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1. 发明授权

US09382361B2 Process to produce ethylene propylene copolymers 有权
标题翻译：生产乙烯丙烯共聚物的方法
公开(公告)号：US09382361B2
公开(公告)日：2016-07-05
申请号：US14640871
申请日：2015-03-06
申请人： Daniel Bilbao , Jeffrey L. Brinen , Carlos U. De Gracia , Henry Dong
发明人： Daniel Bilbao , Jeffrey L. Brinen , Carlos U. De Gracia , Henry Dong
IPC分类号： C08F210/18 , C08F4/643 , C08F4/653 , C08F4/6592 , C08F4/659
CPC分类号： C08F210/18 , C08F4/65904 , C08F4/65908 , C08F4/6592 , C08F210/06 , C08F236/20 , C08F2500/25 , C08F2500/03 , C08F2500/17 , C08F4/65927
摘要： This invention relates to a copolymer prepared using two or more non-coordinating anion activators comprising a first C2 to C12 alpha olefin (such as ethylene), a second C3 to C12 alpha olefin (such as propylene) different from the first alpha olefin, and diene (such as ethylidene norbornene and/or vinyl norbornene), where the polymer has: a) first alpha olefin (ethylene) content of 35 to 90 mol %; b) second alpha olefin (propylene) content of 9.8 to 64.8 mol %; c) diene content of 0.2 to 5 mol %; d) a branching index g′ave of 0.95 or more; e) a complex viscosity ratio (eta*(0.01 rad/s)/eta*(100 rad/s), at 125° C.) greater than 1.1*Y0, where Y0=Y1+{[(Y2−Y1)/(X2−X1)](X0−X1)}, where X0 is the wt % of a first non-coordinating anion activator, NCA1, used to prepare the copolymer (based upon weight of NCA1 and a second non-coordinating anion activator, NCA2, used to prepare the copolymer), X1=0, X2=100, Y1=complex viscosity ratio of polymer made with 100% NCA1 and 0% NCA2, Y2 is complex viscosity ratio of polymer made with 100% NCA2 and 0% NCA1, where NCA1 has an Mw lower than the Mw of NCA2; f) an Mw/Mn of 4.0 or less; g) a melting point of 30° C. or less; and h) a Composition Distribution Breadth Index of 50% or more.
摘要翻译：本发明涉及使用两种或多种非配位阴离子活化剂制备的共聚物，其包含第一C 2 -C 12α-烯烃（如乙烯），不同于第一α-烯烃的第二C 3 -C 12α-烯烃（如丙烯），以及二烯（如亚乙基降冰片烯和/或乙烯基降冰片烯），其中聚合物具有：a）35-90％摩尔的第一α-烯烃（乙烯）含量; b）第二α-烯烃（丙烯）含量为9.8至64.8mol％; c）二烯含量为0.2-5mol％; d）支化指数g'ave为0.95以上; e）大于1.1 * Y0的复数粘度比（eta *（0.01rad / s）/ eta *（100rad / s）），其中Y0 = Y1 + {[（Y2-Y1）/（ X2-X1）]（X0-X1）}，其中X0是用于制备共聚物的第一非配位阴离子活化剂NCA1的重量％（基于NCA1的重量和第二非配位阴离子活化剂NCA2 ，用于制备共聚物），X1 = 0，X2 = 100，Y1 =用100％NCA1和0％NCA2制成的聚合物的复数粘度比，Y2是用100％NCA2和0％NCA1制成的聚合物的复数粘度比，其中NCA1具有低于NCA2的Mw的Mw; f）Mw / Mn为4.0以下; g）熔点为30℃以下; 和h）组合物分布宽度指数为50％以上。

2. 发明申请

US20150307641A1 Process to Produce Ethylene Propylene Copolymers 有权
标题翻译：生产乙烯丙烯共聚物的工艺
公开(公告)号：US20150307641A1
公开(公告)日：2015-10-29
申请号：US14640871
申请日：2015-03-06
申请人： Daniel Bilbao , Jeffrey L. Brinen , Carlos U. De Gracia , Henry Dong
发明人： Daniel Bilbao , Jeffrey L. Brinen , Carlos U. De Gracia , Henry Dong
IPC分类号： C08F210/18
CPC分类号： C08F210/18 , C08F4/65904 , C08F4/65908 , C08F4/6592 , C08F210/06 , C08F236/20 , C08F2500/25 , C08F2500/03 , C08F2500/17 , C08F4/65927
摘要： This invention relates to a copolymer prepared using two or more non-coordinating anion activators comprising a first C2 to C12 alpha olefin (such as ethylene), a second C3 to C12 alpha olefin (such as propylene) different from the first alpha olefin, and diene (such as ethylidene norbornene and/or vinyl norbornene), where the polymer has: a) first alpha olefin (ethylene) content of 35 to 90 mol %; b) second alpha olefin (propylene) content of 9.8 to 64.8 mol %; c) diene content of 0.2 to 5 mol %; d) a branching index g′ave of 0.95 or more; e) a complex viscosity ratio (eta*(0.01 rad/s)/eta*(100 rad/s), at 125° C.) greater than 1.1*Y0, where Y0=Y1+{[(Y2−Y1)/(X2−X1)](X0−X1)}, where X0 is the wt % of a first non-coordinating anion activator, NCA1, used to prepare the copolymer (based upon weight of NCA1 and a second non-coordinating anion activator, NCA2, used to prepare the copolymer), X1=0, X2=100, Y1=complex viscosity ratio of polymer made with 100% NCA1 and 0% NCA2, Y2 is complex viscosity ratio of polymer made with 100% NCA2 and 0% NCA1, where NCA1 has an Mw lower than the Mw of NCA2; f) an Mw/Mn of 4.0 or less; g) a melting point of 30° C. or less; and h) a Composition Distribution Breadth Index of 50% or more.
摘要翻译：本发明涉及使用两种或多种非配位阴离子活化剂制备的共聚物，其包含第一C 2 -C 12α-烯烃（如乙烯），不同于第一α-烯烃的第二C 3 -C 12α-烯烃（如丙烯），以及二烯（如亚乙基降冰片烯和/或乙烯基降冰片烯），其中聚合物具有：a）35-90％摩尔的第一α-烯烃（乙烯）含量; b）第二α-烯烃（丙烯）含量为9.8至64.8mol％; c）二烯含量为0.2-5mol％; d）支化指数g'ave为0.95以上; e）大于1.1 * Y0的复数粘度比（eta *（0.01rad / s）/ eta *（100rad / s）），其中Y0 = Y1 + {[（Y2-Y1）/（ X2-X1）]（X0-X1）}，其中X0是用于制备共聚物的第一非配位阴离子活化剂NCA1的重量％（基于NCA1的重量和第二非配位阴离子活化剂NCA2 ，用于制备共聚物），X1 = 0，X2 = 100，Y1 =用100％NCA1和0％NCA2制成的聚合物的复数粘度比，Y2是用100％NCA2和0％NCA1制成的聚合物的复数粘度比，其中NCA1具有低于NCA2的Mw的Mw; f）Mw / Mn为4.0以下; g）熔点为30℃以下; 和h）组合物分布宽度指数为50％以上。

3. 发明授权

US07981536B2 Microporous membrane, battery separator and battery 有权
标题翻译：微孔膜，电池分离器和电池
公开(公告)号：US07981536B2
公开(公告)日：2011-07-19
申请号：US11513557
申请日：2006-08-31
申请人： Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
发明人： Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
IPC分类号： H01M2/16 , H01M2/18 , B32B27/08 , B29C47/00
CPC分类号： B32B27/32 , B01D67/0009 , B01D67/0027 , B01D69/12 , B01D71/26 , B01D2325/02 , B01D2325/20 , B01D2325/34 , B32B5/22 , H01M2/145 , H01M2/1653 , H01M2/1686 , H01M10/0525 , Y10T428/31913 , Y10T428/31938
摘要： Disclosed herein is multi-layer, microporous polyolefin membrane comprising a first porous layer comprising primarily a polyethylene, and a second porous layer comprising a polyethylene resin and polypropylene, the polypropylene having a weight-average molecular weight of 6×105 or more and a heat of fusion (measured by a differential scanning calorimeter) of 90 J/g or more, a fraction of the polypropylene having a molecular weight of 5×104 or less being 5% or less by mass.
摘要翻译：本文公开了多层微孔聚烯烃膜，其包含主要包含聚乙烯的第一多孔层和包含聚乙烯树脂和聚丙烯的第二多孔层，所述聚丙烯的重均分子量为6×10 5以上，热量（通过差示扫描量热计测定）为90J / g以上，分子量为5×10 4以下的聚丙烯的分数为5质量％以下。

4. 发明授权

US07872086B2 Polymeric material and its manufacture and use 有权
公开(公告)号：US07872086B2
公开(公告)日：2011-01-18
申请号：US12016106
申请日：2008-01-17
申请人： Patrick Brant , Jeffrey L. Brinen , Zerong Lin , Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki
发明人： Patrick Brant , Jeffrey L. Brinen , Zerong Lin , Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki
IPC分类号： C08F10/06 , C08F4/72
CPC分类号： C08F10/06 , C08F10/00 , C08F110/06 , C08L23/04 , C08L23/06 , C08L23/0815 , C08L23/142 , H01M2/145 , H01M2/1653 , Y10S526/916 , C08F4/642 , C08L2666/02 , C08F2500/20 , C08F2500/01 , C08F2500/12 , C08F2500/17 , C08F2500/15 , C08F2500/26
摘要： Disclosed herein is a polymer composition, its manufacture and use, said composition may comprise greater than about 90 mole % propylene monomer, and having a unique combination of properties, including one or more of the following: a heat of fusion of more than about 108 J/g, a melting point of 165° C. or higher, a Melt Flow Rate so low that it is essentially not measurable and a molecular weight of greater than about 1.5×106. Further disclosed herein are blends or mixtures of the present novel polymer composition and products, such as, for example, microporous film structures and the like comprising same.

5. 发明申请

US20090123827A1 Multi-layer, microporous membrane, battery separator and battery 有权
标题翻译：多层，微孔膜，电池分离器和电池
公开(公告)号：US20090123827A1
公开(公告)日：2009-05-14
申请号：US11940196
申请日：2007-11-14
申请人： Koichi Kono , Kohtaro Kimishima , Hiroyuik Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
发明人： Koichi Kono , Kohtaro Kimishima , Hiroyuik Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
IPC分类号： H01M2/18 , B32B3/26 , C08J9/00
CPC分类号： C08J5/2231 , B29C47/0004 , B29C47/0021 , B29C47/06 , B29C47/14 , B29C47/40 , B29C47/8805 , B29C47/8845 , B29K2105/256 , B29L2009/00 , B29L2031/3468 , B29L2031/755 , C08J2323/00 , H01M2/1653 , H01M10/0525 , Y10T428/249978 , Y10T428/24998
摘要： The invention relates to a multi-layer, microporous polyolefin membrane having appropriate permeability, pin puncture strength, shutdown temperature, shutdown speed, meltdown temperature, and thickness uniformity. The invention also relates to a battery separator formed by such multi-layer, microporous membrane, and a battery comprising such a separator. Another aspect of the invention relates to a method for making the multi-layer, microporous polyolefin membrane, a method for making a battery using such a membrane as a separator, and a method for using such a battery.
摘要翻译：本发明涉及具有适当渗透性，针穿刺强度，停机温度，停机速度，熔化温度和厚度均匀性的多层微孔聚烯烃膜。本发明还涉及由这种多层微孔膜形成的电池隔膜以及包括这种隔膜的电池。本发明的另一方面涉及一种制造多层微孔聚烯烃膜的方法，使用这种膜作隔膜制造电池的方法以及使用这种电池的方法。

6. 发明授权

US08012622B2 Multi-layer, microporous membrane, battery separator and battery 有权
标题翻译：多层，微孔膜，电池分离器和电池
公开(公告)号：US08012622B2
公开(公告)日：2011-09-06
申请号：US11940196
申请日：2007-11-14
申请人： Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
发明人： Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
IPC分类号： H01M2/18
CPC分类号： C08J5/2231 , B29C47/0004 , B29C47/0021 , B29C47/06 , B29C47/14 , B29C47/40 , B29C47/8805 , B29C47/8845 , B29K2105/256 , B29L2009/00 , B29L2031/3468 , B29L2031/755 , C08J2323/00 , H01M2/1653 , H01M10/0525 , Y10T428/249978 , Y10T428/24998
摘要： The invention relates to a multi-layer, microporous polyolefin membrane having appropriate permeability, pin puncture strength, shutdown temperature, shutdown speed, meltdown temperature, and thickness uniformity. The invention also relates to a battery separator formed by such multi-layer, microporous membrane, and a battery comprising such a separator. Another aspect of the invention relates to a method for making the multi-layer, microporous polyolefin membrane, a method for making a battery using such a membrane as a separator, and a method for using such a battery.
摘要翻译：本发明涉及具有适当渗透性，针穿刺强度，停机温度，停机速度，熔化温度和厚度均匀性的多层微孔聚烯烃膜。本发明还涉及由这种多层微孔膜形成的电池隔膜以及包括这种隔膜的电池。本发明的另一方面涉及一种制造多层微孔聚烯烃膜的方法，使用这种膜作隔膜制造电池的方法以及使用这种电池的方法。

7. 发明申请

US20110086276A1 Polymeric Material And Its Manufacture And Use 有权
标题翻译：聚合材料及其制造与使用
公开(公告)号：US20110086276A1
公开(公告)日：2011-04-14
申请号：US12962717
申请日：2010-12-08
申请人： Patrick Brant , Jeffrey L. Brinen , Zerong Lin , Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki
发明人： Patrick Brant , Jeffrey L. Brinen , Zerong Lin , Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki
IPC分类号： H01M2/16 , H01M2/18 , B29C35/08 , B29C47/04 , B29C44/00
CPC分类号： C08F10/06 , C08F10/00 , C08F110/06 , C08L23/04 , C08L23/06 , C08L23/0815 , C08L23/142 , H01M2/145 , H01M2/1653 , Y10S526/916 , C08F4/642 , C08L2666/02 , C08F2500/20 , C08F2500/01 , C08F2500/12 , C08F2500/17 , C08F2500/15 , C08F2500/26
摘要： Disclosed herein is a polymer composition, its manufacture and use, said composition may comprise greater than about 90 mole % propylene monomer, and having a unique combination of properties, including one or more of the following: a heat of fusion of more than about 108 J/g, a melting point of 165° C. or higher, a Melt Flow Rate so low that it is essentially not measurable and a molecular weight of greater than about 1.5×106. Further disclosed herein are blends or mixtures of the present novel polymer composition and products, such as, for example, microporous film structures and the like comprising same.
摘要翻译：本文公开了聚合物组合物，其制备和用途，所述组合物可包含大于约90摩尔％的丙烯单体，并且具有独特的性质组合，包括以下一种或多种：约超过约108的熔化热 J / g，熔点为165℃或更高，熔体流动速率低至基本上不可测量，分子量大于约1.5×10 6。本文进一步公开的是本发明的新型聚合物组合物和产品的混合物或混合物，例如包含其的微孔膜结构等。

8. 发明申请

US20080057389A1 Microporous membrane, battery separator and battery 有权
标题翻译：微孔膜，电池分离器和电池
公开(公告)号：US20080057389A1
公开(公告)日：2008-03-06
申请号：US11513557
申请日：2006-08-31
申请人： Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
发明人： Koichi Kono , Kohtaro Kimishima , Hiroyuki Ozaki , Patrick Brant , Jeffrey L. Brinen , Zerong Lin
IPC分类号： H01M2/16 , B32B27/32 , B29C47/00
CPC分类号： B32B27/32 , B01D67/0009 , B01D67/0027 , B01D69/12 , B01D71/26 , B01D2325/02 , B01D2325/20 , B01D2325/34 , B32B5/22 , H01M2/145 , H01M2/1653 , H01M2/1686 , H01M10/0525 , Y10T428/31913 , Y10T428/31938
摘要： Disclosed herein is multi-layer, microporous polyolefin membrane comprising a first porous layer comprising primarily a polyethylene, and a second porous layer comprising a polyethylene resin and polypropylene, the polypropylene having a weight-average molecular weight of 6×105 or more and a heat of fusion (measured by a differential scanning calorimeter) of 90 J/g or more, a fraction of the polypropylene having a molecular weight of 5×104 or less being 5% or less by mass.
摘要翻译：本文公开了多层微孔聚烯烃膜，其包含主要包含聚乙烯的第一多孔层和包含聚乙烯树脂和聚丙烯的第二多孔层，所述聚丙烯的重均分子量为6×10 5 / >以上，聚合热（通过差示扫描量热计测定）为90J / g以上，分子量为5×10 4以下的聚丙烯的比例为5％以下的质量。

9. 发明授权

US07279012B2 Process for producing olefins 有权
标题翻译：烯烃生产方法
公开(公告)号：US07279012B2
公开(公告)日：2007-10-09
申请号：US10882722
申请日：2004-07-01
申请人： Keith H. Kuechler , Jeffrey L. Brinen , Philip Andrew Ruziska
发明人： Keith H. Kuechler , Jeffrey L. Brinen , Philip Andrew Ruziska
IPC分类号： C07C7/00
CPC分类号： C07C11/06 , C07C11/04 , Y02P30/42 , Y02P30/48
摘要： A process for producing olefins comprises providing a vapor product stream from an oxygenate to olefin reaction, the vapor product stream comprising C2 to C4 olefins, C2 to C6 carbonyl compounds and water. The vapor product stream is cooled to provide a first vapor effluent stream comprising no more than 10 wt. % water, and a liquid water-rich stream. The first vapor effluent stream, and a first wash flash vapor stream, are compressed from a first pressure to a second pressure greater than said first pressure to form a second vapor effluent stream, which is then cooled to form a cooled second effluent stream that is at least partially in the vapor state. At least part of the cooled second effluent stream is washed with a liquid alcohol-containing stream, at a third pressure greater than the first pressure but not greater than the second pressure, to produce a wash liquid stream, which comprises C3 and C4 olefins, and a wash vapor stream, which contains less C2 to C6 carbonyl compounds than the first vapor effluent stream. The wash liquid stream is exposed to a pressure of at least the first pressure but less than the third pressure to form a first wash flash liquid stream and the first wash flash vapor stream, the first wash flash vapor stream being provided for compression with the first vapor effluent stream.
摘要翻译：制备烯烃的方法包括提供从含氧化合物到烯烃反应的蒸汽产物流，所述蒸气产物流包含C 2至C 4烯烃，C 2 - / C 1 -C 6羰基化合物和水。蒸气产物流被冷却以提供包含不超过10wt。％的水和富含液体的水。第一蒸汽流出物流和第一洗涤闪蒸蒸气流从第一压力被压缩至大于所述第一压力的第二压力，以形成第二蒸气流出物流，然后将其冷却以形成冷却的第二流出物流，其为至少部分处于蒸汽状态。至少部分冷却的第二流出物流用含液体醇的流在大于第一压力但不大于第二压力的第三压力下洗涤，以产生洗涤液体流，其包含C 3 和C 4 O 3烯烃，以及与第一蒸气相比含有较少C 2 -C 6羰基化合物的洗涤蒸汽流流出物流。洗涤液体流暴露于至少第一压力但小于第三压力的压力以形成第一洗涤闪蒸液流和第一洗涤闪蒸蒸气流，第一洗涤闪蒸蒸气流被提供用于与第一蒸汽流出物流。

10. 发明授权

US07074971B2 Recovery of ethylene and propylene from a methanol to olefin reaction system 有权
标题翻译：乙烯和丙烯从甲醇回收到烯烃反应体系
公开(公告)号：US07074971B2
公开(公告)日：2006-07-11
申请号：US10383204
申请日：2003-03-06
申请人： Cor F. Van Egmond , Jeffrey L. Brinen
发明人： Cor F. Van Egmond , Jeffrey L. Brinen
IPC分类号： C07C41/42
CPC分类号： C07C7/04 , C07C11/04 , C07C11/06
摘要： The present invention provides new highly-efficient separation processes and systems for separating polymerization-grade ethylene and propylene from an initial effluent stream comprising ethane, ethylene, propylene, dimethyl ether, and one or more of propane, acetylene, methyl acetylene, propadiene, methane, hydrogen, carbon monoxide, carbon dioxide and C4+ components. In one embodiment, the initial effluent stream is provided from a methanol-to-olefin reaction system. It has been discovered that the best separation of these components is realized when DME is selectively removed in a first separation step, followed by separation of the remaining components in additional separation steps.
摘要翻译：本发明提供了用于从包含乙烷，乙烯，丙烯，二甲醚和丙烷，乙炔，甲基乙炔，丙二烯，甲烷中的一种或多种的初始流出物流分离聚合级乙烯和丙烯的新的高效分离方法和系统，氢气，一氧化碳，二氧化碳和C4 +组分。在一个实施方案中，初始流出物流由甲醇 - 烯烃反应系统提供。已经发现，当在第一分离步骤中选择性除去DME，然后在另外的分离步骤中分离剩余组分时，实现这些组分的最佳分离。

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