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1. 发明授权

US08192527B2 Purification method by hydrogen adsorbtion with cogeneration of CO2 stream pressure 有权
标题翻译：通过氢气吸附的CO 2流压力的热电联产的纯化方法
公开(公告)号：US08192527B2
公开(公告)日：2012-06-05
申请号：US12520778
申请日：2007-11-30
申请人： Gerhard Pirngruber , Elsa Jolimaitre , Luc Wolff , Damien Leinekugel le Cocq
发明人： Gerhard Pirngruber , Elsa Jolimaitre , Luc Wolff , Damien Leinekugel le Cocq
IPC分类号： B01D59/26
CPC分类号： B01D53/047 , B01D2253/102 , B01D2253/106 , B01D2253/204 , B01D2253/302 , B01D2253/306 , B01D2253/308 , B01D2253/311 , B01D2256/16 , B01D2257/50 , B01D2257/702 , B01D2259/4003 , B01D2259/40045 , B01D2259/404 , B01D2259/4067 , B01D2259/4145 , C01B3/56 , C01B2203/0405 , C01B2203/0415 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , Y02C10/08 , Y02C20/20 , Y02P20/152
摘要： The present invention relates to a method of producing hydrogen of very high purity from a feed predominantly containing said hydrogen and a minor part of impurities mainly consisting of carbon dioxide, carbon monoxide, methane and heavier hydrocarbons. The purification method by hydrogen adsorption using a desorption stage at a lower pressure than the pressure of the feed, such as a PSA method for example, allows to produce the desorption stream and notably to recover the carbon dioxide under pressure and high-purity hydrogen, with a high yield. These performances are obtained by combining the successive stages of the method according to the invention with the use of a new family of adsorbent whose dynamic capacity at a high desorption pressure is greater than that of conventional adsorbents.
摘要翻译：本发明涉及从主要含有所述氢的原料和主要由二氧化碳，一氧化碳，甲烷和较重烃组成的少量杂质生产非常高纯度的氢的方法。使用例如PSA方法的PSA方法在比压力低的压力下使用解吸阶段进行氢吸附的净化方法允许产生解吸流，特别是在压力和高纯度氢气下回收二氧化碳，产量高。这些性能是通过将根据本发明的方法的连续阶段与使用在高解吸压力下的动态容量大于常规吸附剂的新型吸附剂系列相结合而获得的。

2. 发明授权

US07759534B2 Process and device for improved separation of paraxylene in a simulated moving bed 有权
标题翻译：用于改进模拟移动床中对二甲苯分离的方法和装置
公开(公告)号：US07759534B2
公开(公告)日：2010-07-20
申请号：US12181771
申请日：2008-07-29
申请人： Philibert Leflaive , Lue Wolff , Damien Leinekugel Le Cocq
发明人： Philibert Leflaive , Lue Wolff , Damien Leinekugel Le Cocq
IPC分类号： C07C7/12
CPC分类号： B01D15/185 , C07C7/12 , C07C7/13 , C07C15/08
摘要： Process for separating paraxylene with a purity that is at least equal to 99.5% by weight from an aromatic feedstock F in a single adsorption stage in a simulated moving bed (SMB), comprising different numbers of beds, allocated to a zone 1 between the supply of the desorbent D and the draw-off of the extract E; a zone 2 between the draw-off of the extract E and the supply of the feedstock F; a zone 3 between the supply of the feedstock and the draw-off of the raffinate R; a zone 4 between the draw-off of the raffinate R and the supply of the desorbent D, wherein an SMB of 12 adsorbent beds has bed configuration (2, 5, 3, 2), an SMB of 15 adsorbent beds has bed configuration (3, 6, 4 , 2), or an SMB of 19 adsorbent beds has bed configuration (4, 7, 6, 2), wherein the desorbent in this latter case is paradiethylbenzene.
摘要翻译：在模拟移动床（SMB）中在单个吸附阶段中从芳香原料F分离至少等于99.5重量％的纯度的对二甲苯的方法，包括不同数量的床，分配给供应的区域1 的脱附剂D和萃取物E的排出物; 提取物E的抽出和原料F的供给之间的区域2; 在原料供应和萃余液R的排出之间的区域3; 在萃余液R的抽出和解吸剂D的供应之间的区域4，其中12个吸附床的SMB具有床构型（2,5,3,2），15个吸附床的SMB具有床构型 3，6，4，2），或19个吸附剂床的SMB具有床构型（4,7,6,2），其中在后一种情况下的解吸剂是对二甲基苯。

3. 发明授权

US07838714B2 Process and device for improved separation of metaxylene in a simulated moving bed 有权
标题翻译：在模拟移动床中改善间二甲苯分离的方法和装置
公开(公告)号：US07838714B2
公开(公告)日：2010-11-23
申请号：US12181525
申请日：2008-07-29
申请人： Philibert Leflaive , Luc Wolff , Damien Leinekugel Le Cocq
发明人： Philibert Leflaive , Luc Wolff , Damien Leinekugel Le Cocq
IPC分类号： C07C7/12
CPC分类号： B01D15/185 , B01D53/06 , B01D2257/7027 , C07C7/13 , C07C15/08
摘要： Process for separation of metaxylene, with at least 99% by weight of purity of an aromatic feedstock F, in a single adsorption stage in a simulated moving bed in an SMB device that comprises 12, 13 or 15 adsorbent beds with different numbers of beds being employed in zone 1 between the supply of the desorbent D and the draw-off of the extract E; zone 2 between the draw-off of the extract E and the supply of the feedstock F; zone 3 between the supply of the feedstock and the draw-off of the raffinate R; and zone 4 between the draw-off of the raffinate R and the supply of the desorbent D whereby the process is carried out according to a configuration of zones (a, b, c, d), whereby a, b, c, and d represent the number of adsorbent beds that operate respectively in zones 1, 2, 3, 4 in which there is used: Either an SMB of 12 adsorbent beds operating according to the configuration (2, 5, 3, 2), Or an SMB of 13 adsorbent beds operating according to the configuration (2, 5, 4, 2), Or an SMB of 15 adsorbent beds operating according to the configuration (2, 6, 4, 3).
摘要翻译：在SMB装置的模拟移动床的单个吸附阶段中分离具有至少99重量％芳族原料F的至少99重量％的间二甲苯的方法，所述SMB装置包含12,13或15个具有不同床数的吸附剂床在供应解吸剂D与提取物E的排出之间的区域1中使用; 提取物E的抽出和原料F的供给之间的区域2; 在原料供应和萃余液R的排出之间的区域3; 和抽提物R的抽出和解吸剂D的供给之间的区域4，由此根据区域（a，b，c，d）的构造进行处理，由此a，b，c和d 表示分别在其中使用的区域1,2,3,4中操作的吸附剂床的数量：根据配置（2,5,3,2）操作的12个吸附床的SMB，或者根据配置（2,5,3,2）操作的SMB或者 13个吸附床根据结构（2,5,4,2）操作，或15个吸附床的SMB（根据配置操作（2,6,4,3））。

4. 发明申请

US20100089233A1 PURIFICATION METHOD BY HYDROGEN ADSORBTION WITH COGENERATION OF CO2 STREAM PRESSURE 有权
标题翻译：通过氢化二氧化碳流动压力的氢吸附的纯化方法
公开(公告)号：US20100089233A1
公开(公告)日：2010-04-15
申请号：US12520778
申请日：2007-11-30
申请人： Gerhard Pirngruber , Elsa Jolimaitre , Luc Wolff , Damien Leinekugel Le Cocq
发明人： Gerhard Pirngruber , Elsa Jolimaitre , Luc Wolff , Damien Leinekugel Le Cocq
IPC分类号： B01D53/047
CPC分类号： B01D53/047 , B01D2253/102 , B01D2253/106 , B01D2253/204 , B01D2253/302 , B01D2253/306 , B01D2253/308 , B01D2253/311 , B01D2256/16 , B01D2257/50 , B01D2257/702 , B01D2259/4003 , B01D2259/40045 , B01D2259/404 , B01D2259/4067 , B01D2259/4145 , C01B3/56 , C01B2203/0405 , C01B2203/0415 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , Y02C10/08 , Y02C20/20 , Y02P20/152
摘要： The present invention relates to a method of producing hydrogen of very high purity from a feed predominantly containing said hydrogen and a minor part of impurities mainly consisting of carbon dioxide, carbon monoxide, methane and heavier hydrocarbons.The purification method by hydrogen adsorption using a desorption stage at a lower pressure than the pressure of the feed, such as a PSA method for example, allows to produce the desorption stream and notably to recover the carbon dioxide under pressure and high-purity hydrogen, with a high yield.These performances are obtained by combining the successive stages of the method according to the invention with the use of a new family of adsorbent whose dynamic capacity at a high desorption pressure is greater than that of conventional adsorbents.
摘要翻译：本发明涉及从主要含有所述氢的原料和主要由二氧化碳，一氧化碳，甲烷和较重烃组成的少量杂质生产非常高纯度的氢的方法。使用例如PSA方法的PSA方法在比压力低的压力下使用解吸阶段进行氢吸附的净化方法允许产生解吸流，特别是在压力和高纯度氢气下回收二氧化碳，产量高。这些性能是通过将根据本发明的方法的连续阶段与使用在高解吸压力下的动态容量大于常规吸附剂的新型吸附剂系列相结合而获得的。

5. 发明申请

US20090036726A1 PROCESS AND DEVICE FOR IMPROVED SEPARATION OF METAXYLENE IN A SIMULATED MOVING BED 有权
标题翻译：在模拟移动床中改进分离亚甲基的方法和装置
公开(公告)号：US20090036726A1
公开(公告)日：2009-02-05
申请号：US12181525
申请日：2008-07-29
申请人： Philibert Leflaive , Luc Wolff , Damien Leinekugel Le Cocq
发明人： Philibert Leflaive , Luc Wolff , Damien Leinekugel Le Cocq
IPC分类号： C07C7/12
CPC分类号： B01D15/185 , B01D53/06 , B01D2257/7027 , C07C7/13 , C07C15/08
摘要： Process for separation of metaxylene, with at least 99% by weight of purity of an aromatic feedstock F, in a single adsorption stage in a simulated moving bed in an SMB device that comprises 12, 13 or 15 adsorbent beds with different numbers of beds being employed in zone 1 between the supply of the desorbent D and the draw-off of the extract E; zone 2 between the draw-off of the extract E and the supply of the feedstock F; zone 3 between the supply of the feedstock and the draw-off of the raffinate R; and zone 4 between the draw-off of the raffinate R and the supply of the desorbent D whereby the process is carried out according to a configuration of zones (a, b, c, d), whereby a, b, c, and d represent the number of adsorbent beds that operate respectively in zones 1, 2, 3, 4 in which there is used: Either an SMB of 12 adsorbent beds operating according to the configuration (2, 5, 3, 2), Or an SMB of 13 adsorbent beds operating according to the configuration (2, 5, 4, 2), Or an SMB of 15 adsorbent beds operating according to the configuration (2, 6, 4, 3).
摘要翻译：在SMB装置的模拟移动床的单个吸附阶段中分离具有至少99重量％芳族原料F的至少99重量％的间二甲苯的方法，所述SMB装置包含12,13或15个具有不同床数的吸附剂床在供应解吸剂D与提取物E的排出之间的区域1中使用; 提取物E的抽出和原料F的供给之间的区域2; 在原料供应和萃余液R的排出之间的区域3; 和抽提物R的抽出和解吸剂D的供给之间的区域4，由此根据区域（a，b，c，d）的构造进行处理，由此a，b，c和d 表示分别在其中使用的区域1,2,3,4中操作的吸附剂床的数量：根据配置（2,5,3,2）操作的12个吸附床的SMB，或者根据配置（2,5,3,2）操作的SMB或者 13个吸附床根据结构（2,5,4,2）操作，或15个吸附床的SMB（根据配置操作（2,6,4,3））。

6. 发明申请

US20090018380A1 PROCESS AND DEVICE FOR IMPROVED SEPARATION OF PARAXYLENE IN A SIMULATED MOVING BED 有权
标题翻译：在模拟移动床中改善分离PARAXYLENE的方法和装置
公开(公告)号：US20090018380A1
公开(公告)日：2009-01-15
申请号：US12181771
申请日：2008-07-29
申请人： Philibert LEFLAIVE , Lue Wolff , Damien Leinekugel Le Cocq
发明人： Philibert LEFLAIVE , Lue Wolff , Damien Leinekugel Le Cocq
IPC分类号： C07C7/12
CPC分类号： B01D15/185 , C07C7/12 , C07C7/13 , C07C15/08
摘要： Process for separating paraxylene with a purity that is at least equal to 99.5% by weight from an aromatic feedstock F in a single adsorption stage in a simulated moving bed (SMB), comprising different numbers of beds, allocated to a zone 1 between the supply of the desorbent D and the draw-off of the extract E; a zone 2 between the draw-off of the extract E and the supply of the feedstock F; a zone 3 between the supply of the feedstock and the draw-off of the raffinate R; a zone 4 between the draw-off of the raffinate R and the supply of the desorbent D, wherein an SMB of 12 adsorbent beds has bed configuration (2, 5, 3, 2), an SMB of 15 adsorbent beds has bed configuration (3, 6, 4, 2), or an SMB of 19 adsorbent beds has bed configuration (4, 7, 6, 2), wherein the desorbent in this latter case is paradiethylbenzene.
摘要翻译：在模拟移动床（SMB）中在单个吸附阶段中从芳香原料F分离至少等于99.5重量％的纯度的对二甲苯的方法，包括不同数量的床，分配给供应的区域1 的脱附剂D和萃取物E的排出物; 提取物E的抽出和原料F的供给之间的区域2; 在原料供应和萃余液R的排出之间的区域3; 在萃余液R的抽出和解吸剂D的供应之间的区域4，其中12个吸附床的SMB具有床构型（2,5,3,2），15个吸附床的SMB具有床构型 3，6，4，2），或19个吸附剂床的SMB具有床构型（4,7,6,2），其中在后一种情况下的解吸剂是对二甲基苯。

7. 发明授权

US08658848B2 Highly flexible process and apparatus for the simulated counter-current production of para-xylene 有权
标题翻译：用于模拟逆流生产对二甲苯的高度灵活的工艺和设备
公开(公告)号：US08658848B2
公开(公告)日：2014-02-25
申请号：US13593819
申请日：2012-08-24
申请人： Damien Leinekugel Le Cocq , Philibert Leflaive , Luc Wolff , Gerard Hotier
发明人： Damien Leinekugel Le Cocq , Philibert Leflaive , Luc Wolff , Gerard Hotier
IPC分类号： C07C7/12
CPC分类号： B01D15/1821 , C07C7/13 , C07C15/08
摘要： A process for the production of para-xylene by simulated counter-current adsorption with high flexibility with respect to a reference run (100%) uses 2 adsorbers each with 12 beds, said adsorbers being able to be connected in accordance with 3 different modes; the flexibility obtained is 50% to 150%.
摘要翻译：通过相对于参考流程（100％）具有高柔性的模拟逆流吸附生产对二甲苯的方法使用两个具有12个床的吸附器，所述吸附器能够根据3种不同模式连接; 所获得的灵活性为50％至150％。

8. 发明申请

US20130006031A1 PROCESS AND APPARATUS FOR SIMULATED COUNTER-CURRENT CHROMATOGRAPHIC SEPARATION USING TWO ADSORBERS IN PARALLEL FOR OPTIMIZED PARA-XYLENE PRODUCTION 有权
标题翻译：用于模拟对流色谱分离的方法和装置，使用两个吸附剂并行进行优化的PARA-XYLENE生产
公开(公告)号：US20130006031A1
公开(公告)日：2013-01-03
申请号：US13495423
申请日：2012-06-13
申请人： Philibert LEFLAIVE , Damien LEINEKUGEL LE COCQ , Gerard HOTIER , Luc WOLFF
发明人： Philibert LEFLAIVE , Damien LEINEKUGEL LE COCQ , Gerard HOTIER , Luc WOLFF
IPC分类号： C07C7/12
CPC分类号： B01D15/1821 , C07C7/13 , C07C15/08
摘要： The present invention describes a novel configuration for simulated moving bed separation processes characterized by using two adsorbers each containing 12 beds, these two adsorbers functioning in parallel. This novel configuration can be used to optimize para-xylene production.
摘要翻译：本发明描述了一种用于模拟移动床分离方法的新型结构，其特征在于使用两个各自含有12个床的吸附器，这两个吸附器平行起作用。这种新颖的配置可用于优化对二甲苯生产。

9. 发明授权

US08049055B2 Process and device for separation in a simulated moving bed with a bypass fluid flow rate that is not regulated automatically 有权
标题翻译：具有不受自动调节的旁路流体流量的模拟移动床中的分离过程和装置
公开(公告)号：US08049055B2
公开(公告)日：2011-11-01
申请号：US12543091
申请日：2009-08-18
申请人： Xavier Decoodt , Gerard Hotier , Philibert Leflaive , Damien Leinekugel Le Cocq
发明人： Xavier Decoodt , Gerard Hotier , Philibert Leflaive , Damien Leinekugel Le Cocq
IPC分类号： C07C7/12
CPC分类号： B01D15/1835 , B01D15/1842 , C07C7/13 , C07C15/08
摘要： Process for separation of a feedstock F by adsorption in a simulated moving bed in an SMB device that comprises a zone 1 for desorption of compounds produced by extraction, a zone 2 for desorption of compounds produced with a raffinate, a zone 3 for adsorption of compounds produced by extraction, and a zone 4 that is located between the draw-off of the raffinate and the supply of the desorbent,whereby the device comprises external bypass lines Li/i+1 directly joining two successive plates Pi, Pi+, that are equipped with non-automated means for adjusting flow rate and closing means, in which the degree of opening of the restriction means of the scavenging flow rate of the bypass lines Li/i+1 is adjusted so as to obtain the best performance of the SMB.
摘要翻译：在SMB装置的模拟移动床中通过吸附分离原料F的方法，其包括用于解吸由萃取物生产的化合物的区域1，用萃余液生产的化合物解吸区域2，用于吸附化合物的区域3 通过提取产生的区域4和位于萃余液的抽出物和解吸剂的供应之间的区域4，由此该装置包括直接连接两个连续的板Pi，Pi +的外部旁路管线Li / i + 1，其配备用于调节旁路管线Li / i + 1的清除流量限制装置的开度的调节流量和关闭装置的非自动化装置，以获得SMB的最佳性能。

10. 发明申请

US20110201865A1 PROCESS AND DEVICE FOR SIMULATED MOVING BED SEPARATION WITH A MODULATED BY-PASS FLUID FLOW 有权
标题翻译：模拟移动床分离与调制旁路流体流动的过程和装置
公开(公告)号：US20110201865A1
公开(公告)日：2011-08-18
申请号：US13059773
申请日：2009-07-29
申请人： Xavier Decoodt , Gerard Hotier , Philibert Leflaive , Damien Leinekugel Le Cocq
发明人： Xavier Decoodt , Gerard Hotier , Philibert Leflaive , Damien Leinekugel Le Cocq
IPC分类号： C07C7/12 , B01D53/08
CPC分类号： B01D15/1835 , C07C7/12 , C10G25/06 , C10G25/12 , C10G53/08 , C10G2300/1096 , C10G2400/02 , C10G2400/30 , C07C15/08
摘要： A process for separating a feed F by simulated moving bed adsorption in a SMB device comprises at least one zone 1 for desorption of the compounds produced in the extract, a zone 2 for desorption of the compounds produced in the raffinate, a zone 3 for adsorption of the compounds produced in the extract, a zone 4 located between the raffinate withdrawal and the desorbant supply, the device comprising external by-pass lines Li/i+1 directly connecting two successive plates Pi and Pi+1;in which the degree of opening of means for restricting the flushing flow rate of the by-pass lines Li/i+1 are sequentially modified such that: 1) in an operational zone where there is at least one closed by-pass line, a super-synchronicity of the flushing flow rate is established in all of the by-pass lines which are not closed belonging to the zone under consideration, said super-synchronicity being defined by the following formula: S=a+b(nf/nt) in which the constant a is a constant in the range −5 to 5 and b is a constant in the range 40 to 100; 2) if there is no closed by-pass line in the zone under consideration (in other words if all of the by-pass lines of the zone are open), then a flow is established in all of the flushing lines of said zone which corresponds to the synchronicity plus or minus 8%.
摘要翻译：通过SMB装置中的模拟移动床吸附分离进料F的方法包括至少一个用于解吸萃取物中生成的化合物的区域1，用于解吸萃余液中生成的化合物的区域2，用于吸附的区域3 在提取物中产生的化合物，位于萃余液提取和解吸剂供应之间的区域4，该装置包括直接连接两个连续板Pi和Pi + 1的外部旁路管线Li / i + 1; 其中顺序修改限制旁路线Li / i + 1的冲洗流量的装置的打开程度，使得：1）在存在至少一个封闭旁路线的操作区域中，在所考虑的区域内的所有未闭合的旁路线中建立冲洗流速的超同步性，所述超同步性由下式定义：S = a + b（nf / nt）其中常数a为-5至5范围内的常数，b为40至100范围内的常数; 2）如果在所考虑的区域内没有闭路旁路线（换句话说，如果该区域的所有旁路线路都是打开的），则在所述区域的所有冲洗线路中建立流动，对应于同步加或减8％。

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