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1. 发明授权

US06733637B1 Process for producing ultra-high purity isopropanol 失效
标题翻译：生产超高纯异丙醇的方法
公开(公告)号：US06733637B1
公开(公告)日：2004-05-11
申请号：US09587103
申请日：2000-06-02
申请人： Paul E. Burton , Dennis J. Davoren , Timothy P. Dean , John P. Motlow , Charles M. Yarbrough
发明人： Paul E. Burton , Dennis J. Davoren , Timothy P. Dean , John P. Motlow , Charles M. Yarbrough
IPC分类号： B01D300
CPC分类号： C07C29/80 , Y10S203/20 , C07C31/10
摘要： A process for producing high purity isopropyl alcohol. In one embodiment, the process includes the steps of: (a) feeding a feed stream comprising at least about 99.9 wt. % isopropyl alcohol into a separation column; (b) separating the isopropyl alcohol into an overhead stream taken overhead from the separation column and a bottoms stream taken as bottoms from the separation column; and (c) removing the high purity isopropyl alcohol at a point: (i) below where the feed stream enters the separation column but above the bottoms stream, or (ii) above where the feed stream enters the separation column but below the overhead stream. The high purity isopropyl alcohol has a metals content of less than about 1 ppb and a water content of less than about 100 ppm. Optionally, the process includes the step of passing the high purity isopropyl alcohol through an ion exchange resin after removing the high purity isopropyl alcohol from the separation column, thereby forming an ultra-high purity isopropyl alcohol that contains less than 100 ppt of any metal impurity.
摘要翻译：一种生产高纯度异丙醇的方法。在一个实施方案中，该方法包括以下步骤：（a）进料包含至少约99.9wt。％异丙醇进入分离柱; （b）将异丙醇分离成塔顶馏出物，塔顶馏出塔和从分离塔中取出的底部物流; 和（c）在以下点：（i）除去高纯度异丙醇，其中进料流进入分离塔但高于塔底流，或（ii）上述进料流进入分离塔但低于塔顶流。高纯度异丙醇的金属含量小于约1ppb，水含量低于约100ppm。任选地，该方法包括在从分离塔中除去高纯度异丙醇之后使高纯度异丙醇通过离子交换树脂的步骤，从而形成含有小于100ppt的任何金属杂质的超高纯度异丙醇。

2. 发明授权

US06677481B2 Cracking of neo-C9 and neo-C13 carboxylic acids to either pivalic acid or methyl pivalate 失效
公开(公告)号：US06677481B2
公开(公告)日：2004-01-13
申请号：US09901238
申请日：2001-07-09
申请人： Edmund J. Mozeleski , Richard H. Schlosberg , Dennis J. Davoren , Carl Robert Beck , Linda J. Broadbelt , Ned C. Haubein
发明人： Edmund J. Mozeleski , Richard H. Schlosberg , Dennis J. Davoren , Carl Robert Beck , Linda J. Broadbelt , Ned C. Haubein
IPC分类号： C07C5114
CPC分类号： C07C51/44 , C07C51/10 , C07C51/14 , C07C67/36 , C07C53/128 , C07C69/24
摘要： A method for production of pivalic acid comprising the steps of: (a) reacting isobutylene, carbon monoxide, and a first catalyst to produce a reaction mixture; (b) contacting the reaction mixture with water, thereby producing a crude acid product having pivalic acid and oligomeric neo-carboxylic acid; (c) then separating the pivalic acid and the oligomeric neo-carboxylic acid from the crude acid product; (d) then reacting the oligomeric neo-carboxylic acid with a source of carbon monoxide at a temperature of less than 200° C. in the presence of a second catalyst to produce a C5 carbocation product, wherein the first and second catalyst are either the same or different; and (e) reacting the C5 carbocation product with water; thereby producing pivalic acid having an overall yield of at least 80 wt. %.

3. 发明授权

US06919474B2 Cracking of neo-C9 and neo-C13 carboxylic acids to either pivalic acid or methyl pivalate 失效
标题翻译：将新C9和新-C13羧酸裂解成新戊酸或新戊酸甲酯
公开(公告)号：US06919474B2
公开(公告)日：2005-07-19
申请号：US10365132
申请日：2003-03-31
申请人： Edmund J. Mozeleski , Richard H. Schlosberg , Dennis J. Davoren , Carl Robert Beck , Linda J. Broadbelt , Ned C. Haubein
发明人： Edmund J. Mozeleski , Richard H. Schlosberg , Dennis J. Davoren , Carl Robert Beck , Linda J. Broadbelt , Ned C. Haubein
IPC分类号： C07C51/10 , C07C51/14 , C07C51/44 , C07C67/36 , C07C69/00 , C07C67/38
CPC分类号： C07C51/44 , C07C51/10 , C07C51/14 , C07C67/36 , C07C53/128 , C07C69/24
摘要： A method for production of pivalic acid comprising the steps of: (a) reacting isobutylene, carbon monoxide, and a first catalyst to produce a reaction mixture; (b) contacting the reaction mixture with water, thereby producing a crude acid product having pivalic acid and oligomeric neo-carboxylic acid; (c) separating the pivalic acid and the oligomeric neo-carboxylic acid from the crude acid product; (d) reacting the oligomeric neo-carboxylic acid with a source of carbon monoxide at a temperature of less than 200° C. in the presence of a second catalyst to produce a C5 carbocation product, wherein the first and second catalyst are either the same or different; and (e) reacting the C5 carbocation product with water; thereby producing pivalic acid having an overall yield of at least 80 wt. %.
摘要翻译：一种生产新戊酸的方法，包括以下步骤：（a）使异丁烯，一氧化碳和第一催化剂反应以产生反应混合物; （b）使反应混合物与水接触，从而产生具有新戊酸和低聚新羧酸的粗酸产物; （c）从粗酸产物中分离新戊酸和低聚新羧酸; （d）在低于200℃的温度下，在第二种催化剂的存在下使低聚新羧酸与一氧化碳源反应，生成C 5 -C 5碳阳离子产物，其中第一和第二催化剂可以相同或不同; 和（e）使C 5 -C 5碳阳离子产物与水反应; 从而产生总产率至少为80重量％的新戊酸。％。

4. 发明授权

US06717010B2 Cracking of neo-C9 and neo-C13 carboxylic acids to either pivalic acid or methyl pivalate 失效
标题翻译：将新C9和新-C13羧酸裂解成新戊酸或新戊酸甲酯
公开(公告)号：US06717010B2
公开(公告)日：2004-04-06
申请号：US10434915
申请日：2003-05-09
申请人： Edmund J. Mozeleski , Richard H. Schlosberg , Dennis J. Davoren , Carl Robert Beck , Linda J. Broadbelt , Ned C. Haubein
发明人： Edmund J. Mozeleski , Richard H. Schlosberg , Dennis J. Davoren , Carl Robert Beck , Linda J. Broadbelt , Ned C. Haubein
IPC分类号： C07C5114
CPC分类号： C07C51/44 , C07C51/10 , C07C51/14 , C07C67/36 , C07C53/128 , C07C69/24
摘要： A method for production of pivalic acid comprising the steps of: (a) reacting isobutylene, carbon monoxide, and a first catalyst to produce a reaction mixture; (b) contacting the reaction mixture with water, thereby producing a crude acid product having pivalic acid and oligomeric neo-carboxylic acid; (c) then separating the pivalic acid and the oligomeric neo-carboxylic acid from the crude acid product; (d) then reacting the oligomeric neo-carboxylic acid with a source of carbon monoxide at a temperature of less than 200° C. in the presence of a second catalyst to produce a C5 carbocation product, wherein the first and second catalyst are either the same or different; and (e) reacting the C5 carbocation product with water; thereby producing pivalic acid having an overall yield of at least 80 wt. %.
摘要翻译：一种生产新戊酸的方法，包括以下步骤：（a）使异丁烯，一氧化碳和第一催化剂反应以产生反应混合物; （b）使反应混合物与水接触，从而产生具有新戊酸和低聚新羧酸的粗酸产物; （c）然后从所述粗酸产物中分离出所述新戊酸和所述低聚新羧酸; （d）然后使所述低聚新羧酸与一氧化碳源在小于200℃的温度下在第二催化剂存在下反应，以产生C5碳阳离子产物，其中所述第一和第二催化剂是相同或不同; 和（e）使C5碳阳离子产物与水反应; 从而产生总产率至少为80重量％的新戊酸。％。

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