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91. 发明授权

US5221720A Fluorided aluminas, catalysts, and polymerization processes 失效
公开(公告)号：US5221720A
公开(公告)日：1993-06-22
申请号：US929969
申请日：1992-08-14
申请人： Max P. McDaniel , Douglas D. Klendworth , Marvin M. Johnson
发明人： Max P. McDaniel , Douglas D. Klendworth , Marvin M. Johnson
IPC分类号： C08F10/00
CPC分类号： C08F10/00
摘要： High surface are aluminas are pre-calcined to form gamma-alumina. In one embodiment, the gamma-alumina is treated with an anhydrous solution of a fluorine-containing compound. In a second embodiment, alumina is precipitated in the pores of the gamma-alumina and then treated with a fluorine-containing compound. In a third embodiment a cogel of aluminum trifluoride and aluminum hydroxide is prepared. The three inventive fluorided alumina supports can be impregnated with a transition metal, preferably chromium, to form a catalyst system which can be used to polymerize mono-1-olefins.

92. 发明授权

US5221654A Fluorided aluminas, catalysts, and polymerization processes 失效
标题翻译：氟化氧化铝，催化剂和聚合方法
公开(公告)号：US5221654A
公开(公告)日：1993-06-22
申请号：US930961
申请日：1992-08-14
申请人： Max P. McDaniel , Douglas D. Klendworth , Marvin M. Johnson
发明人： Max P. McDaniel , Douglas D. Klendworth , Marvin M. Johnson
IPC分类号： C08F10/00
CPC分类号： C08F10/00
摘要： High surface are aluminas are pre-calcined to form gamma-alumina. In one embodiment, the gamma-alumina is treated with an anhydrous solution of a fluorine-containing compound. In a second embodiment, alumina is precipitated in the pores of the gamma-alumina and then treated with a fluorine-containing compound. In a third embodiment a cogel of aluminum trifluoride and aluminum hydroxide is prepared. The three inventive fluorided alumina supports can be impregnated with a transition metal, preferably chromium, to form a catalyst system which can be used to polymerize mono-1-olefins.
摘要翻译：高表面是氧化铝被预煅烧以形成γ-氧化铝。在一个实施方案中，γ-氧化铝用含氟化合物的无水溶液处理。在第二实施方案中，氧化铝在γ-氧化铝的孔中沉淀，然后用含氟化合物处理。在第三个实施方案中，制备三氟化铝和氢氧化铝的共凝胶。三种本发明的氟化氧化铝载体可以用过渡金属（优选铬）浸渍以形成可用于聚合单-1-烯烃的催化剂体系。

93. 发明授权

US5219962A Fluorided aluminas, catalysts, and polymerization processes 失效
公开(公告)号：US5219962A
公开(公告)日：1993-06-15
申请号：US931094
申请日：1992-08-14
申请人： Max P. McDaniel , Douglas D. Klendworth , Marvin M. Johnson
发明人： Max P. McDaniel , Douglas D. Klendworth , Marvin M. Johnson
IPC分类号： C08F10/00
CPC分类号： C08F10/00
摘要： High surface are aluminas are pre-calcined to form gamma-alumina. In one embodiment, the gamma-alumina is treated with an anhydrous solution of a fluorine-containing compound. In a second embodiment, alumina is precipitated in the pores of the gamma-alumina and then treated with a fluorine-containing compound. In a third embodiment a cogel of aluminum trifluoride and aluminum hydroxide is prepared. The three inventive fluorided alumina supports can be impregnated with a transition metal, preferably chromium, to form a catalyst system which can be used to polymerize mono-1-olefins.

94. 发明授权

US5032232A Extractive distillation of hydrocarbon mixtures 失效
标题翻译：烃混合物的萃取蒸馏
公开(公告)号：US5032232A
公开(公告)日：1991-07-16
申请号：US606690
申请日：1990-10-31
申请人： Fu-Ming Lee , Ronald E. Brown , Marvin M. Johnson
发明人： Fu-Ming Lee , Ronald E. Brown , Marvin M. Johnson
IPC分类号： B01D3/40 , C07C7/08
CPC分类号： B01D3/40 , C07C7/08
摘要： Extractive distillation processes for separating aromatic hydrocarbon(s) or cycloalkane(s) or alkene(s) from close-boiling alkane(s) are carried out with a solvent including at least one N-alkyl-2-thiopyrrolidone compound, preferably N-methyl-2-thiopyrrolidone. Optionally, the solvent additionally contains a cosolvent, preferably tetraethylene glycol or N-(.beta.-mercaptoethyl)-2-pyrrolidone or unsubstituted sulfolane.
摘要翻译：用于从近沸点烷烃分离芳族烃或环烷烃或烯烃的萃取蒸馏方法用包括至少一种N-烷基-2-硫代吡咯烷酮化合物的溶剂进行，优选N- 甲基-2-硫代吡咯烷酮。任选地，溶剂另外含有共溶剂，优选四甘醇或N-（β-巯基乙基）-2-吡咯烷酮或未取代的环丁砜。

95. 发明授权

US4956476A Preparation of thiolactams 失效
标题翻译：硫醇内酯的制备
公开(公告)号：US4956476A
公开(公告)日：1990-09-11
申请号：US486709
申请日：1990-03-01
申请人： Alan D. Eastman , Marvin M. Johnson , Richard D. Skinner
发明人： Alan D. Eastman , Marvin M. Johnson , Richard D. Skinner
IPC分类号： C07D207/24 , C07D227/06
CPC分类号： C07D207/24 , C07D227/06
摘要： The reaction of lactams (preferably N-methyl-2-pyrrolidone) with hydrogen sulfide to thiolactams (preferably N-methyl-2-thiopyrrolidone) is conducted in the presence of a catalyst consisting essentially of alumina.
摘要翻译：内酰胺（优选N-甲基-2-吡咯烷酮）与硫化氢与硫醇内酯（优选N-甲基-2-硫代吡咯烷酮）的反应在基本上由氧化铝组成的催化剂的存在下进行。

96. 发明授权

US4656230A Hydrogenation process 失效
标题翻译：氢化过程
公开(公告)号：US4656230A
公开(公告)日：1987-04-07
申请号：US754388
申请日：1985-07-12
申请人： Yen-Shin Shyr , Rex L. Bobsein , Marvin M. Johnson
发明人： Yen-Shin Shyr , Rex L. Bobsein , Marvin M. Johnson
IPC分类号： C08C19/02 , C08F8/04
CPC分类号： C08F8/04 , C08C19/02
摘要： Process of preventing and/or reducing the rate of catalyst deactivation during hydrogenation of olefinic materials, especially olefinic polymers such as diene-containing polymers, that contain contaminants and/or catalyst poisons which comprises carrying out the hydrogenation in the presence of a small but finite amount of a lower alkanol, such as methanol, which amount is sufficient to substantially reduce catalyst poisoning due to contaminants present in the hydrogenation feed.
摘要翻译：含有污染物和/或催化剂毒物的烯烃材料，特别是烯烃聚合物如含二烯的聚合物在氢化期间预防和/或降低催化剂失活速率的方法包括在有限的条件下进行氢化低级烷醇如甲醇的量，其量足以基本上减少由于加氢进料中存在的污染物引起的催化剂中毒。

97. 发明授权

US4593146A Isomerization process and catalyst therefor 失效
标题翻译：异构化方法和催化剂
公开(公告)号：US4593146A
公开(公告)日：1986-06-03
申请号：US718241
申请日：1985-03-29
申请人： Marvin M. Johnson , Gerhard P. Nowack , Max P. McDaniel
发明人： Marvin M. Johnson , Gerhard P. Nowack , Max P. McDaniel
IPC分类号： C07C5/25
CPC分类号： C07C5/2537 , C07C5/2556
摘要： Aliphatic olefinic hydrocarbons are isomerized in the presence of a catalyst consisting essentially of elemental chromium or a chromium compound and an aluminum phosphate support wherein the phosphorus/aluminum atomic ratio of the support is less than 1.
摘要翻译：脂肪族烯烃在基本上由元素铬或铬化合物和磷酸铝载体组成的催化剂存在下异构化，其中载体的磷/铝原子比小于1。

98. 发明授权

US4558165A Chromium phosphate catalyst 失效
公开(公告)号：US4558165A
公开(公告)日：1985-12-10
申请号：US725052
申请日：1985-04-19
申请人： Marvin M. Johnson , Gerhard P. Nowack
发明人： Marvin M. Johnson , Gerhard P. Nowack
IPC分类号： C07C2/86 , C07C41/09
CPC分类号： C07C41/09 , C07C2/864 , C07C2527/167
摘要： An amorphous chromium (III) phosphate catalyst is used in alkylating aromatics and in the dehydration of alcohols to ethers.

99. 发明授权

US4535070A Acrylamide polymer used to reduce fines in aluminum phosphate gel 失效
标题翻译：丙烯酰胺聚合物用于减少磷酸铝凝胶中的细粉
公开(公告)号：US4535070A
公开(公告)日：1985-08-13
申请号：US565251
申请日：1983-12-23
申请人： Max P. McDaniel , Marvin M. Johnson , Gil R. Hawley , John Westerman , Paul D. Smith
发明人： Max P. McDaniel , Marvin M. Johnson , Gil R. Hawley , John Westerman , Paul D. Smith
IPC分类号： B01J27/16 , C01B25/36 , C08F10/00 , B01J27/14 , B01J31/02 , C01B25/26
CPC分类号： C01B25/36 , B01J27/16 , C08F10/00
摘要： Aluminum phosphate having reduced fines is produced by gelling said aluminum phosphate in the presence of an acrylamide polymer. The resulting support is of primary utility as a base for a chromium olefin polymerization catalyst but is also suitable as a support for titanium catalysts such as TiCl.sub.3, TiCl.sub.4 /MgCl.sub.2 and other conventional catalysts typically associated with polymerization of propylene.
摘要翻译：具有减少的细粉的磷酸铝是通过在丙烯酰胺聚合物的存在下使所述磷酸铝胶凝而产生的。得到的载体作为铬烯烃聚合催化剂的基础是主要用途，但也适用作钛催化剂如TiCl 3，TiCl 4 / MgCl 2和通常与丙烯聚合相关的常规催化剂的载体。

100. 发明授权

US4444963A Polymerization process using catalysts comprising chromium on silica/phosphate support 失效
标题翻译：使用在二氧化硅/磷酸盐载体上包含铬的催化剂的聚合方法
公开(公告)号：US4444963A
公开(公告)日：1984-04-24
申请号：US423595
申请日：1982-09-27
申请人： Max P. McDaniel , Marvin M. Johnson
发明人： Max P. McDaniel , Marvin M. Johnson
IPC分类号： C08F10/00 , C08F4/02 , C08F4/24 , C08F4/62
CPC分类号： C08F10/00
摘要： In one embodiment of this invention, a chromium component is supported on a silica/aluminum orthophosphate combination and used with an organometal cocatalyst. In accordance with other embodiments of the invention, the silica/phosphate combination for a chromium catalyst support is produced by either impregnating a silica xerogel with aluminum phosphate or boron phosphate, precipitating aluminum phosphate in the presence of a silica hydrogel, or physically mixing silica and aluminum phosphate xerogels. The resulting catalysts are capable of producing high melt flow olefin polymers and exhibit high activity. The resulting polymers have many unusual and desirable characteristics, such as high density and good environmental stress crack resistance.
摘要翻译：在本发明的一个实施方案中，铬组分负载在二氧化硅/正磷酸铝组合上并与有机金属助催化剂一起使用。根据本发明的其它实施方案，用于铬催化剂载体的二氧化硅/磷酸盐组合是通过用磷酸铝或磷酸硼浸渍二氧化硅干凝胶，在二氧化硅水凝胶的存在下沉淀磷酸铝，或物理混合二氧化硅和磷酸铝干凝胶。所得催化剂能够生产高熔体流动的烯烃聚合物并表现出高的活性。所得到的聚合物具有许多不寻常和期望的特征，例如高密度和良好的耐环境应力开裂性。

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