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1. 发明授权

US4495327A Aqueous cationic surface-coating system and its use 失效
标题翻译：水性阳离子表面涂层体系及其用途
公开(公告)号：US4495327A
公开(公告)日：1985-01-22
申请号：US515026
申请日：1983-07-18
申请人： Hans-Uwe Schenck , Rainer Blum , Erich Gulbins , Fritz-Erdmann Kempter , Eberhard Schupp
发明人： Hans-Uwe Schenck , Rainer Blum , Erich Gulbins , Fritz-Erdmann Kempter , Eberhard Schupp
IPC分类号： C09D4/00 , C09D5/44 , C09D3/80 , C09D5/40
CPC分类号： C09D5/4492 , Y10S524/901
摘要： An aqueous cationic surface-coating system contains an olefinically unsaturated surface-coating binder having basic nitrogen groups, some or all of which are converted into salts with acid, a Co, Mn, Pb, Ce, Zr, Ca, Zn, Fe, Al, Cu, Ni or Cd complex, if appropriate in combination with an inhibitor and/or an initiator which supplies free radicals.This surface-coating system can be used for cathodic electrocoating or for conventional methods of surface-coating.
摘要翻译：含水阳离子表面涂层体系含有具有碱性氮基的烯属不饱和表面涂层粘合剂，其中一些或全部与酸，Co，Mn，Pb，Ce，Zr，Ca，Zn，Fe，Al ，Cu，Ni或Cd络合物，如果合适的话，与抑制剂和/或提供自由基的引发剂组合。该表面涂层系统可用于阴极电泳或用于常规的表面涂覆方法。

2. 发明授权

US4291147A Polyadducts of ammonia and epoxide compounds, processes for their modification, and their use 失效
标题翻译：氨和环氧化合物的加合物，其改性方法及其用途
公开(公告)号：US4291147A
公开(公告)日：1981-09-22
申请号：US137748
申请日：1980-04-07
申请人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
IPC分类号： C08G12/00 , C08G12/02 , C08G12/46 , C08G59/00 , C08G59/14 , C08G59/40 , C08G65/26 , C08K5/29 , C09D5/44 , C09D163/00
CPC分类号： C08G12/46 , C08G12/00 , C08G12/02 , C08G59/1405 , C08G59/4014 , C08G65/2624 , C09D5/4438 , Y10S524/901 , Y10T428/2933
摘要： Polyadducts, free from epoxide groups, are obtained from ammonia and epoxide compounds by reacting 1 mole of ammonia with from 1.2 to 2.0 equivalents of epoxide, so that if diepoxide compounds are used products of the general formula (I) ##STR1## are obtained, while if triepoxides and/or tetraepoxide compounds are used, by themselves, or together with diepoxide compounds, products of the general formula II ##STR2## are produced; in these formulae, the E.sup.1 's are identical or different hydroxyl-containing divalent radicals and the E.sup.2 's are identical or different hydroxyl-containing trivalent or tetravalent radicals, resulting from the opening of the oxirane rings of epoxide compounds containing two, three or four epoxide groups in the molecule, n.sup.1, n.sup.3 and n.sup.5 are from 0 to 3, n.sup.2 and n.sup.4 are from 1 to 3 and X is 0 or 1, and one or more of the divalent radicals E.sup.1 in the general formula (II) may or may not be replaced by polyvalent radicals E.sup.2.The novel polyadducts can be modified by reaction with aldehydes, ketones, monoepoxide compounds, carboxylic acids, carboxylic acid esters or isocyanates, or by protonation with an acid, and may be used, for example, for the cathodic electrocoating of metallic articles.
摘要翻译：通过使1摩尔氨与1.2-2.0当量的环氧化物反应，从氨和环氧化合物得到不含环氧基的多元加成物，因此如果使用二环氧化合物，则得到通式（I）的产物而如果三环氧化物和/或四环氧化合物本身或与二环氧化合物一起使用，则制备通式II的产物（II）; 在这些式中，E1是相同或不同的含羟基的二价基团，并且E2是相同或不同的含羟基的三价或四价基团，其由环氧乙烷环的环氧化物环开放，所述环氧化物包含两个，三个或四个环氧基团分子n1，n3和n5为0〜3，n2和n4为1〜3，X为0或1，通式（II）中的一个或多个二价基团E1可以是也可以不是由多价基团E2代替。可以通过与醛，酮，单环化合物，羧酸，羧酸酯或异氰酸酯的反应或通过用酸质子化来改变新的多加合物，并且可以用于例如金属制品的阴极电泳涂层。

3. 发明授权

US4363710A Polyadducts of ammonia and epoxide compounds, processes for their modification, and their use 失效
标题翻译：氨和环氧化合物的加合物，其改性方法及其用途
公开(公告)号：US4363710A
公开(公告)日：1982-12-14
申请号：US316797
申请日：1981-10-30
申请人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
IPC分类号： C08G12/00 , C08G12/02 , C08G12/46 , C08G59/00 , C08G59/14 , C08G59/40 , C08G65/26 , C08K5/29 , C09D5/44 , C09D163/00 , C25D13/06
CPC分类号： C08G12/46 , C08G12/00 , C08G12/02 , C08G59/1405 , C08G59/4014 , C08G65/2624 , C09D5/4438 , Y10S524/901 , Y10T428/2933
摘要： Polyadducts, free from epoxide groups, are obtained from ammonia and epoxide compounds by reacting 1 mole of ammonia with from 1.2 to 2.0 equivalents of epoxide, so that if diepoxide compounds are used products of the general formula (I) ##STR1## are obtained, while if triepoxides and/or tetraepoxide compounds are used, by themselves, or together with diepoxide compounds, products of the general formula II ##STR2## are produced; in these formulae, the E.sup.1 's are identical or different hydroxyl-containing divalent radicals and the E.sup.2 's are identical or different hydroxyl-containing trivalent or tetravalent radicals, resulting from the opening of the oxirane rings of epoxide compounds containing two, three or four epoxide groups in the molecule, n.sup.1, n.sup.3 and n.sup.5 are from 0 to 3, n.sup.2 and n.sup.4 are from 1 to 3 and X is 0 or 1, and one or more of the divalent radicals E.sup.1 in the general formlula (II) may or may not be replaced by polyvalent radicals E.sup.2.The novel polyadducts can be modified by reaction with aldehydes, ketones, monoepoxide compounds, carboxylic acids, carboxylic acid esters or isocyanates, or by protonation with an acid, and may be used, for example, for the cathodic electrocoating of metallic articles.
摘要翻译：通过使1摩尔氨与1.2-2.0当量的环氧化物反应，从氨和环氧化合物得到不含环氧基的多元加成物，因此如果使用二环氧化合物，则得到通式（I）的产物而如果三环氧化物和/或四环氧化合物本身或与二环氧化合物一起使用，则制备通式II的产物（II）; 在这些式中，E1是相同或不同的含羟基的二价基团，并且E2是相同或不同的含羟基的三价或四价基团，其由环氧乙烷环的环氧化物环开放，所述环氧化物包含两个，三个或四个环氧基团分子n1，n3和n5为0〜3，n2和n4为1〜3，X为0或1，通式（II）中的一个或多个二价基团E1可以是也可以不是由多价基团E2代替。可以通过与醛，酮，单环化合物，羧酸，羧酸酯或异氰酸酯的反应或通过用酸质子化来改变新的多加合物，并且可以用于例如金属制品的阴极电泳涂层。

4. 发明授权

US4310645A Polyadducts of ammonia and epoxide compounds, processes for their modification, and their use 失效
标题翻译：氨和环氧化合物的加合物，其改性方法及其用途
公开(公告)号：US4310645A
公开(公告)日：1982-01-12
申请号：US213174
申请日：1980-12-04
申请人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
IPC分类号： C08G12/00 , C08G12/02 , C08G12/46 , C08G59/00 , C08G59/14 , C08G59/40 , C08G65/26 , C08K5/29 , C09D5/44 , C09D163/00
CPC分类号： C08G12/46 , C08G12/00 , C08G12/02 , C08G59/1405 , C08G59/4014 , C08G65/2624 , C09D5/4438 , Y10S524/901 , Y10T428/2933
摘要： Polyadducts, free from epoxide groups, are obtained from ammonia and epoxide compounds by reacting 1 mole of ammonia with from 1.2 to 2.0 equivalents of epoxide, so that if diepoxide compounds are used products of the general formula (I) ##STR1## are obtained, while if triepoxides and/or tetraepoxide compounds are used, by themselves, or together with diepoxide compounds, products of the general formula II ##STR2## are produced; in these formulae, the E.sup.1 's are identical or different hydroxyl-containing divalent radicals and the E.sup.2 's are identical or different hydroxyl-containing trivalent or tetravalent radicals, resulting from the opening of the oxirane rings of epoxide compounds containing two, three or four epoxide groups in the molecule, n.sup.1, n.sup.3 and n.sup.5 are from 0 to 3, n.sup.2 and n.sup.4 are from 1 to 3 and X is 0 or 1, and one or more of the divalent radicals E.sup.1 in the general formula (II) may or may not be replaced by polyvalent radicals E.sup.2.The novel polyadducts can be modified by reaction with aldehydes, ketones, monoepoxide compounds, carboxylic acids, carboxylic acid esters or isocyanates, or by protonation with an acid, and may be used, for example, for the cathodic electrocoating of metallic articles.
摘要翻译：通过使1摩尔氨与1.2-2.0当量的环氧化物反应，从氨和环氧化合物得到不含环氧基的多元加成物，因此如果使用二环氧化合物，则得到通式（I）的产物而如果三环氧化物和/或四环氧化合物本身或与二环氧化合物一起使用，则制备通式II的产物（II）; 在这些式中，E1是相同或不同的含羟基的二价基团，并且E2是相同或不同的含羟基的三价或四价基团，其由环氧乙烷环的环氧化物环开放，所述环氧化物包含两个，三个或四个环氧基团分子n1，n3和n5为0〜3，n2和n4为1〜3，X为0或1，通式（II）中的一个或多个二价基团E1可以是也可以不是由多价基团E2代替。可以通过与醛，酮，单环化合物，羧酸，羧酸酯或异氰酸酯的反应或通过用酸质子化来改变新的多加合物，并且可以用于例如金属制品的阴极电泳涂层。

5. 发明授权

US4340714A Preparation of curable polyadducts, containing basic nitrogen groups, and use of the products 失效
标题翻译：制备含碱性氮基的可固化聚合物，以及产品的使用
公开(公告)号：US4340714A
公开(公告)日：1982-07-20
申请号：US266363
申请日：1981-05-22
申请人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
发明人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
IPC分类号： C08G59/00 , C08G14/06 , C08G59/14 , C08G59/64 , C08L63/00 , C09D5/44 , C09D163/00 , C08G59/28
CPC分类号： C08L63/00 , C08G14/06 , C08G59/64 , C09D163/00 , C09D5/4419
摘要： A process for the preparation of curable polyadducts, possessing basic nitrogen groups, wherein (A) monophenols and/or polyphenols, which contain groups of the general formula (I): ##STR1## where R.sup.1 and R.sup.2 are identical or different and each is hydrogen or methyl are reacted with (B) amines having one or more primary and/or secondary amino groups, and the adduct formed is reacted with (C) epoxide compounds having from 1 to 4 epoxide groups per molecule and having a molecular weight of at most 2,500, the ratio of the phenolic hydroxyl groups of (A) to epoxide groups of (C) being from 1:0.5 to 1:2 and the amine (B) being employed in such amount that the resulting polyadduct of (A), (B) and (C) contains from 0.1 to 5% by weight of basic nitrogen, and the use of the products, after protonation with an acid, as binders for the production of coatings, especially for the cathodic electrocoating of metal articles.
摘要翻译：一种制备具有碱性氮基团的可固化聚合物的方法，其中（A）单酚和/或多酚，其含有通式（I）的基团：其中R 1和R 2相同或不同，各自为氢或甲基与（B）具有一个或多个伯和/或仲氨基的胺反应，并且所形成的加合物与（C）每分子具有1至4个环氧基的环氧化物化合物反应，分子量至多为（A）的酚羟基与（C）的环氧基的比例为1:0.5至1:2，胺（B）的使用量使得所得的（A），（ B）和（C）含有0.1至5重量％的碱性氮，并且在用酸质子化后使用该产物作为用于制备涂料的粘合剂，特别是用于金属制品的阴极电泳涂层。

6. 发明授权

US4315840A Preparation of cathodic electrocoating binders 失效
标题翻译：阴极电泳涂料的制备
公开(公告)号：US4315840A
公开(公告)日：1982-02-16
申请号：US85965
申请日：1979-10-18
申请人： Fritz E. Kempter , Eberhard Schupp , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Erich Gulbins
IPC分类号： C08G18/00 , C08G18/08 , C08G18/65 , C08G18/66 , C08G18/80 , C09D5/44 , C09D175/08 , C08G18/48 , C08J3/04 , C08L91/00
CPC分类号： C08G18/0814 , C08G18/8061 , C09D5/4465 , Y10S524/901
摘要： A process for the preparation of self-crosslinking, cathodic electrocoating binders by reacting polyether-polyols, which may or may not contain thio groups, with semi-blocked diisocyanates or partially blocked polyisocyanates, wherein the reaction products (A), containing blocked isocyanate groups, are reacted with a polyamine (B), some of whose amino groups may or may not be in the form of ketimine groups, in such a way that one or more amino groups of the polyamine (B) form a urea group with a blocked isocyanate group of the reaction product (A), and the self-cross-linking reaction product of (A) and (B) is converted into a water-dilutable form in the conventional manner by protonization with an acid.The coating binders prepared according to the invention may be used for cathodic electrocoating of metal articles.
摘要翻译：一种制备自交联阴极电泳涂料粘合剂的方法，该方法是将可能含有或不含有硫基的聚醚多元醇与半封端二异氰酸酯或部分封闭的多异氰酸酯反应，其中含有封端异氰酸酯基团的反应产物（A）与多胺（B）反应，其一些氨基可以是或可以不是酮亚胺基的形式，使得多胺（B）的一个或多个氨基形成具有封闭的脲基团反应产物（A）的异氰酸酯基和（A）和（B）的自交联反应产物以常规方式通过用酸质子化转化成水可稀释形式。根据本发明制备的涂料粘合剂可用于金属制品的阴极电泳涂覆。

7. 发明授权

US4336116A Polyadducts containing unsaturated amide groups and their use in coatings 失效
标题翻译：含有不饱和酰胺基团的多元加成物及其在涂料中的应用
公开(公告)号：US4336116A
公开(公告)日：1982-06-22
申请号：US198226
申请日：1980-10-17
申请人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
发明人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
IPC分类号： C08G59/00 , C08G59/14 , C08G59/56 , C08G59/62 , C09D5/44 , C09D163/00 , C08G59/28 , C08J3/28
CPC分类号： C08G59/56 , C08G59/621 , C09D163/00 , C09D5/4434 , Y10S524/901
摘要： The invention concerns polyadducts and their use.The polyadducts, possessing nitrogen-basic groups, have a mean molecular weight of from 500 to 10,000 and contain groups, attached to aromatic rings, of the general formula (I) ##STR1## where R.sup.1 and R.sup.2 are identical or different and each is hydrogen or methyl.In particular, these polyadducts are used, after protonizing with an acid, as binders for the cathodic electrocoating of metal articles.
摘要翻译：本发明涉及多加合物及其用途。具有氮 - 碱性基团的多元加成物的平均分子量为500〜10,000，并且含有通式（I）的芳环上的基团，其中R 1和R 2相同或不同，各自为氢或甲基。特别地，这些聚加成物在用酸质子化之后用作金属制品的阴极电涂层的粘合剂。

8. 发明授权

US4188312A Surface-coating binders and their use for cathodic electrocoating 失效
标题翻译：表面涂层粘合剂及其用于阴极电泳的用途
公开(公告)号：US4188312A
公开(公告)日：1980-02-12
申请号：US969551
申请日：1978-12-14
申请人： Fritz E. Kempter , Eberhard Schupp , Rainer Blum
发明人： Fritz E. Kempter , Eberhard Schupp , Rainer Blum
IPC分类号： C08G14/06 , C08G59/62 , C08L61/34 , C09D5/44 , C09D163/00 , C25D13/06 , C08L63/00 , C08L91/00
CPC分类号： C09D5/4419 , C08G14/06 , C08G59/623 , C08L61/34 , C09D163/00
摘要： The invention relates to surface-coating binders and to their use.The surface-coating binders, which are substantially free from epoxide groups, are based on a reaction product of (A) a Mannich base obtained from one or more polyhydric phenols which are free from ether groups and contain two or more aromatic rings, and/or one or more monohydric or polyhydric phenols which contain one or more ether groups and contain two or more aromatic rings, one or more secondary amines which contain one or two hydroxyalkyl groups and which may or may not be mixed with secondary dialkylamines or dialkoxyalkylamines, and formaldehyde or a formaldehyde donor, and (B) an epoxy resin, the reaction product of (A) and (B) additionally containing, built into its chemical structure, an olefinically unsaturated alkylphenol of the general formula (I) ##STR1## where R is a radical of 11 to 19 carbon atoms which contains from one to three carbon-carbon double bonds.These surface-coating binders are used, especially in their protonized form, for the cathodic electrocoating of metal articles.
摘要翻译：本发明涉及表面涂层粘合剂及其用途。基本上不含环氧基团的表面涂层粘合剂基于（A）由一种或多种不含醚基并含有两个或多个芳环的多元酚得到的曼尼希碱的反应产物和/ 或一种或多种含有一个或多个醚基并含有两个或更多个芳环的一元或多元酚，一种或多种含有一个或两个羟烷基的仲胺，并且其可与或不与二烷基胺或仲烷氧基烷基胺混合，以及甲醛或甲醛供体，和（B）环氧树脂，（A）和（B）的反应产物在其化学结构中另外含有通式（I）的烯属不饱和烷基酚，其中R 是含有1至3个碳 - 碳双键的11至19个碳原子的基团。这些表面涂层粘合剂特别用于其质子化形式用于金属制品的阴极电泳涂层。

9. 发明申请

US20070149738A1 Method of producing water-soluble nonturbid copolymers of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer 有权
标题翻译：制备至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体的水溶性非混浊共聚物的方法
公开(公告)号：US20070149738A1
公开(公告)日：2007-06-28
申请号：US11643396
申请日：2006-12-21
申请人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell
发明人： Rainer Dobrawa , Ralf Widmaier , Eberhard Schupp , Klaus Schnell
IPC分类号： C08F26/10
CPC分类号： C08F226/10 , C08F216/10
摘要： Method of producing vinyllactam copolymers by free-radical polymerization of at least one water-soluble N-vinyllactam and at least one hydrophobic comonomer in an organic solvent in the presence of an initiator under reflux conditions, where the initiator is introduced into the polymerization mixture from below.
摘要翻译：通过至少一种水溶性N-乙烯基内酰胺和至少一种疏水性共聚单体在引发剂存在下，在回流条件下，在引发剂存在下，在有机溶剂中自由基聚合制备乙烯基内酰胺共聚物的方法，其中将引发剂从下面。

10. 发明授权

US5486586A Adhesives based on polyvinyl ether copolymers 失效
标题翻译：基于聚乙烯醚共聚物的粘合剂
公开(公告)号：US5486586A
公开(公告)日：1996-01-23
申请号：US440119
申请日：1995-05-12
申请人： Hubertus Kroener , Eberhard Schupp , Eckehardt Wistuba , Oral Aydin , Elmar Schwarzenbach , Klaus Schnell
发明人： Hubertus Kroener , Eberhard Schupp , Eckehardt Wistuba , Oral Aydin , Elmar Schwarzenbach , Klaus Schnell
IPC分类号： C08F16/26 , C08F16/14 , C08F16/16 , C08F16/28 , C08F16/30 , C08F216/18 , C09J129/00 , C09J129/10 , C08F16/12
CPC分类号： C09J129/10
摘要： Adhesives containing polyvinyl ether copolymers having a weight average molecular weight of >10,000, comprisea) from 0 to 95% by weight of vinyl ethers of the formula IH.sub.2 C.dbd.CH--O--Rb) from 5 to 100% by weight of hydrophilic vinyl ethers of the formula IIH.sub.2 C.dbd.CH--O--R.sup.1andc) from 0 to 30% by weight of further monomers,where R is C.sub.1 -C.sub.20 -alkyl and R.sup.1 is an aliphatic or cycloaliphatic radical which may be substituted by hydroxyl groups or interrupted by nonadjacent groups --Y--, Y is oxygen, sulfur or a group NR.sup.2 or N.sup.+ R.sup.2 R.sup.3 X.sup.-, R.sup.2 and R.sup.3 independently of one another are each hydrogen or C.sub.1 -C.sub.4 -alkyl and X.sup.- is a counter-anion, and the molar ratio of carbon atoms to the sum of groups Y and hydroxyl groups in the aliphatic or cycloaliphatic radical is from 1.01:1 to 6.5:1.
摘要翻译：包含重均分子量> 10,000的聚乙烯醚共聚物的粘合剂包含a）0至95重量％的式I的乙烯基醚H 2 C = CH-OR b）5至100重量％的亲水乙烯基醚的式IIH 2 C = CH-O-R 1和c）0至30重量％的另外的单体，其中R是C 1 -C 20 - 烷基，R 1是可以被羟基取代或被中断的脂族或脂环族基团通过不相邻的基团-Y-，Y是氧，硫或基团NR2或N + R2R3X-，R2和R3彼此独立地各自是氢或C1-C4-烷基，X是抗衡阴离子，脂肪族或脂环族基团中碳原子与基团Y和羟基之和的比例为1.01:1至6.5:1。

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