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1. 发明授权

KR100397621B1 카페트용 폴리(트리메틸렌 테레프탈레이트) ＢＣＦ이형단면사 失效
标题翻译： 카페트용폴리（트리메틸렌테레이이트）BCF이형단면사
公开(公告)号：KR100397621B1
公开(公告)日：2003-09-13
申请号：KR1020010026146
申请日：2001-05-14
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬 , 이종복
IPC分类号： D01D5/253
CPC分类号： D02G1/20 , D01D5/253 , D01F6/62 , D02G3/445 , Y10T428/23957 , Y10T428/29 , Y10T428/2909 , Y10T428/2913 , Y10T428/2973
摘要： Disclosed is a poly(trimethylene terephthalate) BCF carpet modified cross-section yarn having an modification ratio and a arm angle within a specific range and a Y-shaped cross-section, and a method for preparing it. The BCF modified cross-section yarn has excellent bulk property and spinning efficiency, and a carpet made from the BCF modified cross-section yarn has good appearance, sense of touch, and tufting efficiency.
摘要翻译：本发明公开了具有特定范围和Y形截面的改性比和臂角的聚对苯二甲酸1,3-丙二醇酯BCF地毯改性截面纱及其制备方法。 BCF改性截面纱具有优异的整体性和纺丝效率，由BCF改性截面纱制成的地毯具有良好的外观，触感和簇绒效率。

2. 发明授权

KR100347328B1 폴리트리메틸렌테레프탈레이트 벌키 연속 필라멘트의제조방법 失效
标题翻译：生产聚对苯二甲酸丙二醇酯膨松连续长丝的方法
公开(公告)号：KR100347328B1
公开(公告)日：2002-08-07
申请号：KR1020000060078
申请日：2000-10-12
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬 , 김균호
IPC分类号： D01D5/08
摘要： 본 발명은 폴리트리메틸렌테레프탈레이트 벌키 연속 필라멘트를 제조함에 있어서, 용융 폴리트리메틸렌테프탈레이트를, Y단면형이며 60홀 이상이고 이형도가 1.8∼2.5로 설계된 노즐을 통하여, 245∼285℃의 방사온도 및 1800∼3000m/min의 방사속도로 용융방사하고 방사된 필라멘트는 유제부여, 연신 및 권축과정을 거친 후, 별도로 분리된 집속장치에 의해 15∼20회/m의 단위로 집속을 주는 것을 특징으로 하는 폴리트리메틸렌테레프탈레이트 벌키 연속 필라멘트의 제조방법에 관한 것으로, 본 발명에 의해 물성이 균일하고 방사작업성 및 컷팅성 등이 우수한 폴리트리메틸렌테레프탈레이트 벌키 연속 필라멘트를 제공할 수 있다.

3. 发明公开

KR1020020053935A 피티티를 사용한 비씨에프의 제조방법 失效
标题翻译：使用聚（三甲苯三烯酸）生产稠密连续薄膜
公开(公告)号：KR1020020053935A
公开(公告)日：2002-07-06
申请号：KR1020000081914
申请日：2000-12-26
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬
IPC分类号： D01F6/62
摘要： PURPOSE: A process of preparing bulked continuous filaments capable of reducing streak and increasing spinning workability using poly(trimethylene terephthalate) is provided. By the use of the filament, carpets having extended service life and increased light fastness are produced. CONSTITUTION: A master batch added with 0.1 to 1.0% by weight of a phosphorous-based stabilizer of formula 1 is blended, based on 100 parts by weight of poly(trimethylene terephthalate) base chips. In formula, R1, R2, R3 are a phenyl group, C5-20 alkyl and a combination of a phenyl group attached with a substituted group. The phosphorous-based stabilizer is diphenyloxylphosphite, diphenyldecylphosphite, tri 2,4-di-tert-butylphosphite.
摘要翻译：目的：提供一种使用聚（对苯二甲酸丙二醇酯）制备能够降低条纹并提高纺丝加工性的膨体连续长丝的方法。通过使用长丝，产生延长使用寿命和增加耐光性的地毯。构成：基于100重量份的聚（对苯二甲酸丙二醇酯）基础芯片，共混添加0.1-1.0重量％的式1的磷基稳定剂的母料。在式中，R 1，R 2，R 3为苯基，C 5-20烷基和与取代基连接的苯基的组合。磷系稳定剂为亚苯基亚苯基亚磷酸酯，亚磷酸二苯基癸酯，亚磷酸三（2,4-二叔丁基酯）酯。

4. 发明授权

KR100397620B1 폴리(트리메틸렌 테레프탈레이트) 카페트의 제조방법 失效
标题翻译： 폴리（트리메틸렌테레이레이트）카페트의제조방폴
公开(公告)号：KR100397620B1
公开(公告)日：2003-09-13
申请号：KR1020010026144
申请日：2001-05-14
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬 , 이종복
IPC分类号： D01D5/22
CPC分类号： D01F6/62 , D01D5/253 , D02G3/445 , D06N7/0068 , D06N7/0073 , D06N7/0081 , D06N2201/02 , D06N2201/0254 , D06N2201/042 , D06N2205/20 , D06N2207/04 , D06N2209/0823 , D06N2209/083 , D06N2209/147 , D06N2209/1685 , Y10T428/23993
摘要： Disclosed is a method for preparing a poly(trimethylene terephthalate) carpet, in which the poly(trimethylene terephthalate) carpet is prepared from poly(trimethylene terephthalate) yarns through the post-processes comprising cabling, heat setting, tufting, dyeing, becking, and shearing. The poly(trimethylene terephthalate) yarns have advantages of improved quality, functionality, and workability by optimizing operating conditions of the steps.
摘要翻译：本发明公开了一种制备聚对苯二甲酸1,3-丙二醇酯地毯的方法，其中聚对苯二甲酸1,3-丙二醇酯地毯由聚对苯二甲酸丙二醇酯纱线通过包括布线，热定型，簇绒，染色，夹持和剪切。通过优化步骤的操作条件，聚（对苯二甲酸丙二醇酯）纱具有改善的质量，功能性和可加工性的优点。

5. 发明公开

KR1020020087159A 폴리(트리메틸렌 테레프탈레이트) 카페트의 제조방법 失效
标题翻译：聚（三甲苯三烯酸）地毯的制造方法
公开(公告)号：KR1020020087159A
公开(公告)日：2002-11-22
申请号：KR1020010026144
申请日：2001-05-14
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬 , 이종복
IPC分类号： D01D5/22
CPC分类号： D01F6/62 , D01D5/253 , D02G3/445 , D06N7/0068 , D06N7/0073 , D06N7/0081 , D06N2201/02 , D06N2201/0254 , D06N2201/042 , D06N2205/20 , D06N2207/04 , D06N2209/0823 , D06N2209/083 , D06N2209/147 , D06N2209/1685 , Y10T428/23993
摘要： PURPOSE: Provided is a manufacturing method of a poly(trimethylene terephthalate) carpet having beautiful appearance, excellent touch, abrasion resistance, elastic recovering ratio, excellent anti-fouling property, excellent antistatic property, excellent exfoliating strength, excellent pulling strength and excellent shape stability. CONSTITUTION: The poly(trimethylene terephthalate) carpet is obtained by a process containing the steps of: (s1) cabling; (s2) heat-setting with a superba at 120-160deg.C of temperature on a main tunnel at 4-9m/min of band speed on 200-240g/m of density; (s3) tufting to make 5-15/inch of stitch; (s4) beck-dyeing the tufted carpet with disperse dyes at normal pressure at 90-100deg.C of temperature without carrier; (s5) backing the dyed carpet; and then (s6) shearing.
摘要翻译：目的：提供具有美观，触感，耐磨性，弹性回复率，优异的抗结垢性，优异的抗静电性，优异的剥离强度，优异的拉伸强度和优异的形状稳定性的聚（对苯二甲酸丙二醇酯）地毯的制造方法。构成：通过包括以下步骤的方法获得聚（对苯二甲酸丙二醇酯）地毯：（s1）布线; （s2）以200-240g / m密度，以主干隧道的温度为120-160℃，以4-9m / min的速度进行热定型; （s3）簇绒制作5-15英寸针迹; （s4）使用分散染料在90-100℃的温度下在常压下对簇绒地毯进行染色，无载体; （s5）支持染色地毯; 然后（s6）剪切。

6. 发明公开

KR1020030055471A 난연성 폴리트리메틸렌 테레프탈레이트 벌키 연속필라멘트의 제조방법 失效
标题翻译：具有火焰延迟性的聚对苯二甲酸十二烷基酯连续纤维的制备方法
公开(公告)号：KR1020030055471A
公开(公告)日：2003-07-04
申请号：KR1020010085024
申请日：2001-12-26
申请人： 주식회사 효성
发明人： 최영찬 , 이귤섭 , 이종복
IPC分类号： D01F6/62
摘要： PURPOSE: A manufacturing method of polytrimethylene terephthalate bulky continuous filament having fire retardancy and excellent fastness is characterized by containing a phosphoric flame retardant and using a blending spinning method. The polytrimethylene terephthalate bulky continuous filament is useful for a carpet and a car mat. CONSTITUTION: The manufacturing method thereof is characterized by: using polytrimethylene terephthalate as main polymer; adding 5-20wt.% of master batch of the phosphoric flame retardant(a formula 1) through a first side supplying device; using PTT or PET as a carrier; adding 2-5wt.% of dope dyed master batch through a second side supplying device; and then blending-spinning the polymer. In the formula 1, R1 and R2 are radicals containing each hydrogen or C2-C4 of ¥ø-hydroxyl; and n is an integer of 1-5.
摘要翻译：目的：具有阻燃性和优异坚牢度的聚对苯二甲酸亚乙基对苯二甲酸丁二醇酯体积连续长丝的制造方法的特征在于含有磷阻燃剂并使用共混纺丝法。聚对苯二甲酸丙二醇酯体积大的连续长丝可用于地毯和汽车垫。构成：其制造方法的特征在于：使用聚对苯二甲酸丙二醇酯作为主要聚合物; 通过第一侧供应装置加入5-20重量％的母料磷酸阻燃剂（式1）; 使用PTT或PET作为载体; 通过第二侧供应装置加入2-5重量％的染料母料; 然后混合纺丝聚合物。在式1中，R 1和R 2是含有每个氢或C 1〜C羟基的C 2 -C 4的基团; n为1-5的整数。

7. 发明公开

KR1020020087161A 카페트용 폴리(트리메틸렌 테레프탈레이트) ＢＣＦ이형단면사 失效
标题翻译：聚（三甲基孕酮）BCF改性交叉纤维片
公开(公告)号：KR1020020087161A
公开(公告)日：2002-11-22
申请号：KR1020010026146
申请日：2001-05-14
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬 , 이종복
IPC分类号： D01D5/253
CPC分类号： D02G1/20 , D01D5/253 , D01F6/62 , D02G3/445 , Y10T428/23957 , Y10T428/29 , Y10T428/2909 , Y10T428/2913 , Y10T428/2973
摘要： PURPOSE: Provided is poly(trimethylene terephthalate) BCF modified cross-section fiber for a carpet which is characterized by having uniform physical properties, excellent bulking ability and spinning workability, improving the carpet in quality, and making it possible to produce the carpet having excellent elastic recovering property, beautiful appearance, touch, abrasion resistance, anti-fouling property and antistatic property. CONSTITUTION: The poly(trimethylene terephthalate) BCF modified cross-section fiber is characterized by having "Y" type cross-section and having a shaped ratio and an arm angle being in a range of a parallelogram ABCD of a graph. The poly(trimethylene terephthalate) BCF modified cross-section fiber is obtained by a process containing the steps of: using poly(trimethylene terephthalate) having 0.8-1.2 of inherent viscosity and under 50ppm of moisture; adding 2-5% of color master batch based on base chip quantity; melt-spinning at 1500-4000m/min of speed; drawing; passing through a texturing nozzle(8) to give 10-60% of crimp ratio; and then passing through a confounding device(11) to make 10-45numbers/m of knots.
摘要翻译：目的：提供用于地毯的聚（对苯二甲酸丙二醇酯）BCF改性横截面纤维，其特征在于具有均匀的物理性能，优异的填充能力和纺丝加工性，改善了地毯的质量，并且使得可以生产具有优异的地毯弹性回复性，外观美观，触感，耐磨性，防污性和抗静电性。构成：聚对苯二甲酸丙二醇酯BCF改性横截面纤维的特征在于具有“Y”型横截面并具有成形比和臂角在图的平行四边形ABCD的范围内。通过包括以下步骤的方法获得聚（对苯二甲酸丙二醇酯）BCF改性横截面纤维：使用具有0.8-1.2的特性粘度和低于50ppm水分的聚对苯二甲酸丙二醇酯; 基于芯片数量添加2-5％的色母粒; 以1500-4000m / min的速度熔融纺丝; 画画; 通过变形喷嘴（8），得到10-60％的卷曲率; 然后通过混合装置（11），使结构为10-45numbers / m。

8. 发明公开

KR1020020059023A 폴리트리메틸렌테레프탈레이트 비씨에프사의 제조방법 无效
标题翻译：聚对苯二甲酸乙二醇酯连续纤维纱的制造方法
公开(公告)号：KR1020020059023A
公开(公告)日：2002-07-12
申请号：KR1020000087180
申请日：2000-12-30
申请人： 주식회사 효성
发明人： 최영찬
IPC分类号： D01F6/62
摘要： PURPOSE: A manufacturing method of polytrimethylene terephthalate bulked continuous filament(BCF) yarn is provided which has excellent stability against ultraviolet, decreases dissipation rate of tenacity, reduces defective proportion of streak, reduces deviation of chemical and physical properties such as viscosity and strength, improves spinning workability and makes it possible to lengthen the expected life span of the final carpet. CONSTITUTION: The polytrimethylene terephthalate BCF yarn is obtained by a process containing the steps of: mixing 0.1-1.0pts.wt. of phosphorus type stabilizer of formula based on 100pts.wt. of PTT base chip to produce master batch; mixing the master batch with the PTT base chip; and then melt-spinning. In formula, R1, R2 and R3 are phenyl group, C5-C20 alkyl group or phenyl bonded substituent.
摘要翻译：目的：提供聚对苯二甲酸丁二醇酯膨胀连续长丝（BCF）的制造方法，其对紫外线具有优异的稳定性，降低强度的耗散率，减少条纹的有缺陷的比例，减少化学和物理性质如粘度和强度的偏差，改善纺纱可加工性，并且可以延长最终地毯的预期寿命。组成：聚对苯二甲酸丙二醇酯BCF纱线是通过包括以下步骤的方法获得的：将0.1-1.0pts.wt 的磷型稳定剂，基于100pts.wt。的PTT基片生产母料; 将母料与PTT基片混合; 然后熔融纺丝。在式中，R 1，R 2和R 3为苯基，C 5 -C 20烷基或苯基取代基。

9. 发明公开

KR1020010045416A 폴리에스테르 중축합 장치의 에스테르화 반응장치 失效
标题翻译：聚酯聚合装置的制备装置
公开(公告)号：KR1020010045416A
公开(公告)日：2001-06-05
申请号：KR1019990048697
申请日：1999-11-04
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬
IPC分类号： C08G63/78
摘要： PURPOSE: Provided is an esterification device of a polyester polycondensation apparatus, which maintains an amount of water contained in ethyleneglycol and produces polyester oligomer having a high esterification rate, a high average degree of polymerization, and a small change of DEG content. CONSTITUTION: The esterification device, which is a loop reactor type of a thermal syphon method, comprises a DE heater(1), a DE evaporator(2), a rectifying column(3), a condenser(4), an on-line concentration measuring instrument(5), and an electric heater(6) to maintain the amount of water contained in the ethyleneglycol, wherein the on-line concentration measuring instrument(5) and the electric heater(6) are mounted in a transfer line between the rectifying column(3) and the lower part of the DE heater(1).
摘要翻译：目的：提供一种聚酯缩聚装置的酯化装置，其保持乙二醇中所含的水量，并生成具有高酯化速率，高平均聚合度和DEG含量变化小的聚酯低聚物。构成：作为环形反应器型的热虹吸法的酯化装置包括DE加热器（1），DE蒸发器（2），精馏塔（3），冷凝器（4），在线浓度测量仪器（5）和电加热器（6），用于将在线浓度测量仪器（5）和电加热器（6）中安装的乙二醇中所含的水量保持在传输线之间精馏塔（3）和DE加热器（1）的下部。

10. 发明授权

KR100523812B1 피티티를 사용한 비씨에프의 제조방법 失效
标题翻译：聚对苯二甲酸丁二醇酯生产连续丝的制造方法
公开(公告)号：KR100523812B1
公开(公告)日：2005-10-25
申请号：KR1020000081914
申请日：2000-12-26
申请人： 주식회사 효성
发明人： 이귤섭 , 최영찬
IPC分类号： D01F6/62
摘要： 본 발명은 폴리트리메틸렌텔레프탈레이트(PTT)를 사용한 Bulked continuous filament(BCF)의 제조방법에 관한 것으로, PTT Base chip 100중량부에 대하여 0.1∼1.0 중량부의 인(P)계 안정제, 더욱 상세하게는 가수분해에 탁월한 프로세싱 안정제역활을 하는 페닐, 알킬 포스파이트를 사용해 마스터배치를 제조한후 이를 PTT Base chip대 마스터배치의 feeding비율을 100:0.5∼2로 하여 Blending 방사하므로 최종제품인 카페트용 BCF를 제조하는 방법으로, Cop간의 물성이 균일하여 streak 불량율을 줄일 수 있고 방사작업성을 높일 수 있으며, 기존 PTT 수지로만 방사한 BCF에 비해 자외선에 대한 안정성이 높아져 카페트의 수명을 늘릴 뿐만 아니라 고품위를 장기간 유지시킬 수 있도록 한다.

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