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1. 发明公开

KR1020030016083A 메틸화 멜라민의 제조방법 有权
标题翻译：甲磺酸的制备
公开(公告)号：KR1020030016083A
公开(公告)日：2003-02-26
申请号：KR1020010049997
申请日：2001-08-20
申请人： 케이피엑스케미칼 주식회사
发明人： 허현 , 이상목 , 송기천 , 김승근 , 이진규
IPC分类号： C07D251/64
摘要： PURPOSE: Provided is a method for preparing methylated melamine with high production rate and purity. The process carries out methoxylation reaction in neutral condition so that the amount of acid used therefor is decreased and the generation of salts and ions is remarkably decreased. CONSTITUTION: The preparation method comprises the steps of: mixing 1 mole of melamine, 3-30 moles of formaldehyde, 10-70 moles of methanol and 0.0001-0.1 mole of metal salt catalyst and performing reaction of the mixture under neutral condition of pH 6.5-7.5; methoxylating the reactant using acid catalyst at pH 3-5; neutralizing the reactant with sodium hydroxide and separating it by thin layer evaporation at 100-150deg.C, under the pressure of not more than 100torr with 200-300rpm and 0.1-1.0 liter/hour flow rate; and eliminating remaining salts and ions in the reactant by adding 0.1-10wt.% of magnesium silicate. At least one of metal salt catalyst is selected from the group consisting of NaCO2CH3, KaCO2CH3, Pb(CO2CH3)2, Mg(CO2CH3)2 and NaOCH3 while one or more acid catalysts are chosen from the group consisting of HCOOH, HCO2CH3, HCl, HNO3, H2SO4 and H3PO4.
摘要翻译：目的：提供高生产率和纯度的甲基化三聚氰胺的制备方法。该方法在中性条件下进行甲氧基化反应，使其使用的酸的量减少，盐和离子的产生显着降低。构成：制备方法包括：混合1摩尔三聚氰胺，3-30摩尔甲醛，10-70摩尔甲醇和0.0001-0.1摩尔金属盐催化剂，并在pH 6.5的中性条件下进行混合物的反应 -7.5; 在pH 3-5下使用酸催化剂对反应物进行甲氧基化; 用氢氧化钠中和反应物，并在100-150℃的薄层蒸发下，在不超过100torr的压力下以200-300rpm和0.1-1.0升/小时流速分离反应物; 并通过加入0.1-10重量％的硅酸镁来消除反应物中剩余的盐和离子。金属盐催化剂中的至少一种选自NaCO 2 CH 3，KaCO 2 CH 3，Pb（CO 2 CH 3）2，Mg（CO 2 CH 3）2和NaOCH 3，而一种或多种酸催化剂选自HCOOH，HCO 2 CH 3，HCl， HNO 3，H 2 SO 4和H 3 PO 4。

2. 发明公开

KR1020070067162A 멜라민 및 알데히드를 포함하는 수성 스트림의 제조 방법 无效
标题翻译：生产包含梅花和阿尔德黑的水质流的方法
公开(公告)号：KR1020070067162A
公开(公告)日：2007-06-27
申请号：KR1020077009090
申请日：2005-09-30
申请人： 디에스엠 아이피 어셋츠 비.브이.
发明人： 위트드노라안나 , 호빙헨드릭덱 , 두이스터스헨리커스안토니우스마리아 , 버슈어헨드리누스마리누스
IPC分类号： C08G12/32 , C07D251/56 , C07D251/64
CPC分类号： C07D251/56 , C07D251/64 , C08G12/32
摘要： Process for the production of an aqueous stream comprising melamine and aldehyde in which a melamine comprising aqueous stream is contacted with an aldehyde comprising stream, the melamine comprising aqueous stream originating from a melamine plant, and process for the production of an aqueous stream comprising melamine, urea and aldehyde in which a melamine comprising aqueous stream and a urea comprising stream are being contacted with an aldehyde comprising stream, the melamine comprising aqueous stream originating from a melamine plant.
摘要翻译：用于生产包含三聚氰胺和醛的水流的方法，其中将含有三聚氰胺的水流与含醛的流体接触，所述三聚氰胺包含源自三聚氰胺植物的水流，以及用于生产含有三聚氰胺的含水流的方法，脲和醛，其中包含含水流的三聚氰胺和包含尿素的物流与含醛的物流接触，所述三聚氰胺包含源自三聚氰胺植物的水流。

3. 发明授权

KR100449883B1 메틸화 멜라민의 제조방법 有权
标题翻译： 메틸화멜라민의제조방법
公开(公告)号：KR100449883B1
公开(公告)日：2004-09-22
申请号：KR1020010049997
申请日：2001-08-20
申请人： 케이피엑스케미칼 주식회사
发明人： 허현 , 이상목 , 송기천 , 김승근 , 이진규
IPC分类号： C07D251/64
摘要： PURPOSE: Provided is a method for preparing methylated melamine with high production rate and purity. The process carries out methoxylation reaction in neutral condition so that the amount of acid used therefor is decreased and the generation of salts and ions is remarkably decreased. CONSTITUTION: The preparation method comprises the steps of: mixing 1 mole of melamine, 3-30 moles of formaldehyde, 10-70 moles of methanol and 0.0001-0.1 mole of metal salt catalyst and performing reaction of the mixture under neutral condition of pH 6.5-7.5; methoxylating the reactant using acid catalyst at pH 3-5; neutralizing the reactant with sodium hydroxide and separating it by thin layer evaporation at 100-150deg.C, under the pressure of not more than 100torr with 200-300rpm and 0.1-1.0 liter/hour flow rate; and eliminating remaining salts and ions in the reactant by adding 0.1-10wt.% of magnesium silicate. At least one of metal salt catalyst is selected from the group consisting of NaCO2CH3, KaCO2CH3, Pb(CO2CH3)2, Mg(CO2CH3)2 and NaOCH3 while one or more acid catalysts are chosen from the group consisting of HCOOH, HCO2CH3, HCl, HNO3, H2SO4 and H3PO4.
摘要翻译：目的：提供一种高产率和高纯度的甲基化三聚氰胺的制备方法。该方法在中性条件下进行甲氧基化反应，使得其用量减少，并且盐和离子的生成显着降低。构成：制备方法包括以下步骤：将1摩尔三聚氰胺，3-30摩尔甲醛，10-70摩尔甲醇和0.0001-0.1摩尔金属盐催化剂混合，并在pH6.5的中性条件下进行混合物的反应 -7.5; 在pH 3-5下使用酸催化剂使反应物甲氧基化; 用氢氧化钠中和反应物并在100-150℃，在不超过100torr的压力下，以200-300rpm和0.1-1.0升/小时流速薄层蒸发分离; 并通过加入0.1-10wt。％的硅酸镁来消除反应物中残留的盐和离子。至少一种金属盐催化剂选自NaCO 2 CH 3，KaCO 2 CH 3，Pb（CO 2 CH 3）2，Mg（CO 2 CH 3）2和NaOCH 3，而一种或多种酸催化剂选自HCOOH，HCO 2 CH 3，HCl， HNO3，H2SO4和H3PO4。

4. 发明授权

KR101119431B1 고도로 메틸올화된 멜라민 및 에테르화된 멜라민포름알데히드 수지의 연속 제조 방법 有权
标题翻译：连续生产高含量甲基丙烯酸甲酯和乙烯甲醛甲醛树脂的方法
公开(公告)号：KR101119431B1
公开(公告)日：2012-02-22
申请号：KR1020067016354
申请日：2005-01-13
申请人： 바스프 에스이
发明人： 히팅거,크리스텔 , 슈나이더,조르그 , 슈에르,군터 , 라이프,마틴 , 로베르뜨,알랭 , 슈프,한스 , 에이츠펠터,안드레아스 , 에르하르트,라이너 , 히르쉬,스테판
IPC分类号： C08G12/38 , C07D251/64 , C08G12/00
CPC分类号： C07D251/64
摘要： 본 발명은 폴리메틸올화 멜라민, 및 알칸올로 폴리에테르화된 폴리메틸올화 멜라민 화합물을 제조하는 방법에 관한 것으로서, 메틸올화 반응은 혼련 반응기 내에서 수행한다.

5. 发明公开

KR1020060125856A 고도로 메틸올화된 멜라민 및 에테르화된 멜라민포름알데히드 수지의 연속 제조 방법 有权
标题翻译：连续生产高含量甲基丙烯酸甲酯和乙烯甲醛甲醛树脂的方法
公开(公告)号：KR1020060125856A
公开(公告)日：2006-12-06
申请号：KR1020067016354
申请日：2005-01-13
申请人： 바스프 에스이
发明人： 히팅거,크리스텔 , 슈나이더,조르그 , 슈에르,군터 , 라이프,마틴 , 로베르뜨,알랭 , 슈프,한스 , 에이츠펠터,안드레아스 , 에르하르트,라이너 , 히르쉬,스테판
IPC分类号： C08G12/38 , C07D251/64 , C08G12/00
CPC分类号： C07D251/64
摘要： The invention relates to a method for producing polymethylolated melamine and polymethylolated melamine compounds that are polyetherified with alkanol, the methylolation reaction being carried out in a mixing reactor.
摘要翻译：本发明涉及一种与链烷醇多乙酰化的多羟甲基化三聚氰胺和多羟甲基化三聚氰胺化合物的制备方法，所述羟甲基化反应在混合反应器中进行。

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