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91. 发明授权

US07649062B2 Solid titanium catalyst component, catalyst for polymerization of olefin and process for producing olefin polymer 有权
标题翻译：固体钛催化剂组分，烯烃聚合催化剂和烯烃聚合物生产方法
公开(公告)号：US07649062B2
公开(公告)日：2010-01-19
申请号：US11878740
申请日：2007-07-26
申请人： Kazuhisa Matsunaga , Hisao Hashida , Toshiyuki Tsutsui , Kunio Yamamoto , Atsushi Shibahara , Tetsunori Shinozaki
发明人： Kazuhisa Matsunaga , Hisao Hashida , Toshiyuki Tsutsui , Kunio Yamamoto , Atsushi Shibahara , Tetsunori Shinozaki
IPC分类号： C08F4/42
CPC分类号： B01J31/0209 , B01J31/0212 , B01J31/128 , B01J31/143 , B01J31/38 , C08F10/00 , C08F110/06 , C08F110/08 , C08F110/14 , C08F210/06 , C08F4/6543 , C08F4/651 , C08F2500/04 , C08F2500/18 , C08F210/16 , C08F4/6465
摘要： A solid titanium catalyst component (I) of the present invention is characterized in that it contains titanium, magnesium, halogen, and a cyclic ester compound (a) represented by the following formula (1): wherein n is an integer of 5 to 10; R2 and R3 are each independently COOR1 or R, and at least one of R2 and R3 is COOR1; a single bond (excluding Ca—Ca bonds, and a Ca—Cb bond in the case where R3 is R) in the cyclic backbone may be replaced with a double bond; a plurality of R1's are each independently a monovalent hydrocarbon group having 1 to 20 carbon atoms; and a plurality of R's are each independently a hydrogen atom or a substituent, but at least one of R's is not a hydrogen atom. When using this solid titanium catalyst component (I), an olefin polymer having a broad molecular weight distribution can be produced.
摘要翻译：本发明的固体钛催化剂组分（I）的特征在于它含有钛，镁，卤素和由下式（1）表示的环酯化合物（a）：其中n是5至10的整数 ; R2和R3各自独立地是COOR1或R，R2和R3中的至少一个是COOR1; 环状骨架中的单键（不包括Ca-Ca键，在R3为R的情况下为Ca-Cb键）可以被双键取代; 多个R 1各自独立地为具有1〜20个碳原子的一价烃基; 并且多个R各自独立地为氢原子或取代基，但R中的至少一个不是氢原子。当使用该固体钛催化剂组分（I）时，可以生产具有宽分子量分布的烯烃聚合物。

92. 发明申请

US20080125555A1 Catalyst for olefin polymerization and process for olefin polymerization 有权
标题翻译：用于烯烃聚合的催化剂和烯烃聚合方法
公开(公告)号：US20080125555A1
公开(公告)日：2008-05-29
申请号：US11878739
申请日：2007-07-26
申请人： Kazuhisa Matsunaga , Hisao Hashida , Toshiyuki Tsutsui , Kunio Yamamoto , Atsushi Shibahara , Tetsunori Shinozaki
发明人： Kazuhisa Matsunaga , Hisao Hashida , Toshiyuki Tsutsui , Kunio Yamamoto , Atsushi Shibahara , Tetsunori Shinozaki
IPC分类号： C08F4/72 , B01J31/12
CPC分类号： C08F10/00 , C08F4/651 , C08F4/6543
摘要： A catalyst for olefin polymerization of the present invention includes a solid titanium catalyst component (I) including titanium, magnesium, halogen, and a cyclic ester compound (a) represented by the following formula (1): wherein n is an integer of 5 to 10; R2 and R3 are each independently COOR1 or R, and at least one of R2 and R3 is COOR1; a single bond (excluding Ca—Ca bonds, and a Ca—Cb bond in the case where R3 is R) in the cyclic backbone may be replaced with a double bond; a plurality of R1's are each independently a monovalent hydrocarbon group having 1 to 20 carbon atoms; and a plurality of R's are each independently a hydrogen atom or a substituent, but at least one of R's is not a hydrogen atom, and an organometal compound catalyst component (II). When this catalyst for olefin polymerization is used, an olefin polymer having a broad molecular weight distribution can be produced.
摘要翻译：本发明的烯烃聚合用催化剂包括由下述通式（1）表示的钛，镁，卤素和环状酯化合物（a）的固体钛催化剂成分（I）：其中n为5〜 10; R 2和R 3各自独立地为COOR 1或R 2，R 2和R 2中的至少一个为R ^{3 是COOR 1; 单键（不包括C ^{a a 键和C a 环状骨架中R 3为R的情况）可以用双键代替; 多个R 1各自独立地为具有1〜20个碳原子的一价烃基; 和多个R各自独立地为氢原子或取代基，但R中的至少一个不为氢原子，和有机金属化合物催化剂成分（II）。当使用用于烯烃聚合的催化剂时，可以生产具有宽分子量分布的烯烃聚合物。}}

93. 发明申请

US20070114273A1 Transaction cooperation method in branch office system 审中-公开
标题翻译：分公司系统交易合作方式
公开(公告)号：US20070114273A1
公开(公告)日：2007-05-24
申请号：US11513381
申请日：2006-08-31
申请人： Toshiyuki Tsutsui , Kazuma Kurata , Akihito Itou , Masataka Itakura , Tetsuhide Ikeda
发明人： Toshiyuki Tsutsui , Kazuma Kurata , Akihito Itou , Masataka Itakura , Tetsuhide Ikeda
IPC分类号： G07F19/00 , G06Q40/00
CPC分类号： G06Q20/385 , G06Q20/40 , G06Q20/4014 , G06Q40/02
摘要： A cooperating process between respective terminals (apparatuses) in a branch office system for a transaction for a customer who does not have an account or a customer who is supposed to open an account (namely, a customer who does not have a card) is disclosed. In the case where a customer does not have an account, executable transactions are extracted and authority (temporary authority) for the input transaction is issued. The authority is used to operate plural transaction terminals in a cooperating manner so as to enable the transactions. The authority includes issuing of a transaction card. Further, the authority includes using biological information including a vein of a finger or a palm in order to specify an individual.
摘要翻译：公开了在没有帐户的客户的交易的分支机构系统中的各个终端（设备）之间的合作过程，或者应该开立账户的顾客（即，没有卡的客户）。在客户没有帐户的情况下，提取可执行交易，并且发出用于输入交易的权限（临时权限）。该权限用于以协作的方式操作多个交易终端，以便能够进行交易。该机构包括发行交易卡。此外，权威部门包括使用包括手指或手掌的静脉的生物信息来指定个体。

94. 发明授权

US06774190B1 Ethylene copolymer composition 失效
标题翻译：乙烯共聚物组成
公开(公告)号：US06774190B1
公开(公告)日：2004-08-10
申请号：US09949675
申请日：2001-09-12
申请人： Mamoru Takahashi , Akira Todo , Seiichi Ikeyama , Toshiyuki Tsutsui , Shinya Matsunaga , Norio Kaneshige
发明人： Mamoru Takahashi , Akira Todo , Seiichi Ikeyama , Toshiyuki Tsutsui , Shinya Matsunaga , Norio Kaneshige
IPC分类号： C08L2304
CPC分类号： C08L23/0815 , C08L23/06 , C08L2314/06 , Y10T428/1345 , C08L2666/04
摘要： An ethylene copolymer composition comprising an ethylene/&agr;-olefin copolymer (A-1), which has a density, a melt flow rate (MFR), an amount of a n-decane-soluble portion in the specific ranges and whose melt tension (MT) at 190° C. and MFR satisfy the relation MT>2.2×MFR−0.84, and one (co)polymer selected from the group consisting of (B-1) a low-density polyethylene obtained by high-pressure radical polymerization, (B-2) a crystalline polyolefin and (B-3) an olefin type elastomer. Also disclosed is an ethylene copolymer composition comprising an ethylene/&agr;-olefin copolymer composition and the low-density polyethylene (B-1) obtained by high-pressure radical polymerization, said ethylene/&agr;-olefin copolymer (A-2) and (A-3) both having physical properties similar to those of the above ethylene/&agr;-olefin copolymer (A-1) and having intrinsic viscosities different from each other. The ethylene copolymer compositions of the invention are excellent in heat stability and moldability, and able to form films of high transparency, high mechanical strength and anti-blocking resistance.
摘要翻译：一种包含乙烯/α-烯烃共聚物（A-1）的乙烯共聚物组合物，其具有密度，熔体流动速率（MFR），特定范围内的正癸烷可溶部分的量及其熔体张力（ MT）和MFR满足MT> 2.2×MFR <-0.84>的关系，以及选自（B-1）由（B-1）组成的组中的一种（共）聚合物，通过高压自由基聚合获得的低密度聚乙烯，（B-2）结晶聚烯烃和（B-3）烯烃类弹性体。还公开了包含乙烯/α-烯烃共聚物组合物和通过高压自由基聚合获得的低密度聚乙烯（B-1）的乙烯共聚物组合物，所述乙烯/α-烯烃共聚物（A-2）和（A -3），其物理性质与上述乙烯/α-烯烃共聚物（A-1）的物理性质相似，并且具有彼此不同的特性粘度。本发明的乙烯共聚物组合物的热稳定性和成型性优异，能够形成高透明度，高机械强度和抗粘连性的薄膜。

95. 发明授权

US06723794B2 Olefin thermoplastic elastomer composition comprising crystalline polyolefin resin and ethylene/&agr;-olefin/nonconjugated polyene copolymer rubber 有权
标题翻译：包含结晶聚烯烃树脂和乙烯/α-烯烃/非共轭多烯共聚物橡胶的烯烃热塑性弹性体组合物
公开(公告)号：US06723794B2
公开(公告)日：2004-04-20
申请号：US10066575
申请日：2002-02-06
申请人： Masaaki Kawasaki , Keiji Okada , Tetsuo Tojo , Kyoko Kobayashi , Yuichi Itoh , Akira Uchiyama , Toshiyuki Tsutsui , Toshihiro Sagane
发明人： Masaaki Kawasaki , Keiji Okada , Tetsuo Tojo , Kyoko Kobayashi , Yuichi Itoh , Akira Uchiyama , Toshiyuki Tsutsui , Toshihiro Sagane
IPC分类号： C08L2302
CPC分类号： C08L23/02 , A61J1/03 , B65D23/003 , B65D51/28 , C08K5/14 , C08L23/0815 , C08L23/10 , C08L23/142 , C08L23/16 , C08L23/22 , C08L91/00 , C08L2205/03 , C08L2207/04 , C08L2312/00 , C08L2666/04
摘要： An olefin thermoplastic elastomer composition comprises a crystalline polyolefin resin (A) and an ethylene/&agr;-olefin/nonconjugated polyene copolymer rubber (B), and optionally a softener (C) and/or an inorganic filler (D), in a specific ratio. The copolymer rubber (B) is prepared by the use of a metallocene catalyst and comprises ethylene, an &agr;-olefin of 3 to 20 carbon atoms and a nonconjugated polyene. This composition ca provide molded products of more excellent tensile strength, elongation at break, elastomeric properties (elongation set, permanent compression set, etc.), heat resistance and low-temperature properties than the conventional non-crosslinked olefin thermoplastic elastomers, even if the composition is in the non-crosslinked form. The composition in the partially or completely crosslinked form can provided molded products of more excellent low-temperature properties, tensile strength, elongation at break and elastomeric properties than the conventional vulcanized rubbers.
摘要翻译：烯烃热塑性弹性体组合物包含结晶聚烯烃树脂（A）和乙烯/α-烯烃/非共轭多烯共聚物橡胶（B）和任选的软化剂（C）和/或无机填料（D）。共聚物橡胶（B）通过使用茂金属催化剂制备，包括乙烯，3-20个碳原子的α-烯烃和非共轭多烯。该组合物提供比常规非交联烯烃热塑性弹性体更优异的拉伸强度，断裂伸长率，弹性体性能（伸长率设定，永久压缩变形等），耐热性和低温性能的成型产品，即使组合物为非交联形式。部分或完全交联形式的组合物可以提供比常规硫化橡胶更优异的低温性能，拉伸强度，断裂伸长率和弹性体性能的成型产品。

96. 发明授权

US06303713B1 Graft modified ethylene &agr;-olefin copolymer obtained by graft copolymerzing an ethylene/&agr;-olefin copolymer with a polar monomer 有权
标题翻译：通过将乙烯/α-烯烃共聚物与极性单体接枝共聚获得的接枝改性乙烯α-烯烃共聚物
公开(公告)号：US06303713B1
公开(公告)日：2001-10-16
申请号：US09377918
申请日：1999-08-20
申请人： Toshiyuki Tsutsui , Ken Yoshitsugu , Mamoru Takahashi , Akira Todo , Seiji Ohta , Hajime Inagaki
发明人： Toshiyuki Tsutsui , Ken Yoshitsugu , Mamoru Takahashi , Akira Todo , Seiji Ohta , Hajime Inagaki
IPC分类号： C08F444
CPC分类号： C08J5/18 , C08F4/65904 , C08F4/65912 , C08F4/65916 , C08F4/65925 , C08F4/65927 , C08F10/00 , C08F210/16 , C08F255/00 , C08F255/02 , C08J2323/08 , C08L23/02 , C08L23/0815 , C08L51/06 , Y10S526/943 , C08L2666/24 , C08L2666/04 , C08F210/08 , C08F2500/12 , C08F2500/11 , C08F2500/03 , C08F2500/26 , C08F210/14 , C08F2500/17
摘要： A graft modified ethylene/&agr;-olefin copolymer obtained by graft polymerizing an ethylene/&agr;-olefin of 3 to 20 carbon atoms copolymerizing with a polar monomer in the presence of a catalyst for olefin polymerization comprising an organoaluminum oxy-compound (a) and at least two kinds of transition metal compounds (b). This ethylene/&agr;-olefin copolymer has high melt tension and high flowability. An ethylene copolymer composition comprising the above-mentioned graft modified ethylene/&agr;-olefin copolymer and polyolefin. The graft modified ethylene/&agr;-olefin copolymer of the invention is excellent in heat stability and moldability. From this copolymer, a film having a high transparency and good adhesion to highly polar materials can be produced. The ethylene copolymer composition of the invention is excellent in heat stability and moldability. From this composition, a film having high transparency and good adhesion to highly polar materials can be produced.
摘要翻译：在烯烃聚合催化剂存在下，将极性单体与极性单体共聚3-20个碳原子的乙烯/α-烯烃接枝聚合得到的接枝改性乙烯/α-烯烃共聚物，包括有机铝氧化合物（a）和至少两种过渡金属化合物（b）。该乙烯/α-烯烃共聚物具有高熔体张力和高流动性。一种包含上述接枝改性的乙烯/α-烯烃共聚物和聚烯烃的乙烯共聚物组合物。本发明的接枝改性乙烯/α-烯烃共聚物的热稳定性和成型性优异。从该共聚物可以制造具有高透明性和对高极性材料的良好粘附性的膜。本发明的乙烯共聚物组合物的热稳定性和成型性优异。通过该组合物，可以制造具有高透明性和对高极性材料的良好粘附性的膜。

97. 发明授权

US6133490A Dispersant for pigments for aromatic polymers 有权
标题翻译：用于芳族聚合物颜料的分散剂
公开(公告)号：US6133490A
公开(公告)日：2000-10-17
申请号：US155479
申请日：1998-09-29
申请人： Hideo Toyoda , Hideki Sakai , Kenichi Morizono , Toshiyuki Tsutsui
发明人： Hideo Toyoda , Hideki Sakai , Kenichi Morizono , Toshiyuki Tsutsui
IPC分类号： C08L101/00 , C08F4/659 , C08F4/6592 , C08F210/02 , C08F212/08 , C10L1/16 , C10G73/36 , C10M101/02 , C10M107/00 , C10M143/00
CPC分类号： C08F210/02 , C08F4/65912 , C08F4/65927
摘要： A dispersant for pigments for aromatic polymers, which is superior not only in the ability of dispersing pigments in aromatic polymers but also in attaining high transparency and stability of the resulting color, while avoiding grafting step and attaining a lower production cost. The dispersant for pigments for aromatic polymers comprises a wax composed of a random copolymer of ethylene with an aromatic vinyl compound, which has a content of structural unit derived from ethylene of 99-10% by weight and a content of structural unit derived form the aromatic vinyl compound of 1-90% by weight and exhibiting an intrinsic viscosity of 0.04-0.6 dl/g.
摘要翻译： PCT No.PCT / JP98 / 00374 Sec。 371日期：1998年9月29日 102（e）1998年9月29日PCT PCT 1998年1月29日PCT公布。公开号WO98 / 33852 日期1998年8月6日A用于芳族聚合物颜料的分散剂，其不仅在颜料分散在芳族聚合物中的能力，而且在获得所得颜色的高透明度和稳定性方面优异，同时避免接枝步骤并获得较低的生产成本。用于芳族聚合物颜料的分散剂包括由乙烯与芳族乙烯基化合物的无规共聚物组成的蜡，其具有衍生自乙烯的结构单元的含量为99-10重量％，衍生自芳族化合物的结构单元的含量乙烯基化合物为1-90重量％，特性粘度为0.04-0.6dl / g。

98. 发明授权

US6063726A Catalyst for polymerizing alpha-olefins and process for polymerization 失效
标题翻译：用于聚合α-烯烃的催化剂和聚合方法
公开(公告)号：US6063726A
公开(公告)日：2000-05-16
申请号：US862174
申请日：1997-05-22
申请人： Mamoru Kioka , Akinori Toyota , Norio Kashiwa , Toshiyuki Tsutsui
发明人： Mamoru Kioka , Akinori Toyota , Norio Kashiwa , Toshiyuki Tsutsui
IPC分类号： C08F4/02 , C08F4/655 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F10/10 , C08F110/02 , C08F4/64
CPC分类号： C08F10/00 , C08F10/10 , C08F110/02 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F4/65925 , Y10S526/901 , Y10S526/943
摘要： The invention relates to a polymerization catalyst for alpha-olefins and a process for polymerizing alpha-olefins. The catalyst comprises a component having a transition metal compound supported on a carrier and an aluminoxane. The carrier may be pre-treated with an organometallic compound, a halogen-containing silicon compound or an aluminoxane. Alternatively, the above two catalyst components are subjected to preliminary polymerization of olefins. The catalyst of this invention enables the production of a spherical polymer having a good particle size distribution, an excellent bulk density and a narrow molecular weight distribution in a slurry polymerization method or a vapor-phase polymerization method, particulary the vapor-phase polymerization method. When applied to the copolymerization of at least two olefins, the catalyst has excellent polymerization activity such that an olefin copolymer having a narrow molecular weight distribution and a narrrow composition distribution is obtained.
摘要翻译：本发明涉及α-烯烃的聚合催化剂和α-烯烃的聚合方法。催化剂包含负载在载体上的过渡金属化合物和铝氧烷的组分。载体可以用有机金属化合物，含卤素的硅化合物或铝氧烷进行预处理。或者，将上述两种催化剂组分进行烯烃的预聚合。本发明的催化剂能够制备在淤浆聚合法或气相聚合法中具有良好的粒度分布，优异的堆积密度和窄分子量分布的球形聚合物，特别是气相聚合法。当应用于至少两种烯烃的共聚时，催化剂具有优异的聚合活性，从而获得具有窄分子量分布和叙述组成分布的烯烃共聚物。

99. 发明授权

US6040407A Chain polyene group-containing norbornene compound and unsaturated ethylene copolymer using the same 失效
标题翻译：含链多烯基的降冰片烯化合物和使用其的不饱和乙烯共聚物
公开(公告)号：US6040407A
公开(公告)日：2000-03-21
申请号：US860442
申请日：1997-06-26
申请人： Tatsuyoshi Ishida , Masaaki Yasuda , Hitoshi Onishi , Noriaki Kihara , Toshiyuki Tsutsui , Toshihiro Sagane , Masaaki Kawasaki , Hidenari Nakahama
发明人： Tatsuyoshi Ishida , Masaaki Yasuda , Hitoshi Onishi , Noriaki Kihara , Toshiyuki Tsutsui , Toshihiro Sagane , Masaaki Kawasaki , Hidenari Nakahama
IPC分类号： C07C2/50 , C07C13/43 , C08F210/18 , C08F10/02
CPC分类号： C08F210/18 , C07C13/43 , C07C2/50 , C07C2102/42
摘要： The chain polyene-group containing norbornene compound of the invention is represented by the formula [I]: ##STR1## wherein n is an integer of 1 to 5, R.sup.1 is an alkyl group of 1 to 5 carbon atoms, and R.sup.2 and R.sup.3 are each independently a hydrogen atom or an alkyl group of 1 to 5 carbon atoms.The unsaturated ethylene copolymer of the invention is a random copolymer of 30 to 92% by mol of (i) ethylene units, 6 to 70% by mol of (ii) specific .alpha.-olefin units and 0.1 to 30% by mol of (iii) units derived from the norbornene compound [I], where the molar ratio of (i)/(ii) is in the range of 40/60 to 92/8 and the unit (iii) is represented by the specific formula, and has an intrinsic viscosity [.eta.] of 0.05 to 10 dl/g.The novel unsaturated ethylene copolymer is excellent in weathering resistance, heat resistance and ozone resistance and has a high vulcanizing rate.
摘要翻译： PCT No.PCT / JP95 / 02655第 371日期：1997年6月26日 102（e）日期1997年6月26日PCT 1995年12月25日PCT PCT。 WO96 / 20150 PCT出版物日本1996年7月4日本发明的含链多烯基的降冰片烯化合物由式[I]表示：其中n为1〜5的整数，R1为碳原子数1〜5的烷基，R2和 R 3各自独立地为氢原子或1〜5个碳原子的烷基。本发明的不饱和乙烯共聚物为（i）乙烯单元为30〜92摩尔％，（ii）特定α-烯烃单元为6〜70摩尔％，（iii）为0.1〜30摩尔％）衍生自降冰片烯化合物[I]的单元，其中（i）/（ii）的摩尔比在40/60至92/8的范围内，单元（iii）由具体式表示，并且具有特性粘度η为0.05-10dl / g。新型不饱和乙烯共聚物耐候性，耐热性和耐臭氧性优异，硫化速度高。

100. 发明授权

US6013743A Process for polymerization of alpha-olefins 失效
标题翻译： α-烯烃聚合方法
公开(公告)号：US6013743A
公开(公告)日：2000-01-11
申请号：US105221
申请日：1998-06-26
申请人： Toshiyuki Tsutsui , Akinori Toyota , Norio Kashiwa
发明人： Toshiyuki Tsutsui , Akinori Toyota , Norio Kashiwa
IPC分类号： C08F4/642 , C08F210/16 , C08F4/64
CPC分类号： C08F4/642 , C08F210/16 , Y10S526/943
摘要： A process for producing an alpha-olefin polymer, which comprises polymerizing an alpha-olefin in the presence of a catalyst formed from (A) a solid catalyst component comprising an inorganic carrier and deposited thereon a compound of a transition metal of Group IVB of the periodic table treated with an organometallic compound, and (B) an aluminoxane.
摘要翻译：一种制备α-烯烃聚合物的方法，其包括在由（A）包含无机载体的固体催化剂组分形成的催化剂存在下聚合α-烯烃，并将其上沉积有第ⅣB族过渡金属的化合物用有机金属化合物处理的周期表，和（B）铝氧烷。

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