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1. 发明授权

US06869508B2 Physical vapor deposition apparatus and process 有权
标题翻译：物理气相沉积装置及工艺
公开(公告)号：US06869508B2
公开(公告)日：2005-03-22
申请号：US10063808
申请日：2002-05-15
申请人： Ramgopal Darolia , Reed Roeder Corderman , Joseph David Rigney , Richard Arthur Nardi, Jr. , Michael James Weimer
发明人： Ramgopal Darolia , Reed Roeder Corderman , Joseph David Rigney , Richard Arthur Nardi, Jr. , Michael James Weimer
IPC分类号： C23C14/16 , C23C14/24 , C23C14/30 , C23C14/34 , C23C16/00 , H05H1/24
CPC分类号： B82Y10/00 , C23C14/16 , C23C14/246 , C23C14/30
摘要： A PVD process and apparatus (120) for depositing a coating (132) from multiple sources (110, 111) of different materials. The process and apparatus (120) are particulaity intended to deposit a beta-nickel aluminide coating (132) containing one or more elements whose vapor pressures are lower than NiAl. The PVD process and apparatus (120) entail feeding at least two materials (110, 111) into a coating chamber (122) and evaporating the materials (110, 111) at different rates from separate molten pools (114, 115) thereof. Articles (130) to be coated are suspended within the coating chamber (122), and transported with a support apparatus (118) relative to the two molten pools (114, 115) so as to deposit a coating (132) with a controlled composition that is a mixture of the first and second materials (110, 111).
摘要翻译：一种用于从不同材料的多个源（110,111）沉积涂层（132）的PVD工艺和设备（120）。该方法和装置（120）特别用于沉积含有一种或多种蒸气压低于NiAl的元素的β-镍铝化物涂层（132）。 PVD工艺和设备（120）需要将至少两种材料（110,111）进料到涂覆室（122）中并且以与其分离的熔池（114,115）不同的速率蒸发材料（110,111）。待涂覆的制品（130）悬浮在涂覆室（122）内，并相对于两个熔池（114,115）用支撑装置（118）运输，以便沉积具有受控组合物的涂层（132）即第一和第二材料（110,111）的混合物。

2. 发明授权

US06620524B2 Nickel aluminide coating and coating systems formed therewith 有权
标题翻译：由此形成的铝化镍涂层和涂层系统
公开(公告)号：US06620524B2
公开(公告)日：2003-09-16
申请号：US10044618
申请日：2002-01-11
申请人： Jeffrey Allan Pfaendtner , Joseph David Rigney , Ramgopal Darolia , Reed Roeder Corderman , Richard Arthur Nardi, Jr.
发明人： Jeffrey Allan Pfaendtner , Joseph David Rigney , Ramgopal Darolia , Reed Roeder Corderman , Richard Arthur Nardi, Jr.
IPC分类号： B32B1504
CPC分类号： C23C28/321 , C23C28/345 , C23C28/3455 , C23C30/00 , Y10T428/12535 , Y10T428/1259 , Y10T428/12611 , Y10T428/12618 , Y10T428/1275 , Y10T428/12806 , Y10T428/12861 , Y10T428/12944
摘要： A predominantly beta-phase NiAl overlay coating for use as an environmental coating or a TBC bond coat for articles used in hostile thermal environments, such as components of a gas turbine engine. The coating contains up to about 4 atomic percent hafnium, such as in excess of 1.0 atomic percent hafnium. The coating may also contain about 2 to about 15 atomic percent chromium.
摘要翻译：主要是β相NiAl覆盖涂层，用作环境涂层或TBC粘合涂层，用于恶劣热环境中使用的物品，例如燃气涡轮发动机的部件。该涂层含有高达约4原子％的铪，例如超过1.0原子％的铪。该涂层还可含有约2至约15原子％的铬。

3. 发明授权

US06682827B2 Nickel aluminide coating and coating systems formed therewith 失效
标题翻译：由此形成的铝化镍涂层和涂层系统
公开(公告)号：US06682827B2
公开(公告)日：2004-01-27
申请号：US10029320
申请日：2001-12-20
申请人： Ramgopal Darolia , Joseph David Rigney , Jeffrey Allan Pfaendtner
发明人： Ramgopal Darolia , Joseph David Rigney , Jeffrey Allan Pfaendtner
IPC分类号： B32B1504
CPC分类号： C23C28/321 , B32B15/01 , B32B15/013 , C22C19/03 , C23C14/16 , C23C28/345 , C23C28/3455 , C23C30/00 , Y10T428/1259 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/1275 , Y10T428/12861 , Y10T428/12875 , Y10T428/12944
摘要： A protective overlay coating for articles used in hostile thermal environments, and particularly for use as a bond coat for a thermal barrier coating deposited on the coating. The coating is predominantly beta-phase NiAl into which a platinum-group metal is incorporated, yielding a coating system capable of exhibiting improved spallation resistance as compared to prior bond coat materials containing platinum, must notably the platinum aluminide diffusion coatings. A preferred composition for the beta-phase NiAl overlay coating further contains chromium and zirconium or hafnium.
摘要翻译：用于敌对热环境中用于制品的保护性覆盖涂层，特别用作沉积在涂层上的热障涂层的粘合涂层。涂层主要是其中掺入铂族金属的β相NiAl，与现有的包含铂的粘结涂层材料相比，产生能够表现出改善的抗剥落性的涂层体系，必须特别是铂铝化物扩散涂层。用于β相NiAl覆盖涂层的优选组合物还含有铬和锆或铪。

4. 发明授权

US06663983B1 Thermal barrier coating with improved strength and fracture toughness 有权
$Thermal barrier coating with improved strength and fracture toughness$
标题翻译：热障涂层具有改善的强度和断裂韧性
公开(公告)号：US06663983B1
公开(公告)日：2003-12-16
申请号：US10064562
申请日：2002-07-26
申请人： Ramgopal Darolia , Joseph David Rigney
发明人： Ramgopal Darolia , Joseph David Rigney
IPC分类号： B32B1504
CPC分类号： C23C28/3215 , C23C14/083 , C23C28/321 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/25
摘要： A thermal barrier coating (TBC) (26) for a component (10) intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC (26) is formed of at least partially stabilized zirconia, preferably yttria-stabilized zirconia (YSZ), and exhibits improved strength and fracture toughness as a result of containing a dispersion of chromia precipitates or particles (32). The TBC (26) preferably consists essentially of YSZ and the chromia particles (32), which are preferably dispersed throughout the microstructure of the TBC (26), including the YSZ grains (30) and grain boundaries. The chromia particles (32) constitute at least 1 to about 10 volume percent of the TBC (26).
摘要翻译：用于在敌对环境中使用的组件（10）的隔热涂层（TBC）（26），例如燃气涡轮发动机的超级合金涡轮机，燃烧器和增压器部件。 TBC（26）由至少部分稳定的氧化锆，优选氧化钇稳定的氧化锆（YSZ）形成，并且由于含有氧化铬析出物或颗粒（32）的分散体而显示出改善的强度和断裂韧性。 TBC（26）优选基本上由YSZ和氧化铬颗粒（32）组成，其优选分散在包括YSZ晶粒（30）和晶界的TBC（26）的整个微结构中。氧化铁颗粒（32）构成TBC（26）的至少1至约10体积％。

5. 发明授权

US06586115B2 Yttria-stabilized zirconia with reduced thermal conductivity 有权
公开(公告)号：US06586115B2
公开(公告)日：2003-07-01
申请号：US09833446
申请日：2001-04-12
申请人： Joseph David Rigney , Ramgopal Darolia
发明人： Joseph David Rigney , Ramgopal Darolia
IPC分类号： B32B1504
CPC分类号： F01D5/288 , C04B35/486 , C04B2235/3206 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/3272 , C04B2235/3275 , C04B2235/3279 , C04B2235/787 , C04B2235/80 , C04B2235/85 , C23C28/00 , C23C30/00 , F05D2300/134 , F05D2300/5024 , Y10T29/49922 , Y10T428/12611 , Y10T428/12618 , Y10T428/249956
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC is formed of zirconia that is partially stabilized with yttria (YSZ), preferably not more than 3 weight percent yttria, and to which one or more additional metal oxides are alloyed to increase crystallographic defects and lattice strains in the TBC grains and/or form precipitates of zirconia and/or compound(s) of zirconia and/or yttria and the additional metal oxide(s), the inclusion of which reduces the thermal conductivity of the YSZ to levels lower than conventional 6-8% YSZ. Improvements are particularly contemplated for TBC having a columnar grain structure, such as those deposited by EBPVD and other PVD techniques.

6. 发明授权

US06544665B2 Thermally-stabilized thermal barrier coating 失效
公开(公告)号：US06544665B2
公开(公告)日：2003-04-08
申请号：US09765228
申请日：2001-01-18
申请人： Joseph David Rigney , Ramgopal Darolia
发明人： Joseph David Rigney , Ramgopal Darolia
IPC分类号： B32B1504
CPC分类号： C23C14/083 , C23C28/321 , C23C28/3215 , C23C28/323 , C23C28/325 , C23C28/345 , C23C28/3455 , C23C30/00 , Y10T428/12549 , Y10T428/1259 , Y10T428/12618 , Y10T428/249953 , Y10T428/26 , Y10T428/268
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC is formed to contain small amounts of alumina precipitates dispersed throughout the grain boundaries and pores of the TBC to getter oxide impurities that would otherwise allow or promote grain sintering and coarsening and pore coarsening, the consequence of which would be densification of the TBC and therefore increased thermal conductivity. If sufficiently fine, the precipitates also serve to pin the grains and pore boundaries of the TBC, the effect of which is to reduce the tendency for the microstructure of the TBC to sinter, coarsen and undergo pore redistribution, which also increase thermal conductivity of the TBC 26.

7. 发明授权

US06492038B1 Thermally-stabilized thermal barrier coating and process therefor 失效
标题翻译：热稳定的热障涂层及其工艺
公开(公告)号：US06492038B1
公开(公告)日：2002-12-10
申请号：US09723273
申请日：2000-11-27
申请人： Joseph David Rigney , Ramgopal Darolia
发明人： Joseph David Rigney , Ramgopal Darolia
IPC分类号： B32B1504
CPC分类号： C23C14/0021 , C23C8/02 , C23C14/06 , C23C28/321 , C23C28/3215 , C23C28/324 , C23C28/325 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2230/90 , F05D2300/2118 , F05D2300/226 , F05D2300/228 , F05D2300/611 , Y10T428/12576 , Y10T428/12611 , Y10T428/249953 , Y10T428/249986
摘要： A thermal barrier coating (TBC) and method for forming the coating on a component intended for use in a hostile environment. The coating and method are particularly directed to inhibiting sintering, grain coarsening/growth and pore redistribution in the coating during high temperature excursions by providing limited amounts of extremely fine carbide-based and/or nitride-based precipitates preferably formed at defects and pores at and between the grain boundaries of the TBC microstructure. The precipitates pin the TBC grain boundaries and pores during high temperature excursions, with the effect that the TBC microstructure is thermally stabilized. A coating containing the carbides and/or nitrides can be formed using a physical vapor deposition technique in an atmosphere that contains carbon and/or nitride gases or compounds thereof, or by evaporating a source material that contains carbon, carbon-containing compounds, carbides and/or nitrides.
摘要翻译：热障涂层（TBC）以及用于在敌对环境中使用的部件上形成涂层的方法。涂层和方法特别涉及通过提供有限量的非常细小的碳化物基和/或氮化物基沉淀物，优选在缺陷和孔处形成，并且在高温偏移期间在缺陷和孔处形成，从而抑制涂层中的烧结，晶粒粗化/生长和孔再分布在TBC微结构的晶界之间。沉淀物在高温偏移期间将TBC晶粒边界和孔隙固定，从而使TBC微结构热稳定。含有碳化物和/或氮化物的涂层可以使用物理气相沉积技术在含有碳和/或氮化物气体或其化合物的气氛中或通过蒸发含有碳，含碳化合物，碳化物的源材料和 /或氮化物。

8. 发明授权

US08512874B2 Coating systems containing beta phase and gamma-prime phase nickel aluminide 有权
标题翻译：包含β相和γ相的镍化合物的涂层体系
公开(公告)号：US08512874B2
公开(公告)日：2013-08-20
申请号：US11757521
申请日：2007-06-04
申请人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
发明人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
IPC分类号： B32B15/04 , C22C19/05 , C23C30/00 , F01D5/28
CPC分类号： F01D5/288 , C23C4/18 , C23C10/02 , C23C10/48 , C23C10/50 , C23C10/52 , C23C28/021 , C23C28/321 , C23C28/3455 , C23C30/00 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/24967 , Y10T428/264 , Y10T428/265 , Y10T428/31678
摘要： A coating and process for depositing the coating on a substrate. The coating is a nickel aluminide overlay coating of predominantly the beta (NiAl) and gamma-prime (Ni3Al) intermetallic phases, and is suitable for use as an environmental coating and as a bond coat for a thermal barrier coating (TBC). The coating can be formed by depositing nickel and aluminum in appropriate amounts to yield the desired beta+gamma prime phase content. Alternatively, nickel and aluminum can be deposited so that the aluminum content of the coating exceeds the appropriate amount to yield the desired beta+gamma prime phase content, after which the coating is heat treated to diffuse the excess aluminum from the coating into the substrate to yield the desired beta+gamma prime phase content.
摘要翻译：用于将涂层沉积在基材上的涂层和方法。涂层是主要是β（NiAl）和γ-prime（Ni3Al）金属间相的镀镍铝覆盖涂层，适用于环境涂层和用作热障涂层（TBC）的粘合涂层。可以通过以适当的量沉积镍和铝来形成所述涂层，以产生所需的β+γ初相相含量。或者，可以沉积镍和铝，使得涂层的铝含量超过适当的量以产生所需的β+γ初相相含量，之后热处理涂层以将过量的铝从涂层扩散到基底中产生期望的β+γ'相相含量。

9. 发明授权

US07326441B2 Coating systems containing beta phase and gamma-prime phase nickel aluminide 有权
标题翻译：包含β相和γ相的镍化合物的涂层体系
公开(公告)号：US07326441B2
公开(公告)日：2008-02-05
申请号：US10904844
申请日：2004-12-01
申请人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
发明人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
IPC分类号： B05D3/02
CPC分类号： F01D5/288 , C23C4/18 , C23C10/02 , C23C10/48 , C23C10/50 , C23C10/52 , C23C28/021 , C23C28/321 , C23C28/3455 , C23C30/00 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/24967 , Y10T428/264 , Y10T428/265 , Y10T428/31678
摘要： A coating and process for depositing the coating on a substrate. The coating is a nickel aluminide overlay coating of predominantly the beta (NiAl) and gamma-prime (Ni3Al) intermetallic phases, and is suitable for use as an environmental coating and as a bond coat for a thermal barrier coating (TBC). The coating can be formed by depositing nickel and aluminum in appropriate amounts to yield the desired beta+gamma prime phase content. Alternatively, nickel and aluminum can be deposited so that the aluminum content of the coating exceeds the appropriate amount to yield the desired beta+gamma prime phase content, after which the coating is heat treated to diffuse the excess aluminum from the coating into the substrate to yield the desired beta+gamma prime phase content.
摘要翻译：用于将涂层沉积在基材上的涂层和方法。涂层是主要是β（NiAl）和γ-prime（Ni 3 Al 3 Al）金属间相的镍铝化物覆盖涂层，并且适合用作环境涂层和作为粘合涂层隔热涂层（TBC）。可以通过以适当的量沉积镍和铝来形成所述涂层，以产生所需的β+γ初相相含量。或者，可以沉积镍和铝，使得涂层的铝含量超过适当的量以产生所需的β+γ初相相含量，之后热处理涂层以将过量的铝从涂层扩散到基底中产生期望的β+γ'相相含量。

10. 发明授权

US07244467B2 Process for a beta-phase nickel aluminide overlay coating 有权
标题翻译：一种β相镍铝覆盖涂层的工艺
公开(公告)号：US07244467B2
公开(公告)日：2007-07-17
申请号：US10604368
申请日：2003-07-15
申请人： Theodore Robert Grossman , Ramgopal Darolia , Joseph David Rigney
发明人： Theodore Robert Grossman , Ramgopal Darolia , Joseph David Rigney
IPC分类号： C23C16/00
CPC分类号： C23C14/5886 , C23C4/18 , C23C14/16 , C23C26/00 , C23C28/3215 , C23C28/345 , C23C28/3455
摘要： A process for forming a beta-phase nickel aluminide (NiAl) overlay coating that is suitable for use as a bond coat for a thermal barrier coating (TBC). The overlay coating is deposited by a method that produces a generally columnar grain structure in which grains extend through the coating such that at least some grain boundaries are open at the coating surface. The coating is then peened with a particulate media, followed by heating the overlay coating to a temperature sufficient to cause the overlay coating to recrystallize and form new grain boundaries that are not open to the outer surface of the coating and significantly less susceptible to accelerated oxidation than the original grain boundaries. The particulate media is formed of a composition containing nickel and aluminum, such that an oxide scale that forms on the surface of the coating after the peening operation is substantially free of deleterious oxide compounds, notably iron-containing spinels.
摘要翻译：用于形成适合用作热障涂层（TBC）的粘合涂层的β-相镍铝化物（NiAl）覆盖涂层的方法。覆盖涂层通过产生大致柱状晶粒结构的方法沉积，其中晶粒延伸穿过涂层，使得至少一些晶界在涂层表面开口。然后用颗粒介质对涂层进行喷丸处理，然后将覆盖涂层加热至足以使覆盖涂层再结晶并形成不对涂层外表面开放的新晶粒边界，并显着降低易受加速氧化影响的温度比原来的晶界。颗粒介质由包含镍和铝的组合物形成，使得在喷丸操作之后在涂层表面上形成的氧化皮基本上不含有害氧化物化合物，特别是含铁尖晶石。

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