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1. 发明授权

KR100777261B1 아미드와 에스테르 리간드를 가지는 윤활제용 몰리브데늄착화합물의 제조 有权
标题翻译：用酰胺或硫酸酯配方作为润滑剂制备莫来石复合物
公开(公告)号：KR100777261B1
公开(公告)日：2007-11-28
申请号：KR1020060047436
申请日：2006-05-26
申请人： 장암칼스 주식회사
发明人： 조원오 , 황광진 , 윤혁채
IPC分类号： C07F11/00 , C10M133/00
CPC分类号： C07F11/00 , C10M139/06
摘要： A method for preparing a molybdenum complex is provided to obtain the molybdenum complex having an amide and an ester-based ligands as an additive for improving the physical properties of a lubricating oil. A method for preparing a molybdenum complex comprises the steps of: (a) adding a fatty acid such as oleic acid, castor oil, rape oil, coconut oil and tollow oil and diethanolamine and agitating it at a temperature of 130-140 deg.C for 3-5 hours to obtain an amide compound, wherein the reaction in each step is performed on base oil; and (b) after mixing glycerol monostearate(GMS) with the amide compound obtained from the step(a), mixing an aqueous solution of ammonium heptamolybdate therewith, wherein the molar ratio of the glycerol monostearate and the ammonium heptamolybdate is 1:0.009-0.01.
摘要翻译：提供了一种制备钼络合物的方法，以获得具有酰胺和酯基配位体的钼络合物作为用于改善润滑油的物理性质的添加剂。制备钼络合物的方法包括以下步骤：（a）加入脂肪酸如油酸，蓖麻油，油菜籽油，椰子油和底油和二乙醇胺，并在130-140℃的温度下搅拌进行3-5小时以获得酰胺化合物，其中每个步骤中的反应在基础油上进行; 和（b）在将甘油单硬脂酸酯（GMS）与由步骤（a）获得的酰胺化合物混合后，将七钼酸铵的水溶液与其混合，其中甘油单硬脂酸酯和七钼酸铵的摩尔比为1:0.009-0.01 。

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