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1. 发明公开

KR1020060097002A 메틸아민 제조 중의 반응기 유입 온도 조절 방법 无效
标题翻译：控制甲基胺生产过程中反应器进入温度的方法
公开(公告)号：KR1020060097002A
公开(公告)日：2006-09-13
申请号：KR1020067005760
申请日：2004-09-24
申请人： 바스프 에스이
发明人： 로이트만,베르너 , 밤프스간스,롤프 , 포플로프,프랑크 , 베버,테오도르 , 로스,칼-하인즈 , 율리우스,만프레드
IPC分类号： C07C209/14 , C07C211/04
CPC分类号： C07C209/16 , C07C211/04
摘要： The invention relates to a method for the production of metylamines by means of gas phase reaction from methanol and ammonia as educts in the presence of a heterogeneous catalyst at a pressure in the region of 15 - 30 bars. Said educts are vaporised in one or several heat exchangers (1, 2, 3) in order to overheat an educt gas flow and are subsequently guided to a reactor (4). The educts can be mixed in the inlets of one of the heat exchangers (1, 2, 3) or at one remaining position in a heat exchanger (1, 2, 3). A product gas flow containing monomethylamine, dimethylamine and trimethylamine, in addition to reaction auxiliary products, is removed from the reactor (4). In order to regulate the reactor admission temperature of the educts to a temperature in the region of 360 °C - 370 °C, the educt gas flow or the product gas flow is guided partially or completely through an adjustable valve (5) enabling the pressure and the condensation temperature to be varied.
摘要翻译：本发明涉及一种在非均相催化剂存在下，在15-30巴的压力下，通过甲醇和氨的气相反应生产甲胺的方法。所述排出物在一个或多个热交换器（1,2,3）中蒸发，以便使过渡气体流过热并随后被引导至反应器（4）。排出口可以在热交换器（1,2,3）的一个入口处或在热交换器（1,2,3）中的一个剩余位置处混合。从反应器（4）除去含有一甲胺，二甲胺和三甲胺的产物气流，以及反应助剂。为了将出口的反应器入口温度调节到360℃至370℃的温度，通过可调节阀（5）部分或完全地引导排气流或产物气流，使压力并且冷凝温度要变化。

2. 发明授权

KR101140055B1 부식의 회피방법 有权
标题翻译：避免腐蚀的方法
公开(公告)号：KR101140055B1
公开(公告)日：2012-05-02
申请号：KR1020067005742
申请日：2004-09-24
申请人： 바스프 에스이
发明人： 로이트만,베르너 , 베버,테오도르 , 로스,칼-하인즈 , 율리우스,만프레드
IPC分类号： C07C209/86 , C07C211/04
CPC分类号： C07C211/04 , C07C209/86 , Y10S203/20 , Y10S203/24
摘要： 제1 컬럼(1)에서 순수 증류에 의해 암모니아(11)를 분리-제거하고,
기저 부분(12)으로서 수득된 생성물 스트림의 잔류 성분을 제2 컬럼(2)으로 공급하고,
트리메틸아민(14)를 물을 도입하면서 추출 증류에 의해 제2 컬럼(2)에 분리-제거하고,
제2 컬럼(2)으로부터 기저 부분(15)으로 수득된 생성물 스트림의 추가 성분을 제3 컬럼(3)에 공급하고,
모노메틸아민과 디메틸아민을 제3 컬럼(3)에서 분리-제거하고,
상기 모노메틸아민과 디메틸아민을 제4 컬럼(4)에서 증류에 의해 분리하는 것
을 포함하며, 여기서 알칼리 금속 히드록사이드가 제2 컬럼 또는 제3 컬럼(3)에 첨가되는 것인,
메탄올과 암모니아의 기상 반응에 의한 메틸아민의 제조반응에서 수득되는 생성물 스트림(10)으로부터 메틸아민을 분리하는데에 있어서 부식을 회피하는 방법에 관한 것이다.
메틸아민, 부식회피 방법, 알칼리 금속 히드록사이드, 증류, 컬럼

3. 发明公开

KR1020060081709A 부식의 회피방법 有权
标题翻译：避免腐蚀的方法
公开(公告)号：KR1020060081709A
公开(公告)日：2006-07-13
申请号：KR1020067005742
申请日：2004-09-24
申请人： 바스프 에스이
发明人： 로이트만,베르너 , 베버,테오도르 , 로스,칼-하인즈 , 율리우스,만프레드
IPC分类号： C07C209/86 , C07C211/04
CPC分类号： C07C211/04 , C07C209/86 , Y10S203/20 , Y10S203/24
摘要： The invention relates to a method for avoiding corrosion on the separation of methylamine from a product stream (10) with the components monomethylamine, dimethylamine, trimethylamine, ammonia and methanol, arising during the production of methylamine by the gas phase reaction of methanol and ammonia, whereby ammonia is separated off in a first column (1), by simple distillation and the bottom components of the product stream remaining in the kettle (12) are fed to a second column (2). Trimethylamine (14) is separated off in the second column (2), by means of extractive distillation with addition of water. The further components of the product stream remaining in the kettle (15) of the second column (2) are introduced into a third column (3), in which monomethylamine and dimethylamine are separated off through the head. The monomethylamine and dimethylamine are separated in a fourth column (4) by distillation. In order to avoid corrosion, alkaline hydroxide is added to the second or third column (3).
摘要翻译：本发明涉及一种避免甲胺从甲醇和氨气相反应生成甲胺生成的产物流（10）与甲胺，二甲胺，三甲胺，氨和甲醇成分分离的方法，由此通过简单蒸馏在第一塔（1）中分离出氨，并将残留在釜（12）中的产物流的底部组分进料至第二塔（2）。在第二塔（2）中通过萃取蒸馏除去三甲胺（14）。残留在第二塔（2）的釜（15）中的产物流的其它组分被引入第三塔（3）中，其中一甲胺和二甲胺通过头分离。通过蒸馏在第四塔（4）中分离单甲胺和二甲胺。为了避免腐蚀，将碱性氢氧化物加入到第二或第三塔（3）中。

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