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51. 发明授权

KR100791955B1 안정한 1,2-벤즈이소티아졸린-3-온 액상 조성물과 이의제조방법 有权
标题翻译：稳定的1,2-苯并异噻唑啉-3-酮的液体组合物及其制备方法
公开(公告)号：KR100791955B1
公开(公告)日：2008-01-04
申请号：KR1020020048072
申请日：2002-08-14
申请人： 에스케이케미칼주식회사
发明人： 박기만 , 박정호 , 김진만 , 하재민
IPC分类号： A61K31/425
摘要： 본 발명은 안정한 1,2-벤즈이소티아졸린-3-온 액상 조성물과 이의 제조방법에 관한 것으로서, 더욱 상세하세는 다음 화학식 1로 표시되는 1,2-벤즈이소티아졸린-3-온에 알카리 금속염, 히드록시 유기용매 및 물을 혼합한 후 활성탄을 이용하여 불순물을 제거함으로써 색도가 개선되고 안정성이 우수한 1,2-벤즈이소티아졸린-3-온 액상 조성물 및 이를 대량 생산하는데 유용한 제조방법에 관한 것이다.

1,2-벤즈이소티아졸린-3-온, 히드록시 유기용매, 활성탄

52. 发明授权

KR100791931B1 디이모늄염 및 이를 포함하는 근적외선 흡수필름 有权
标题翻译：二盐酸盐和近红外辐射吸收膜
公开(公告)号：KR100791931B1
公开(公告)日：2008-01-04
申请号：KR1020060085529
申请日：2006-09-06
申请人： 에스케이케미칼주식회사
发明人： 이민혁 , 강주식 , 박정호 , 이성용
IPC分类号： C07C251/24 , C07C255/24
CPC分类号： C07F9/28 , C07C251/30
摘要： A diimmonium salt is provided to obtain a near infrared ray absorbing film having excellent durability against light, heat and water, non-harmful to the human body, and showing excellent absorbance in the near infrared region. A diimmonium salt for a near infrared ray absorbing film is represented by the following formula 1. In formula 1, n is an integer of 1-2; each of R1-R8 independently represents a substituted or non-substituted C1-C10 linear or branched alkyl, wherein the substituent is cyano, nitro, carboxy, sulfone, halogen, hydroxy, C1-C8 alkoxy, alkoxyalkoxy, acyloxy, alkylamino, C6-C18 aryl or aryloxy; X- is a substituted fluoroalkyl phosphate anion represented by the following formula 2. In formula 2, x is 0 or 1; y is an integer of 1-3; z is an integer of 6-y; and each of R9-R13 independently represents H or F, with the proviso that at least one of R9-R13 is F.
摘要翻译：提供了一种二亚铵盐，以获得对人体无害的对光，热和水的耐久性优良的近红外线吸收膜，并且在近红外区域显示出优异的吸光度。用于近红外线吸收膜的二亚铵盐由下式1表示。在式1中，n为1-2的整数; 硝基，羧基，砜，卤素，羟基，C 1 -C 8烷氧基，烷氧基烷氧基，酰氧基，烷基氨基，C 6 -C 10芳基， C18芳基或芳氧基; X-是由下式2表示的取代的氟烷基磷酸根阴离子。在式2中，x是0或1; y为1-3的整数; z是6-y的整数; 并且R 9 -R 13各自独立地表示H或F，条件是R 9 -R 13中的至少一个为F.

53. 发明公开

KR1020070070986A 디이모늄염 올리고머, 이의 제조방법 및 용도 有权
标题翻译：二盐酸盐低聚物，其制备方法及其用途
公开(公告)号：KR1020070070986A
公开(公告)日：2007-07-04
申请号：KR1020050134076
申请日：2005-12-29
申请人： 에스케이케미칼주식회사
发明人： 박정호 , 이민혁 , 강주식
IPC分类号： C07C251/24
摘要： Provided are a diimonium oligomer which is improved in the absorption of near infrared ray(NIR) and is excellent in the compatibility with a binder, a method for preparing the diimonium oligomer, and a NIR absorbing dye containing the diimonium oligomer. The diimonium oligomer is represented by the formula(1), wherein R1 is a C3-C10 linear or branched alkyl group; R2 is a C1-C10 linear or branched alkyl group; Z is a dialkylsulfonyl imido group wherein the hydrogen atom of a C1-C10 alkyl group is substituted with a halogen atom, or a dialkylsulfonyl imido group; l is 1 or 2; and m is an integer of 2-10. The method comprises the steps of reacting an amine compound of the formula(2), an alkyl halogenide compound represented by R2-X and an alkyl dihalogenide compound represented by X'-R1-X'' to prepare an amine oligomer of the formula(5); and oxidizing the amine oligomer with an oxidizing agent, wherein X, X' and X'' are Cl, Br, F or I independently.
摘要翻译：提供了近红外线（NIR）的吸收性提高的二亚铵低聚物，与粘合剂的相容性优异，二亚铵低聚物的制造方法和含有二亚铵低聚物的NIR吸收性染料。二咪唑低聚物由式（1）表示，其中R1是C3-C10直链或支链烷基; R2是C1-C10直链或支链烷基; Z是C1-C10烷基的氢原子被卤素原子或二烷基磺酰基亚氨基取代的二烷基磺酰亚胺基; l为1或2; m为2-10的整数。该方法包括使式（2）的胺化合物，由R2-X表示的烷基卤化物化合物和由X'-R1-X“表示的烷基二卤化物化合物反应以制备下式的胺低聚物 5）; 并用氧化剂氧化胺低聚物，其中X，X'和X“独立地为Cl，Br，F或I。

54. 发明授权

KR100703997B1 이소티아졸론 조성물과 안정화 방법, 및 이를 이용하는미생물의 생장 억제방법 有权
标题翻译：异噻唑酮组合物和稳定化方法，以及使用它们抑制微生物生长的方法
公开(公告)号：KR100703997B1
公开(公告)日：2007-04-04
申请号：KR1020010024989
申请日：2001-05-08
申请人： 에스케이케미칼주식회사
发明人： 홍완표 , 김진만 , 최기승 , 박정호 , 하재민 , 정희원 , 한순종
IPC分类号： A01N25/22
摘要： 본 발명은 이소티아졸론 조성물과 안정화 방법, 및 이를 이용하는 미생물의 생장 억제방법에 관한 것으로서, 보다 상세하게는 (a) 3-이소티아졸론 화합물; (b) 금속 질산염; (c) 염화마그네슘; (d) 요오드산, 과요오드산, 요오드산 염, 과요오드산염, 또는 이들의 혼합물; (e) 금속브롬산염; 및 (f) 용매를 포함하는 이소티아졸론 조성물과 안정화 방법, 및 이를 이용하는 미생물의 생장 억제방법을 제공하여 이소티아졸론 용액의 제조공정 중에 생성된 부산물 및 보관 중에 생성된 화합물에 의한 침전의 발생을 효과적으로 억제할 수 있다.
이소티아졸론, 금속질산염, 염화마그네슘, 침전형성 방지제, 요오드산, 과요오드산, 요오드산염, 과요오드산염, 금속브롬산염, 안정화, 살균제
摘要翻译：本发明异噻唑酮组合物和稳定化方法，以及涉及一种用于使用相同的，更特别是（一）3-异噻唑酮化合物抑制微生物生长; （b）金属硝酸盐; （c）氯化镁; （d）碘酸，高碘酸，碘酸，高碘酸或其混合物; （e）金属溴酸盐; 和（f）与所述稳定化方法的异噻唑酮组合物中，和沉淀的由于所得到的化合物在副产物的产生，并在异噻唑酮溶液，以提供使用相同的抑制微生物，包含溶剂的生长方法的制造过程中保持产生的可以有效抑制。

55. 发明公开

KR1020040093502A Ｎ,Ｎ'-디치환-3,3'-디티오프로피온아미드의 제조방법 有权
标题翻译：生产N，N'-分离的3,3'-二羟基磷酰胺的方法，其预防有机硫化合物的不必要的过氧化
公开(公告)号：KR1020040093502A
公开(公告)日：2004-11-06
申请号：KR1020030027372
申请日：2003-04-30
申请人： 에스케이케미칼주식회사
发明人： 하재민 , 김진만 , 박기만 , 박정호 , 한순종
IPC分类号： C07C319/24
摘要： PURPOSE: A process is provided to produce N,N'-disubstituted-3,3'-dithiopropionamide in high yield and high purity, which prevents unnecessary peroxidation of an organic sulfur compound, controls oxidation easily, can recover the product and recycle a solvent. CONSTITUTION: The N,N'-disubstituted-3,3'-dithiopropionamide represented by the formula 1 is produced by oxidizing N-substituted-3-mercaptopropionamide represented by the formula 2, 0.4-0.5 equivalent(based on the N-substituted-3-mercaptopropionamide) of a peracid or hydrogen peroxide, and 0.001-0.5 equivalent(based on the N-substituted-3-mercaptopropionamide) of an iodine compound at 0-80deg.C in the presence of a solvent containing a water solution, an organic solvent, or an organic solvent containing a water solution. In the formulas, X and Z are hydrogens or alkyl groups and Y is hydrogen, a C1-C18 alkyl group, a cycloalkyl group of up to C10, an aralkyl group of up to C10, an aryl group of up to C10, a halogen-substituted aryl group, and etc.
摘要翻译：目的：提供以高产率和高纯度制备N，N'-二取代-3,3'-二硫丙酰胺的方法，其防止有机硫化合物的不必要的过氧化，容易控制氧化，可回收产物并再循环溶剂。构成：由式1表示的N，N'-二取代-3,3'-二硫丙酰胺通过氧化由式2表示的N-取代-3-巯基丙酰胺，0.4-0.5当量（基于N-取代 - 3-巯基丙酰胺）和0.001-0.5当量（基于N-取代-3-巯基丙酰胺）的碘化合物在0-80℃，在含有水溶液，有机溶剂或含有水溶液的有机溶剂。在该式中，X和Z是氢或烷基，Y是氢，C1-C18烷基，至多C10的环烷基，至多C10的芳烷基，至多C10的芳基，卤素取代的芳基等

56. 发明授权

KR100433206B1 3-이소티아졸론 용액 조성물 有权
标题翻译： 3-이소티아졸론용액조성3-
公开(公告)号：KR100433206B1
公开(公告)日：2004-05-28
申请号：KR1020030005973
申请日：2003-01-29
申请人： 에스케이케미칼주식회사
发明人： 최기승 , 김진만 , 박정호 , 한순종 , 김기배
IPC分类号： A61K31/425
摘要： PURPOSE: A 3-isothiazolone solution composition obtained by addition of a specified amount of a compound selected from metal bromate, NaOCl, trichloroisocyanulate, NaHCO3 and H3PO4 to an isothiazolone solution is provided. Therefore, the solution composition has an enhanced color effect without affecting bactericidal activity and storage stability of isothiazolone compounds. CONSTITUTION: In the solution composition containing 3-isothiazolone compound represented by the formula(1), the composition contains 1ppm to 3% by weight of a decolorizing agent of H3PO4. In formula, R1 and R2 are the same or different, represent H, halogen or C1-4 alkyl, or form cyclic aryl by binding R1 and R2; and R3 is H, C1-18 alkyl, C2-18 alkenyl, C2-18 alkinyl, C3-12 cycloalkyl substituted by 3-8 rings, C10-12 aralkyl or C10-18 aryl. The solution compound contains at least one selected from water, ethylene glycol, propylene glycol, dipropylene glycol, polypropylene glycol, diethylene glycol, triethylene glycol, 1,5-pentanediol, 2,4-pentanediol and benzyl alcohol.
摘要翻译：目的：提供了通过向异噻唑酮溶液中加入特定量的选自金属溴酸盐，NaOCl，三氯异氰酸盐，NaHCO3和H3PO4的化合物而得到的3-异噻唑酮溶液组合物。因此，该溶液组合物具有增强的颜色效果而不影响异噻唑酮化合物的杀菌活性和储存稳定性。构成：在含有由式（1）表示的3-异噻唑酮化合物的溶液组合物中，组合物含有1ppm至3重量％的H3PO4的脱色剂。式中，R 1和R 2相同或不同，表示H，卤素或C 1-4烷基，或通过结合R 1和R 2形成环状芳基; 和R3是H，C1-18烷基，C2-18烯基，C2-18炔基，被3-8个环取代的C3-12环烷基，C10-12芳烷基或C10-18芳基。溶液化合物含有选自水，乙二醇，丙二醇，二丙二醇，聚丙二醇，二甘醇，三甘醇，1,5-戊二醇，2,4-戊二醇和苯甲醇中的至少一种。

57. 发明授权

KR100385714B1 안정화된 이소티아졸론 용액 및 이소티아졸론의 안정화 방법 有权
标题翻译： 안정화된이소티아졸론용액및이소티아졸론의안정화방안
公开(公告)号：KR100385714B1
公开(公告)日：2003-05-27
申请号：KR1020000027455
申请日：2000-05-22
申请人： 에스케이케미칼주식회사
发明人： 한순종 , 김진만 , 최기승 , 김승환 , 박정호 , 하재민 , 김기배
IPC分类号： A01N43/48
CPC分类号： A01N43/80 , A01N59/02 , A01N25/22 , A01N2300/00
摘要： The present invention relates to stabilized isothiazolone compositions and methods of stabilization of isothiazolone, more particularly, to stabilized isothiazolone solutions comprising (a) an isothiazolone composition, (b) sulfuric acid, and (c) solvent.
摘要翻译：本发明涉及稳定的异噻唑酮组合物和稳定异噻唑酮的方法，更具体地涉及包含（a）异噻唑酮组合物，（b）硫酸和（c）溶剂的稳定的异噻唑酮溶液。

58. 发明公开

KR1020030015345A 3-이소티아졸론 용액 조성물 有权
标题翻译： 3-ISOTHIAZOLONE溶液组合物
公开(公告)号：KR1020030015345A
公开(公告)日：2003-02-20
申请号：KR1020030005972
申请日：2003-01-29
申请人： 에스케이케미칼주식회사
发明人： 최기승 , 김진만 , 박정호 , 한순종 , 김기배
IPC分类号： A61K31/425
CPC分类号： A01N25/00 , A01N43/80
摘要： PURPOSE: A 3-isothiazolone solution composition containing a specified amount of a compound selected from metal bromate, NaOCl, trichloroisocyanulate, NaHCO3 and H3PO4 in an isothiazolone solution is provided which has no trouble in storage stability, maintains bactericidal activity of 3-isothiazolone and removes a color peculiar to the compound. CONSTITUTION: The solution composition containing 3-isothiazolone compound represented by the formula(1) is characterized in that it contains 0.5 to 10% by weight of a decolorizing agent selected from NaHCO3 and Na2CO3. In formula, R1 and R2 are the same or different, represent H, halogen or C1-4 alkyl, or form cyclic aryl by binding R1 and R2; and R3 is H, C1-18 alkyl, C2-18 alkenyl, C2-18 alkinyl, C3-12 cycloalkyl substituted by 3-8 rings, C10-12 aralkyl or C10-18 aryl. The 3-isothiazolone compound is a mixture in which 5-chloro-2-methyl-4-isothiazolone-3-one and 2-methyl-4-isothiazolone-3-one are mixed in a weight ratio of 1:20 to 20:1.
摘要翻译：目的：提供在异噻唑酮溶液中含有特定量的选自金属溴酸盐，NaOCl，三氯异氰酸盐，NaHCO 3和H 3 PO 4的化合物的3-异噻唑酮溶液组合物，其储存稳定性没有问题，维持3-异噻唑酮的杀菌活性并除去化合物特有的颜色。构成：含有式（1）表示的3-异噻唑酮化合物的溶液组合物的特征在于其含有0.5至10重量％的选自NaHCO 3和Na 2 CO 3的脱色剂。在式中，R 1和R 2相同或不同，代表H，卤素或C 1-4烷基，或通过结合R1和R2形成环状芳基; R3是H，C1-18烷基，C2-18烯基，C2-18炔基，被3-8环取代的C3-12环烷基，C10-12芳烷基或C10-18芳基。 3-异噻唑酮化合物是其中5-氯-2-甲基-4-异噻唑酮-3-酮和2-甲基-4-异噻唑酮-3-酮以1:20至20:1的重量比混合的混合物。 1。

59. 发明公开

KR1020030015344A 3-이소티아졸론 용액 조성물 有权
标题翻译： 3-ISOTHIAZOLONE溶液组合物
公开(公告)号：KR1020030015344A
公开(公告)日：2003-02-20
申请号：KR1020030005971
申请日：2003-01-29
申请人： 에스케이케미칼주식회사
发明人： 최기승 , 김진만 , 박정호 , 한순종 , 김기배
IPC分类号： A61K31/425
CPC分类号： A01N25/00 , A01N43/80
摘要： PURPOSE: A 3-isothiazolone solution composition containing a decolorizing agent which is particularly well suited for chemical characteristic peculiar to a 3-isothiazolone compound is provided. The composition is removed in a color peculiar to the compound and maintains bactericidal activity and storage stability. CONSTITUTION: The solution composition containing 3-isothiazolone compound represented by the formula(1) is characterized in that it contains 0.1 to 10% by weight of a decolorizing agent of trichloroisocyanurate. In formula, R1 and R2 are the same or different, represent H, halogen or C1-4 alkyl, or form cyclic aryl by binding R1 and R2; and R3 is H, C1-3 alkyl, C1-18 alkenyl, C2-18 alkynyl, C3-12 cycloalkyl substituted by 3-8 rings, C10-12 aralkyl or C10-18 aryl.
摘要翻译：目的：提供含有特别适用于3-异噻唑酮化合物特有的化学特性的脱色剂的3-异噻唑酮溶液组合物。以化合物特有的颜色去除组合物，并保持杀菌活性和储存稳定性。构成：含有式（1）表示的3-异噻唑酮化合物的溶液组合物的特征在于其含有0.1至10重量％的三氯异氰尿酸脱色剂。在式中，R 1和R 2相同或不同，代表H，卤素或C 1-4烷基，或通过结合R1和R2形成环状芳基; R3为H，C1-3烷基，C1-18烯基，C2-18炔基，被3-8环取代的C3-12环烷基，C10-12芳烷基或C10-18芳基。

60. 发明公开

KR1020020079628A 3-이소티아졸론 용액 조성물 有权
标题翻译： 3-ISOTHIAZOLONE溶液组合物
公开(公告)号：KR1020020079628A
公开(公告)日：2002-10-19
申请号：KR1020020044587
申请日：2002-07-29
申请人： 에스케이케미칼주식회사
发明人： 최기승 , 김진만 , 박정호 , 한순종 , 김기배
IPC分类号： A61K31/425
摘要： PURPOSE: A isothiazolone solution composition having a chromaticity improving effect of the solution composition while exerting no influence on sterilizing power and stability of isothiazolone compounds is provided which has an excellent decolorizing effect. CONSTITUTION: The 3-isothiazolone solution containing isothiazolone represented by the formula 1 comprises 0.1ppm to 20% by weight of a decolorizing agent selected from NaOCl, trichloroisocyanulate, NaHCO3 and H3PO4. In formula 1, R1 and R2 are the same or different H, halogen or C1-4 alkyl, or forms a cycled aryl group by the bonding of R1 and R2; R3 is H, C1-18 alkyl, C2-18 alkenyl, C2-18 alkynyl, C3-12 cyclo alkyl bonded with 3 to 8 atoms, C10-24 aralkyl or C10-18 aryl.
摘要翻译：目的：提供具有优异的脱色效果的溶液组合物的色度提高效果，同时不影响杀菌力和异噻唑酮化合物稳定性的异噻唑酮溶液组合物。构成：含有式1表示的异噻唑酮的3-异噻唑酮溶液含有0.1ppm至20重量％的选自NaOCl，三氯异氰酸酯，NaHCO 3和H 3 PO 4的脱色剂。在式1中，R 1和R 2是相同或不同的H，卤素或C 1-4烷基，或通过R 1和R 2的键合形成环状芳基; R3是H，C1-18烷基，C2-18烯基，C2-18炔基，与3至8个原子键合的C3-12环烷基，C10-24芳烷基或C10-18芳基。

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