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1. 发明授权

US5739369A Water-soluble surface treating agents 失效
标题翻译：水溶性表面处理剂
公开(公告)号：US5739369A
公开(公告)日：1998-04-14
申请号：US634829
申请日：1996-04-19
申请人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
发明人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
IPC分类号： C09D183/08 , C03C17/30 , C09D183/04 , C09K3/18 , C07F7/10
CPC分类号： C09K3/18 , C03C17/30 , C09K3/185
摘要： A surface treating agent comprising a reaction product of (A) a fluoroalkyl group-containing alkoxysilane with (B) an amino group-containing alkoxysilane and optionally further with (C) an alkyl group-containing alkoxysilane is water soluble. The agent is diluted with water to form a solution for treating glass and other substrates to impart durable water repellency and other improved properties to the substrates.
摘要翻译：包含（A）含氟烷基的烷氧基硅烷与（B）含氨基的烷氧基硅烷和任选地还含有（C）含烷基的烷氧基硅烷的反应产物的表面处理剂是水溶性的。用水稀释试剂以形成用于处理玻璃和其它基材的溶液，以赋予基材持久的拒水性和其它改进的性能。

2. 发明授权

US06521290B1 Silica particles surface-treated with silane, process for producing the same and uses thereof 有权
标题翻译：用硅烷表面处理的二氧化硅颗粒，其制造方法及其用途
公开(公告)号：US06521290B1
公开(公告)日：2003-02-18
申请号：US09312054
申请日：1999-05-17
申请人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
发明人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
IPC分类号： B05D700
CPC分类号： C08K9/06
摘要： Fine silica particles surface-treated with a silane and having primary particles having a particle diameter of from 0.01 to 5 &mgr;m, which fine silica particles fulfill the following conditions (i) and (ii), a process for their production and an organic resin composition containing such particles as a component are provided. (i) When an organic compound which is liquid at room temperature and has a dielectric constant of from 1 to 40 F/m and fine silica particles are mixed in a weight ratio of 5:1 and shaked, the fine silica particles disperse uniformly in the organic compound, and (ii) the quantity of primary particles remaining as primary particles when methanol is evaporated under heating by means of an evaporator from a dispersion prepared by dispersing the fine silica particles in methanol and thereafter the particles are held at a temperature of 100° C. for 2 hours, is in a percentage of at least 20% based on the quantity of primary particles originally present. The present fine silica particles are highly dispersible and low aggregative, and the organic resin composition containing them is useful for obtaining films having a good transparency and superior blocking resistance, slip properties and scratch resistance.
摘要翻译：二氧化硅微粒用硅烷表面处理，具有粒径为0.01〜5μm的一次粒子，二氧化硅微粒满足下述条件（i）和（ii），其制造方法和有机树脂组合物提供含有作为组分的颗粒。（i）当室温下介电常数为1〜40F / m的有机化合物和二氧化硅微粒以5:1的重量比混合并摇动时，二氧化硅微粒分散在有机化合物，和（ii）当通过蒸发器从通过将二氧化硅微粒分散在甲醇中制备的分散体在蒸发器中加热蒸发甲醇时剩余的一次颗粒的量，然后将颗粒保持在 100℃，2小时，以原始存在的一次粒子的量为至少20％的百分比。本发明的二氧化硅微粒高分散性和低聚集性，含有它们的有机树脂组合物可用于获得具有良好透明性和优异的抗粘连性，滑爽性和耐划伤性的膜。

3. 发明授权

US6077966A Preparation of water-soluble organic silicon compounds 失效
标题翻译：水溶性有机硅化合物的制备
公开(公告)号：US6077966A
公开(公告)日：2000-06-20
申请号：US709036
申请日：1996-09-06
申请人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
发明人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
IPC分类号： C09K3/18 , B27K3/50 , B27K3/52 , C04B41/49 , C07F7/08 , C07F7/18 , C08G77/26 , C07F7/10
CPC分类号： C08G77/26 , C04B41/4922 , C07F7/0859 , C07F7/1836 , C08L97/02 , B27K2240/70 , B27K3/15 , C08L83/04
摘要： Water-soluble organic silicon compounds are prepared by effecting co-hydrolysis of (A) 1-30 parts of an alkyltrialkoxysilane of R.sup.1 Si(OR.sup.2).sub.3 or a partial hydrolyzate thereof, (B) 70-90 parts of an alkoxy-containing siloxane of R.sup.3.sub.a (OR.sup.2).sub.b SiO.sub.(4-a-b)/2, and (C) 1-20 parts of an amino-containing alkoxysilane of R.sup.4 R.sup.5 NR.sup.6 --SiR.sup.7.sub.n (OR.sup.2).sub.3-n or a partial hydrolyzate thereof in the presence of an organic or inorganic acid. R.sup.1 is a C.sub.7 -C.sub.18 alkyl group, R.sup.2 is a C.sub.1 -C.sub.4 alkyl group, R.sup.3 is a C.sub.1 -C.sub.6 alkyl group, R.sup.4 and R.sup.5 are a hydrogen atom, C.sub.1 -C.sub.15 alkyl or aminoalkyl group, R.sup.6 is a divalent C.sub.1 -C.sub.18 hydrocarbon group, and R.sup.7 is a C.sub.1 -C.sub.4 alkyl group. Letters a and b are 0.75.ltoreq.a.ltoreq.1.5, 0.2.ltoreq.b.ltoreq.2, and 0.95
摘要翻译：水溶性有机硅化合物是通过（A）1-30份的R 1 Si（OR 2）3的烷基三烷氧基硅烷或其部分水解产物，（B）70-90份含烷氧基的硅氧烷 R3a（OR2）bSiO（4-ab）/ 2和（C）在有机或无机存在下，将1-20份R4R5NR6-SiR7n（OR2）3-n的氨基烷氧基硅烷或其部分水解产物酸。 R1是C7-C18烷基，R2是C1-C4烷基，R3是C1-C6烷基，R4和R5是氢原子，C1-C15烷基或氨基烷基，R6是二价C1-C18 烃基，R 7为C 1〜C 4烷基。字母a和b为0.75

4. 发明授权

US06855759B2 Silica particles surface-treated with silane, process for producing the same and uses thereof 有权
标题翻译：用硅烷表面处理的二氧化硅颗粒，其制造方法及其用途
公开(公告)号：US06855759B2
公开(公告)日：2005-02-15
申请号：US10284149
申请日：2002-10-31
申请人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
发明人： Muneo Kudo , Shoji Ichinohe , Atsushi Asami , Mitsuo Asai , Kazuyuki Matsumura , Masaki Tanaka
IPC分类号： C08K9/06 , C08K5/24
CPC分类号： C08K9/06
摘要： Fine silica particles surface-treated with a silane and having primary particles having a particle diameter of from 0.01 to 5 μm, which fine silica particles fulfill the following conditions (i) and (ii), a process for their production and an organic resin composition containing such particles as a component are provided. (i) When an organic compound which is liquid at room temperature and has a dielectric constant of from 1 to 40 F/m and fine silica particles are mixed in a weight ratio of 5:1 and shaked, the fine silica particles disperse uniformly in the organic compound, and (ii) the quantity of primary particles remaining as primary particles when methanol is evaporated under heating by means of an evaporator from a dispersion prepared by dispersing the fine silica particles in methanol and thereafter the particles are held at a temperature of 100° C. for 2 hours, is in a percentage of at least 20% based on the quantity of primary particles originally present. The present fine silica particles are highly dispersible and low aggregative, and the organic resin composition containing them is useful for obtaining films having a good transparency and superior blocking resistance, slip properties and scratch resistance.
摘要翻译：二氧化硅微粒用硅烷表面处理，具有粒径为0.01〜5μm的一次粒子，二氧化硅微粒满足下述条件（i）和（ii），其制造方法和有机树脂组合物提供含有作为组分的颗粒。（i）当室温下介电常数为1〜40F / m的有机化合物和二氧化硅微粒以5:1的重量比混合并摇动时，二氧化硅微粒分散在有机化合物，和（ii）当通过蒸发器从通过将二氧化硅微粒分散在甲醇中制备的分散体在蒸发器中加热蒸发甲醇时剩余的一次颗粒的量，然后将颗粒保持在 100℃，2小时，以原始存在的一次粒子的量为至少20％的百分比。本发明的二氧化硅微粒高分散性和低聚集性，含有它们的有机树脂组合物可用于获得具有良好透明性和优异的抗粘连性，滑爽性和耐划伤性的膜。

5. 发明授权

US5883185A Water soluble fiber-treating agent and method of making 失效
标题翻译：水溶性纤维处理剂及其制备方法
公开(公告)号：US5883185A
公开(公告)日：1999-03-16
申请号：US818937
申请日：1997-03-17
申请人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
发明人： Kazuyuki Matsumura , Mitsuo Asai , Shoji Ichinohe
IPC分类号： C08L83/08 , C08G77/06 , C08G77/22 , C08G77/26 , C08G77/46 , C08L83/04 , D06M15/643 , D06M15/65 , D06M15/657 , C08L83/06
CPC分类号： D06M15/65 , C08G77/22 , C08G77/26 , C08G77/46 , D06M15/643 , D06M15/6436 , D06M15/657 , Y10S8/01
摘要： A fiber-treating agent is obtained by dissolving in water a reaction product resulting from co-hydrolysis and condensation of (A) a fluorinated alkyl group-containing alkoxysilane, (B) an alkyl group-containing alkoxysilane, (C) an amino group-containing alkoxysilane, and (D) an epoxy group-containing alkoxysilane. The fiber-treating agent is water soluble and thus safe while it imparts satisfactory water repellency, oil repellency, stain-proof property and even durable water repellency.
摘要翻译：通过将（A）含氟烷基的烷氧基硅烷，（B）含烷基的烷氧基硅烷，（C）氨基 - 烷氧基硅烷，（D）含环氧基的烷氧基硅烷。纤维处理剂是水溶性的，因此安全，同时赋予了令人满意的拒水性，拒油性，防污性和甚至耐久的拒水性。

6. 发明授权

US06316155B1 External additive for electrostatically charged latent image developing toner 有权
标题翻译：用于静电充电潜像显影调色剂的外用添加剂
公开(公告)号：US06316155B1
公开(公告)日：2001-11-13
申请号：US09524907
申请日：2000-03-13
申请人： Muneo Kudo , Masaki Tanaka , Yoshiteru Sakatsume , Shoji Ichinohe , Mitsuo Asai
发明人： Muneo Kudo , Masaki Tanaka , Yoshiteru Sakatsume , Shoji Ichinohe , Mitsuo Asai
IPC分类号： G03G908
CPC分类号： C09C1/3081 , C01P2004/32 , C01P2004/62 , G03G9/09725
摘要： An external additive for electrostatically charged latent image developing toner is provied. The additive includes spherical hydrophobic fine silica particles having primary particles having a particle diameter of from 0.01 to 5 &mgr;m, which fine silica particles fulfill the following conditions (i) and (ii): (i) when an organic compound which is liquid at room temperature and has a dielectric constant of from 1 to 40 F/m and fine silica particles are mixed in a weight ratio of 5:1 and shaken, the fine silica particles disperse uniformly in the organic compound; and (ii) the quantity of primary particles remaining as primary particles when methanol is evaporated under heating by means of an evaporator from a dispersion prepared by dispersing the fine silica particles in methanol and thereafter the particles are held at a temperature of 100° C. for 2 hours, represents at least 20% of the quantity of primary particles originally present. The external additive does not react or has no interaction with an organic photoreceptor and therefore change in quality does not occur or the photoreceptor is not scraped. Furthermore, it has a good flowability and therefore adhesion of a toner to the photoreceptor does not occur.
摘要翻译：证明了静电充电潜像显影调色剂的外用添加剂。添加剂包括具有粒径为0.01〜5μm的一次粒子的球状疏水性细二氧化硅粒子，二氧化硅微粒满足以下条件（i）和（ii）：（i）当室内为液体的有机化合物时介电常数为1〜40F / m，二氧化硅微粒以5:1的重量比混合并摇动，二氧化硅微粒分散在有机化合物中; 和（ii）当通过蒸发器在加热下从通过将二氧化硅微粒分散在甲醇中制备的分散体蒸发而蒸发甲醇时的初级颗粒的量，然后将颗粒保持在100℃的温度。 2小时，表示原始存在的初级粒子的量的至少20％。外部添加剂不与有机感光体反应或没有相互作用，因此不会发生质量变化或感光体不被刮擦。此外，它具有良好的流动性，因此不会发生调色剂对感光体的粘附。

7. 发明授权

US5705590A Water absorption preventing agent having water solubility and a method for preventing water absorption 失效
标题翻译：具有水溶性的吸水防止剂和防止吸水的方法
公开(公告)号：US5705590A
公开(公告)日：1998-01-06
申请号：US621682
申请日：1996-03-26
申请人： Tomohisa Suzuki , Kenichi Isobe , Mitsuo Asai , Shoji Ichinohe , Akira Yamamoto
发明人： Tomohisa Suzuki , Kenichi Isobe , Mitsuo Asai , Shoji Ichinohe , Akira Yamamoto
IPC分类号： C03C25/40 , C04B41/49 , C04B41/64 , C04B41/84 , C07F7/18 , C08G65/336 , C09K3/18 , D06M13/513 , D06M15/647 , C08G77/04
CPC分类号： C04B41/009 , C03C25/40 , C04B41/495 , C04B41/64 , C04B41/84 , C07F7/1836 , C08G65/336 , C09K3/18 , D06M13/513 , D06M15/647
摘要： A water soluble water absorption preventing agent mainly comprising an organic silicon compound and/or its partial hydrolytic condensate, represented by the following general formula: ##STR1## wherein R.sup.1 denotes an alkyl group with 1-20 carbon atoms and with a linear chain or branched chain for which a halogen can substitute for part or all of the hydrogen atoms, R.sup.2 denotes a hydrogen atom or an alkyl group with 1-10 carbon atoms and with a linear chain or branched chain, R.sup.3 denotes a hydrogen atom or an alkyl group with 1-8 carbon atoms and with a linear chain or branched chain, m denotes an integer 1-2 and n denotes an integer 1-3 where m+n=3 or 4, p denotes an integer 1-50, and q denotes an integer 0-25.
摘要翻译：一种主要包含有机硅化合物和/或其部分水解缩合物的水溶性吸水防止剂，由以下通式表示：其中R1表示具有1-20个碳原子的直链或支链的烷基卤素可以代替部分或全部氢原子的链，R2表示氢原子或具有1-10个碳原子的直链或支链的烷基，R3表示氢原子或具有 1-8个碳原子并且具有直链或支链，m表示整数1-2，n表示整数1-3，其中m + n = 3或4，p表示1-50的整数，q表示整数0-25。

8. 发明申请

US20070049509A1 Highly volatile polyether-modified silicone surfactant 有权
标题翻译：高挥发性聚醚改性硅氧烷表面活性剂
公开(公告)号：US20070049509A1
公开(公告)日：2007-03-01
申请号：US11511351
申请日：2006-08-29
申请人： Akira Yamamoto , Shoji Ichinohe
发明人： Akira Yamamoto , Shoji Ichinohe
IPC分类号： C11D1/66
CPC分类号： C11D1/82 , C08G77/46 , C08L83/12
摘要： A highly volatile electrical/electronic parts surfactant containing a polyether-modified silicone having one polyether chain in the molecule, wherein the surface tension at 25° C. of a 0.01 mass % aqueous solution thereof is 25 mN/m or less, the aforesaid silicone is expressed by the following average structural formula (1), and when heated from room temperature to 200° C. at a rate of 5° C./minute to 200° C. and maintained at a temperature of 200° C. for 100 minutes, the polyether-modified silicone completely volatilizes without leaving any remainder, and a method of manufacturing this highly volatile polyether-modified silicone are disclosed. AMe2SiO(MeASiO)nSiMe2A (1) In formula (1), any one of A is a substituent group expressed by the following general formula (2), the remaining A are methyl groups and n is an integer from 0-2. —CaH2aO(C2H4O)bR (2) In formula (2), a is 3-4, b is an integer from 1-7 and R is a methyl group or an ethyl group.
摘要翻译：含有分子中具有一个聚醚链的聚醚改性硅酮的高挥发性电气/电子部件表面活性剂，其中0.01质量％水溶液在25℃下的表面张力为25mN / m以下，上述硅氧烷由以下平均结构式（1）表示，当以5℃/分钟至200℃的温度从室温加热至200℃并保持在200℃的温度下保持100 分钟，聚醚改性硅氧烷完全挥发而不留下任何剩余部分，并且公开了制造这种高挥发性聚醚改性硅氧烷的方法。 <？in-line-formula description =“In-line Formulas”end =“lead”？>第二个二氧化硅（MeASiO）N 2 SiMe 2 在式（1）中，A中的任何一个是由以下通式（2）表示的取代基，其中，A是（1）<αin-line-formula description =“In-line Formulas”end =“tail” ），其余的A为甲基，n为0-2的整数。 <？in-line-formula description =“In-line Formulas”end =“lead”？ - - - - - - - - - - - - - - - - - - - - （2） R（2）<βin-line-formula description =“In-line Formulas”end =“tail”？>在式（ 2）中，a为3-4，b为1-7的整数，R为甲基或乙基。

9. 发明申请

US20070015884A1 Epoxy resin additives and epoxy resin compositions 审中-公开
标题翻译：环氧树脂添加剂和环氧树脂组合物
公开(公告)号：US20070015884A1
公开(公告)日：2007-01-18
申请号：US11483587
申请日：2006-07-11
申请人： Akira Yamamoto , Shoji Ichinohe , Eiichi Tabei
发明人： Akira Yamamoto , Shoji Ichinohe , Eiichi Tabei
IPC分类号： C08L63/00 , C08L83/00 , C08G77/04 , B32B27/38
CPC分类号： C08L63/00 , C07F7/0838 , C08G59/306 , C08K5/54 , C08L83/00
摘要： Epoxy-modified low molecular weight silicones are added to epoxy resins for reducing surface tension and improving fluidity.
摘要翻译：将环氧改性的低分子量硅氧烷加入到环氧树脂中以降低表面张力并提高流动性。

10. 发明授权

US06495651B1 Process for preparing urethane compound for medical instruments 有权
标题翻译：制备医疗器械用聚氨酯化合物的方法
公开(公告)号：US06495651B1
公开(公告)日：2002-12-17
申请号：US09608004
申请日：2000-06-30
申请人： Tsuyoshi Watanabe , Eri Ito , Sadayasu Tanikawa , Shoji Ichinohe , Toshio Yamazaki
发明人： Tsuyoshi Watanabe , Eri Ito , Sadayasu Tanikawa , Shoji Ichinohe , Toshio Yamazaki
IPC分类号： C08G1822
CPC分类号： C08G18/8175 , C08G18/2063 , C08G18/222 , C08G18/672 , C08G18/61
摘要： A process for preparing an urethane compound for medical instruments, characterized by reacting a hydroxyl compound (A) with an isocyanate compound (B) in the absence of a catalyst or in the presence of a reaction catalyst other than an organic tin compound to give an urethane compound (I). According to the process, the urethane compound showing high safety can be easily prepared, in particular, while molecular weight of the compound is controlled.
摘要翻译：一种用于医疗器械的氨基甲酸酯化合物的制备方法，其特征在于在不存在催化剂的情况下或在除有机锡化合物以外的反应催化剂存在下使羟基化合物（A）与异氰酸酯化合物（B）反应，得到氨基甲酸酯化合物（I）。根据该方法，可以容易地制备显示高安全性的氨基甲酸酯化合物，特别是在控制化合物的分子量时。

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