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91. 发明申请

US20020058743A1 Thermally conductive polymer composition and thermally conductive molded article 有权
标题翻译：导热聚合物组合物和热导成型制品
公开(公告)号：US20020058743A1
公开(公告)日：2002-05-16
申请号：US09943006
申请日：2001-08-31
发明人： Masayuki Tobita , Natsuko Ishihara , Naoyuki Shimoyama , Shinya Tateda
IPC分类号： C08K003/04 , C08K003/18 , C01B031/04
CPC分类号： D01F9/145 , C08K7/06 , C08K9/02 , D01F9/15 , D01F9/155 , H01L23/3737 , H01L23/433 , H01L24/48 , H01L2224/05599 , H01L2224/16 , H01L2224/16225 , H01L2224/16227 , H01L2224/32245 , H01L2224/45099 , H01L2224/48247 , H01L2224/73253 , H01L2224/85399 , H01L2924/00014 , H01L2924/01012 , H01L2924/01019 , H01L2924/01078 , H01L2924/01079 , H01L2924/12042 , H01L2924/181 , H01L2924/00 , H01L2924/00012 , H01L2224/45015 , H01L2924/207
摘要： A thermally conductive polymer composition includes polymer matrix such as thermoplastic resin or thermoplastic elastomer and a graphitized carbon fiber which serves as a thermally conductive filler. The graphitized carbon fiber is made from a mesophase pitch. The mesophase pitch is spun, infusibilized, carbonized, pulverized, and graphitized to form powdery graphitized carbon fibers. Preferably, the graphitized carbon fibers have a diameter of 5-20 nullm, an average particle size of 10-500 nullm, and a density of 2.20-2.26 g/cm3. The composition may be molded to form a thermally conductive molded article such as a thermally conductive sheet. The thermally conductive polymer composition and thermally conductive molded article have high thermal conductivity and transfer large amounts of heat from electric or electronic parts.
摘要翻译：导热聚合物组合物包括聚合物基质，例如热塑性树脂或热塑性弹性体，以及用作导热填料的石墨化碳纤维。石墨化碳纤维由中间相沥青制成。将中间相沥青纺丝，不熔化，碳化，粉碎和石墨化，形成粉状石墨化碳纤维。优选石墨化碳纤维的直径为5-20μm，平均粒径为10-500μm，密度为2.20-2.26g / cm3。组合物可以被模制以形成导热模制品，例如导热片。导热聚合物组合物和热导成型制品具有高导热性并且从电子或电子部件传递大量的热量。

92. 发明授权

US5620674A Carbon fibers and process for their production 失效
标题翻译：碳纤维及其生产工艺
公开(公告)号：US5620674A
公开(公告)日：1997-04-15
申请号：US327818
申请日：1994-10-17
申请人： Iwao Yamamoto , Hiroyuki Aikyo
发明人： Iwao Yamamoto , Hiroyuki Aikyo
IPC分类号： C01B31/04 , C08J5/04 , D01F9/14 , D01F9/145 , D01F9/155 , B01F9/12
CPC分类号： D01F9/145 , D01F9/155
摘要： A carbon fiber having a fiber diameter of at least 15 .mu.m, a tensile modulus of elasticity of more than 104 ton/mm.sup.2 and a spread L of graphite crystallites in the direction of axis a of at least 1,000 .ANG. as determined from the powder X-ray spectrum.
摘要翻译：纤维直径至少为15μm，拉伸弹性模量大于104ton / mm2的碳纤维和由α粉末X确定的至少为1000的轴向a的石墨微晶的扩展L 射线谱

93. 发明授权

US5238672A Mesophase pitches, carbon fiber precursors, and carbonized fibers 失效
标题翻译：中间相沥青，碳纤维前体和碳化纤维
公开(公告)号：US5238672A
公开(公告)日：1993-08-24
申请号：US369442
申请日：1989-06-20
申请人： Michael B. Sumner , William P. Hettinger
发明人： Michael B. Sumner , William P. Hettinger
IPC分类号： C10C3/00 , D01F9/155
CPC分类号： D01F9/155 , C10C3/002
摘要： Producing carbon fiber precursors and carbonized fibers comprise by treating a thin film of catalytic pitch at elevated temperature conditions, treating the resulting heavy isotropic pitch by agitating with an inert gas under elevated temperature conditions to form a mesophase pitch, forming green fibers from said mesophase pitch, stabilizing and optionally carbonizing said green fibers to obtain the desired product.
摘要翻译：生产碳纤维前体和碳化纤维包括通过在高温条件下处理催化沥青的薄膜，在高温条件下用惰性气体搅拌处理所得重的各向同性沥青以形成中间相沥青，由所述中间相沥青形成绿色纤维，稳定和任选地碳化所述绿色纤维以获得所需产物。

94. 发明授权

US5156831A Method for producing high strength, melt spun carbon fibers 失效
标题翻译：生产高强度熔融纺丝碳纤维的方法
公开(公告)号：US5156831A
公开(公告)日：1992-10-20
申请号：US34226
申请日：1987-04-02
申请人： Charles C. Fain , Danny D. Edie
发明人： Charles C. Fain , Danny D. Edie
IPC分类号： D01D5/253 , D01F9/14 , D01F9/155 , D01F9/22 , D01F9/32
CPC分类号： D01F9/32 , D01D5/253 , D01F9/14 , D01F9/155 , D01F9/22 , D01F9/322
摘要： Hollow carbon fibers and carbon fibers having a generally C-shaped transverse cross-sectional area are produced by extruding a carbonaceous anisotropic liquid precursor through a spinneret having a capillary with a generally C-shaped cross-sectional area, into a fiber filament, controlling the viscosity of the molten precursor, the pressure of the molten precursor and the linear take-up speed of the filament to yield a fiber filament having a cross-sectional area shaped substantially like the shape of the cross-sectional area of the capillary and further having a line-origin microstructure, rendering the filament infusible, heating the filament in an inert pre-carbonizing environment at a temperature in the range of 600.degree. C. to 1000.degree. C. for 1 to 5 minutes, and heating the filament in an inert carbonizing environment at a temperature in the range of 1550.degree. C. to 1600.degree. C. for 5 to 10 minutes, to substantially increase the tensile strength of the filament. The carbon fiber filament so produced has a line-origin microstructure in which the origin line is located and shaped substantially as a line which constitutes the line formed by uniformly collapsing the perimeter of the transverse cross-sectional area of the fiber filament upon itself. The carbon fiber filament has a tensile strength greater than 200 ksi and as high as the 700 to 800 ksi range, yet a modulus of elasticity on the order of 25-35 msi. The top to bottom outside diameter of the fiber's transverse cross-sectional area is on the order of 30 to 50 microns, and the wall thicknesses are on the order of 8 to 15 microns.
摘要翻译：通过将碳质各向异性液体前体通过具有大致C形横截面积的毛细管的喷丝头挤出到纤维丝中来制造具有大致C形横截面积的中空碳纤维和碳纤维，从而控制熔融前体的粘度，熔融前体的压力和丝的线性吸收速度，以产生纤维长丝，该纤维长丝的截面积基本上类似于毛细管的横截面积的形状，并且还具有线源微结构，使细丝不熔，在惰性预碳化环境中在600℃至1000℃的温度范围内加热丝，持续1至5分钟，并将惰性物质加热至惰性碳化环境在1550℃至1600℃的温度下进行5至10分钟，以显着提高长丝的拉伸强度。如此制造的碳纤维丝具有线状微结构，其中原点线基本上定位成线，该线构成通过将纤维丝的横截面积的周长均匀地折叠在其自身上而形成的线。碳纤维长丝的拉伸强度大于200ksi，高达700至800ksi的范围，弹性模量为25-35毫秒。纤维横向横截面积的顶部到底部的外径约为30至50微米，壁厚约为8至15微米。

95. 发明授权

US5057341A Method of processing carbon fiber precursor from pitchy materials 失效
标题翻译：从沥青材料加工碳纤维前体的方法
公开(公告)号：US5057341A
公开(公告)日：1991-10-15
申请号：US309297
申请日：1989-02-10
申请人： Osamu Ogiso , Hideto Uchida
发明人： Osamu Ogiso , Hideto Uchida
IPC分类号： D01F9/15 , D01F9/155
CPC分类号： D01F9/155 , D01F9/15 , Y10T428/2933 , Y10T428/2962 , Y10T428/30
摘要： Carbon fiber precursors from pitchy materials are processed by applying thereonto an aqueous emulsion containing a single silicone oil or a mixture of silicone oils selected from polydimethyl siloxane, phenyl modified polydimethyl siloxane and aminoalkyl modified polydimethyl siloxane and having kinetic viscosity at 25.degree. C. of 100 centistokes or less, an alkanolamine salt of aliphatic monocarboxylic acid with 8-18 carbon atoms, and one or more non-ionic surfactants selected from polyoxyethylene alkylphenylethers polyoxyethylene alkylates, polyoxyethylene alkylaminoethers, and aliphatic monocarboxylic alkanolamides such that 0.1-5 wt % by solid deposit on fiber from this aqueous emulsion apply to the pitch fibers during any of the processes from the spinning and to the oxidizing.

96. 发明授权

US4895712A Process for producing carbon fiber and graphite fiber 失效
标题翻译：生产碳纤维和石墨纤维的方法
公开(公告)号：US4895712A
公开(公告)日：1990-01-23
申请号：US185110
申请日：1988-04-22
申请人： Kikuji Komine , Hisao Kato , Tsutomu Naito , Takashi Hino , Hiroyuki Kuroda
发明人： Kikuji Komine , Hisao Kato , Tsutomu Naito , Takashi Hino , Hiroyuki Kuroda
IPC分类号： D06M13/00 , D01F9/14 , D01F9/15 , D01F9/155 , D06M13/02 , D06M13/188 , D06M13/322 , D06M13/325 , D06M13/335 , D06M13/35 , D06M13/355 , D06M13/51 , D06M13/513 , D06M15/643 , D06M101/00 , D06M101/12 , D06M101/40
CPC分类号： D01F9/155 , D01F9/15
摘要： A process for producing carbon fiber or graphite fiber is provided. The process comprises spinning a carbonaceous pitch, doubling spun pitch fiber bundles, adding a heat resistant doubling treatment oil, passing the fiber bundles continuously and linearly through an oxygen rich gas, infusibilizing at a temperature of 350.degree. C. or less, then carbonizing or graphitizing infusibilized fiber bundles.

97. 发明授权

US4891126A Mesophase pitch for use in the making of carbon materials and process for producing the same 失效
标题翻译：用于制造碳材料的中间相沥青及其制备方法
公开(公告)号：US4891126A
公开(公告)日：1990-01-02
申请号：US276468
申请日：1988-11-22
申请人： Isao Mochida , Yukio Sakai , Hiroyuki Otsuka
发明人： Isao Mochida , Yukio Sakai , Hiroyuki Otsuka
IPC分类号： C10C3/00 , D01F9/15 , D01F9/155
CPC分类号： D01F9/15 , C10C3/00 , D01F9/155
摘要： Pitch that is obtained from a condensed polycyclic aromatic hydrocarbon and the content of an optically anisotropic phase in which is substantially 100% is disclosed. This mesophase pitch has a H/C atomic ratio of 0.5-1.0, contains naphthenic carbon in an amount of at least 7% of the total carbon, and has a softening point of 180.degree.-400.degree. C. Fibers melt-spun from this mesophase pitch can be converted to carbon or graphite fibers having high strength and modulus of elasticity by a heat treatment which consists of heating to a temperature of 250.degree.-300.degree. C. in an air atmosphere, then heating to 1,000.degree. C. or higher in an inert gas atmosphere. Such mesophase pitch is produced by polymerizing a condensed polycyclic aromatic hydrocarbon for 5-300 minutes at a temperature of 180.degree.-400.degree. C. and at a pressure of 5-100 atmospheres in the presence of 0.1-20 moles of HF and 0.05-1 mole of BF.sub.3 per mole of the condensed polycyclic aromatic hydrocarbon.

98. 发明授权

US4882139A Improved production of carbon fibers 失效
标题翻译：改善碳纤维的生产
公开(公告)号：US4882139A
公开(公告)日：1989-11-21
申请号：US277700
申请日：1988-11-30
申请人： Herbert Beneke , Siegfried Peter
发明人： Herbert Beneke , Siegfried Peter
IPC分类号： C10C3/02 , C10C3/04 , C10C3/10 , D01F9/14 , D01F9/15 , D01F9/155
CPC分类号： D01F9/15 , D01F9/155
摘要： In a process for the production of carbon fibers from high boiling bituminous substances in which a purified and polymerized concentrated carbon fiber precursor is spun into fibers which are oxidized and then carbonized and optionally graphitized, the improvement comprising just before spinning a supercritical gas is dissolved in mesophase pitch at a pressure of 100 to 350 bars and a temperature up to 150.degree. K. below the melting temperature of the mesophase pitch to form a low viscosity melt, separating the latter into an isotropic phase and an anisotropic carbon fiber precursor and spinning the latter into fibers whereby the spinning temperature is lowered and the mesophase contact is increased due to the viscosity lowering activity of the supercritical gas.
摘要翻译：在由高沸点沥青物质生产碳纤维的方法中，将纯化和聚合的浓缩碳纤维前体纺丝成氧化然后碳化并任选石墨化的纤维，在将超临界气体旋转之前的改进溶解在在100至350巴的压力下，中温相沥青的温度高于中间相沥青的熔融温度至150°K，以形成低粘度熔体，将其分离成各向同性相和各向异性碳纤维前体，并纺丝后者变成纤维，由此由于超临界气体的降粘活性，纺丝温度降低并且中间相接触增加。

99. 发明授权

US4865931A Secondary electrical energy storage device and electrode therefor 失效
标题翻译：二次电储能装置及其电极
公开(公告)号：US4865931A
公开(公告)日：1989-09-12
申请号：US678186
申请日：1984-12-04
申请人： Francis P. McCullough, Jr. , Alvin F. Beale, Jr.
发明人： Francis P. McCullough, Jr. , Alvin F. Beale, Jr.
IPC分类号： D01F9/155 , D01F9/22 , D01F9/32 , H01M4/96 , H01M10/05
CPC分类号： H01M10/05 , D01F9/155 , D01F9/22 , D01F9/32 , H01M4/96
摘要： An electrode suitable for use in energy storage devices is described which is made of an assembly of an electrically conductive carbonaceous material having conjugated and preferably polybenzenoid plate-like structures. The carbonaceous material has a Youngs modulus of greater than 1,000,000 psi. The so-defined electrode material does not undergo a substantial change in dimension during repeated electrical charge and discharge cycles. Additionally there is described an energy storage device utilizing the above described electrode.
摘要翻译：描述了适用于能量存储装置的电极，其由具有共轭且优选多苯胺板状结构的导电碳质材料的组件制成。碳质材料的杨氏模量大于1,000,000psi。如此限定的电极材料在重复充电和放电循环期间不会发生尺寸的实质变化。此外，还描述了利用上述电极的能量存储装置。

100. 发明授权

US4861653A Pitch carbon fibers and batts 失效
标题翻译：沥青碳纤维和棉絮
公开(公告)号：US4861653A
公开(公告)日：1989-08-29
申请号：US092217
申请日：1987-09-02
申请人： Robert G. Parrish
发明人： Robert G. Parrish
IPC分类号： D01F9/12 , D01D5/18 , D01F9/14 , D01F9/15 , D01F9/155 , D01F9/32 , D04H1/42
CPC分类号： D01D5/18 , D01F9/15 , D01F9/155 , D01F9/322 , Y10T428/249921 , Y10T428/30 , Y10T442/624 , Y10T442/681 , Y10T442/691
摘要： Mesophase pitch centrifugally spun as described over a lip yields upon stabilization and carbonization with or without graphitization carbon fibers with a lamellar microstructure.

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