C08B11/08 , C08L3/04
CPC分类号： C08B31/02 , A61K8/062 , A61K8/731 , A61K8/732 , A61K2800/10 , A61Q19/00 , C08B11/02 , C08B11/08 , C08B15/00 , C08B15/06 , C08B31/00 , C08B31/04 , C08L1/08 , C08L3/04 , C08L3/06
摘要： To provide a novel substance having an excellent water-dispersibility capable of forming an emulsion which spreads rapidly onto the skin, does not undergo aggregation or segregation due to a salt, and is excellent in a low temperature stability. The aforementioned problems were found to be solved by means of a certain polysaccharide and the invention was established.
摘要翻译：为了提供能够形成迅速扩散到皮肤上的乳液的优异的水分散性的新型物质，不会由于盐而发生聚集或分离，并且具有优异的低温稳定性。发现上述问题是通过某种多糖来解决的，并且建立了本发明。

97. 发明授权

US09216191B2 Methods and composition for inducing satiety 有权
标题翻译：诱发饱腹感的方法和组成
公开(公告)号：US09216191B2
公开(公告)日：2015-12-22
申请号：US14350819
申请日：2012-10-11
申请人： Dow Global Technologies LLC
发明人： Roland Adden , Matthias Knarr , Britta Huebner-Keese , Robert L. Sammler
IPC分类号： A61K31/717 , A61K31/7016 , C08B11/02 , A61P3/04 , A23L1/308 , A23L1/00 , A23L1/0534 , A23L1/09 , A23L1/29 , A61K31/7004 , A61K31/702
CPC分类号： A61K31/717 , A23L5/00 , A23L7/00 , A23L9/00 , A23L29/262 , A23L29/30 , A23L33/125 , A23L33/21 , A23L33/24 , A23L33/30 , A23P10/20 , A23V2002/00 , A61K31/7004 , A61K31/7016 , A61K31/702 , A23V2200/228 , A23V2250/28 , A23V2250/51088 , A23V2250/60 , A23V2200/332
摘要： A flowable or spoonable medicament, food, food ingredient or food supplement is useful for inducing satiety. It comprises (a) one or more mono-, di- and/or oligosaccharides and (b) a methylcellulose, wherein the methylcellulose has anhydroglucose units joined by 1-4 linkages wherein hydroxy groups of anhydroglucose units are substituted with methyl groups such that s23/s26 is from 0.17 to 0.36, wherein s23 is the molar fraction of anhydroglucose units wherein only the two hydroxy groups in the 2- and 3-positions of the anhydroglucose unit are substituted with methyl groups and wherein s26 is the molar fraction of anhydroglucose units wherein only the two hydroxy groups in the 2- and 6-positions of the anhydroglucose unit are substituted with methyl groups.
摘要翻译：可流动或可匙取的药物，食物，食物成分或食物补充剂可用于诱导饱腹感。它包含（a）一种或多种单糖，二糖和/或寡糖和（b）甲基纤维素，其中甲基纤维素具有通过1-4键连接的脱水葡萄糖单元，其中脱水葡萄糖单元的羟基被甲基取代，使得s23 / s26为0.17至0.36，其中s23为脱水葡萄糖单元的摩尔分数，其中脱水葡萄糖单元的2-和3-位上的两个羟基仅被甲基取代，并且其中s26是脱葡萄糖单元的摩尔分数其中在脱水葡萄糖单元的2位和6位只有两个羟基被甲基取代。

98. 发明申请

US20150231082A1 HYDROXYALKYLALKYL CELLULOSE FOR TABLETING AND SOLID PREPARATION COMPRISING THE SAME 审中-公开
标题翻译：用于包含其的成型和固体制剂的羟基甲基纤维素
公开(公告)号：US20150231082A1
公开(公告)日：2015-08-20
申请号：US14617487
申请日：2015-02-09
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Takuya YOKOSAWA , Naosuke MARUYAMA
IPC分类号： A61K9/20 , A61K31/167 , C08B11/02
CPC分类号： A61K9/2054 , A61K9/2018 , A61K31/167 , A61K47/38 , C08B1/06 , C08B1/08 , C08B11/02 , C08B11/08 , C08B11/193 , C08B11/20 , C08L1/284 , Y10T428/2982
摘要： Provided are a hydroxyalkylalkyl cellulose excellent in formability and not causing marked delay in disintegration when added even in a small amount; a solid preparation including the hydroxyalkylalkyl cellulose; and a method for producing the solid preparation. More specifically, provided are a hydroxyalkylalkyl cellulose for tableting having a specific surface area of from 0.5 to 5.0 m2/g as measured by BET and a solid preparation including the hydroxyalkylalkyl cellulose. Also provided is a method for producing the hydroxyalkylalkyl cellulose for tableting, including the steps of: bringing pulp into contact with an alkali metal hydroxide solution to obtain an alkali cellulose, reacting the alkali cellulose with an etherifying agent to obtain a first hydroxyalkylalkyl cellulose, grinding the first hydroxyalkylalkyl cellulose, and subjecting the ground first hydroxyalkylalkyl cellulose to hydrolysis in the presence of an acid catalyst or oxidative degradation in the presence of an oxidant to obtain a second hydroxyalkylalkyl cellulose.
摘要翻译：提供了成型性优异的羟烷基烷基纤维素，即使少量添加也不会引起明显的崩解延迟; 包括羟烷基烷基纤维素的固体制剂; 和固体制剂的制造方法。更具体地，提供了通过BET测定的比表面积为0.5-5.0m 2 / g的压片用羟烷基烷基纤维素和包含羟烷基烷基纤维素的固体制剂。还提供了用于制备用于压片的羟烷基烷基纤维素的方法，包括以下步骤：使纸浆与碱金属氢氧化物溶液接触以获得碱纤维素，使碱纤维素与醚化剂反应，得到第一羟烷基烷基纤维素，研磨第一羟烷基烷基纤维素，并且在酸催化剂存在下使研磨的第一羟烷基烷基纤维素水解，或在氧化剂存在下进行氧化降解，得到第二羟烷基烷基纤维素。

99. 发明授权

US08822675B2 Low-substituted hydroxypropylcellulose and solid preparation comprising the same 有权
标题翻译：低取代羟丙基纤维素和包含其的固体制剂
公开(公告)号：US08822675B2
公开(公告)日：2014-09-02
申请号：US13043113
申请日：2011-03-08
申请人： Naosuke Maruyama , Yasuyuki Hirama
发明人： Naosuke Maruyama , Yasuyuki Hirama
IPC分类号： C08B11/08 , A61K31/167 , A61K9/00 , A61K47/18 , C08B11/02 , A61K9/20
CPC分类号： C08B11/02 , A61K9/0056 , A61K9/2054 , A61K31/167 , A61K47/18
摘要： Provided is nonionic and excellently stable low-substituted hydroxypropylcellulose having improved compressibility and flowability, and further having improved disintegration and texture in oral cavity. More specifically provided is low-substituted hydroxypropylcellulose having a crystallinity of 60% or less, a degree of hydroxypropoxyl substitution of 5 to 9% by weight, and an aspect ratio of less than 2.5, wherein the crystallinity is calculated based on a diffraction intensity by wide-angle X-ray diffraction measurement according to the following formula (1): Crystallinity(%)={(Ic−Ia)/Ic}×100 (1) wherein Ic means a diffraction intensity at a diffraction angle 2θ of 22.5° and Ia means a diffraction intensity at a diffraction angle 2θ of 18.5°.
摘要翻译：本发明提供了具有改进的可压缩性和流动性的非离子和非常稳定的低取代羟丙基纤维素，并且还具有口腔改善的崩解和质地。更具体地提供了结晶度为60％以下，羟丙氧基取代度为5〜9重量％，长径比小于2.5的低取代羟丙基纤维素，其中结晶度基于衍射强度由根据下式（1）的广角X射线衍射测定：结晶度（％）= {（Ic-Ia）/ Ic}×100（1）其中，Ic表示衍射角2°时的衍射强度; 为22.5°，Ia表示衍射角2°时的衍射强度; 为18.5°。

100. 发明申请

US20140179049A1 SILICON/GERMANIUM-BASED NANOPARTICLE PASTES WITH ULTRA LOW METAL CONTAMINATION 审中-公开
标题翻译：具有超低金属污染的硅/基于锗的纳米材料
公开(公告)号：US20140179049A1
公开(公告)日：2014-06-26
申请号：US14087872
申请日：2013-11-22
申请人： NanoGram Corporation
发明人： Ha Thi-Hoang Nguyen , Masaya Soeda , Weidong Li , Uma Srinivasan
IPC分类号： C09D11/14 , C08B11/02 , C08B11/20 , H01L31/18
CPC分类号： C08B11/02 , C08B11/22 , C09D11/52 , H01L31/022441 , H01L31/0384 , H01L31/03921 , H01L31/1804 , H01L31/1864 , Y02E10/547 , Y02P70/521
摘要： Silicon based nanoparticle inks are described with very low metal contamination levels. In particular, metal contamination levels can be established in the parts-per-billion range. The inks of particular interest generally comprise a polymer to influence the ink rheology. Techniques are described that are suitable for purifying polymers soluble in polar solvents, such as alcohols, with respect metal contamination. Very low levels of metal contamination for cellulose polymers are described.
摘要翻译：以非常低的金属污染水平描述了基于硅的纳米颗粒油墨。特别是金属污染水平可以建立在十亿分之一的范围内。特别感兴趣的油墨通常包含影响油墨流变性的聚合物。描述了适用于纯化可溶于极性溶剂如醇的聚合物的技术，涉及金属污染。描述了纤维素聚合物的非常低的金属污染水平。

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