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1. 发明专利

JP2013043832A Purification method of fluoroalkyl vinyl ether 有权
标题翻译：氟烷基乙烯醚的纯化方法
公开(公告)号：JP2013043832A
公开(公告)日：2013-03-04
申请号：JP2011180426
申请日：2011-08-22
申请人： Unimatec Co Ltd , ユニマテック株式会社
发明人： AKEMA YUKI , KOGANE KEISUKE , MURAI DAISUKE
IPC分类号： C07C41/42 , C07C41/46 , C07C43/17
摘要： PROBLEM TO BE SOLVED: To provide a purification method by which a fluoroalkyl vinyl ether is efficiently separated by using a specified treatment agent whose final removal is not needed.SOLUTION: A crude fluoroalkyl vinyl ether containing a hydrogen fluoride addition product of fluoroalkyl vinyl ether is distilled in the presence of 1 to 10 wt.% amines to the crude fluoroalkyl vinyl ether, having a boiling point higher than that of fluoroalkyl vinyl ether by 70°C or more. The fluoroalkyl vinyl ether contains fluoroalkyl monovinyl ether and fluoroalkylene divinyl ether.
摘要翻译：要解决的问题：提供通过使用不需要最终去除的特定处理剂来有效分离氟烷基乙烯基醚的纯化方法。解决方案：将含有氟代烷基乙烯基醚的氟化氢加成产物的粗的氟代烷基乙烯基醚在1至10重量％的胺存在下蒸馏至粗的氟代烷基乙烯基醚，其沸点高于氟代烷基乙烯基乙醚70℃以上。氟烷基乙烯基醚包含氟烷基单乙烯基醚和氟代亚烷基二乙烯基醚。版权所有（C）2013，JPO＆INPIT

2. 发明专利

JP2014047314A Fluorinated rubber composition 有权
标题翻译：氟化橡胶组合物
公开(公告)号：JP2014047314A
公开(公告)日：2014-03-17
申请号：JP2012193022
申请日：2012-09-03
申请人： Unimatec Co Ltd , ユニマテック株式会社
发明人： AKEMA YUKI , SHIRANE ATSUSHI , MAEDA MITSURU
IPC分类号： C08L27/12 , C08K3/04 , C08K5/14 , C09K3/10
摘要： PROBLEM TO BE SOLVED: To provide a fluorinated rubber composition yielding a cross-linked product having an improved pressure-resistant compressive permanent set characteristic at a high temperature of 200°C or above.SOLUTION: The provided fluorinated rubber composition is obtained by mixing, with 100 pts.wt. of a peroxide-cross-linkable fluorine-containing rubber, 1-50 pts.wt. of a plant-derived porous carbon powder, 1-10 pts.wt. of an organic peroxide cross-linking agent, and no more than 10 pts.wt. of a polyfunctional unsaturated compound co-cross-linking agent. This fluorine-containing rubber composition is capable, by virtue of the use thereby of the plant-derived porous carbon powder in place of reinforcements or fillers used in the prior art such as carbon black or Austin Black, etc., of increasing the blending ratio of the carbon powder to approximately 4 times the blending ratio of carbon black used in the prior art and of accordingly yielding a cross-linked product not only realizing electric effects but also having a significantly improved pressure-resistant compressive permanent set characteristic at a high temperature of 200°C or above.
摘要翻译：要解决的问题：提供一种产生在200℃或更高的高温下具有改进的耐压缩永久变形特性的交联产物的氟化橡胶组合物。溶液：所提供的含氟橡胶组合物通过混合，用100 pts.wt 的过氧化物可交联的含氟橡胶，1-50重量份的植物来源的多孔碳粉，1-10重量份的有机过氧化物交联剂，不超过10重量份的多官能不饱和化合物共交联剂。这种含氟橡胶组合物由于使用植物来源的多孔碳粉代替现有技术中使用的增强物或填料，例如炭黑或奥斯汀黑等能够提高共混比的碳粉至现有技术中使用的炭黑的共混比的约4倍，并因此产生交联产物，不仅实现电效应，而且在高温下具有显着改善的耐压缩永久变形特性为200℃以上。

3. 发明专利

JP2013060412A Method of manufacturing perfluoroalkyl vinyl ether 有权
标题翻译：制备全氟代乙烯基醚的方法
公开(公告)号：JP2013060412A
公开(公告)日：2013-04-04
申请号：JP2011264200
申请日：2011-12-02
申请人： Unimatec Co Ltd , ユニマテック株式会社
发明人： KOGANE KEISUKE , MURAI DAISUKE , AKEMA YUKI , MURAKAMI SOICHIRO
IPC分类号： C07C41/24 , C07C43/17
摘要： PROBLEM TO BE SOLVED: To provide a method of obtaining perfluoroalkyl vinyl ether in high yield without causing any problems of a waste solvent treatment.SOLUTION: An aqueous solution or an alcohol solution of a perfluoroalkyl carboxylic acid alkali metal salt represented by the general formula Rf[OCF(CF)-COOM]n (where n is an integer of 1 or 2, Rf is a perfluoroalkyl group with 2-12C having a straight-chain or branch structure when n=1 or a perfluoroalkylene group with 2-12C having a straight-chain or branch structure when n=2, and M is alkali metal) is atomized and dried until the remaining amount of the solvent becomes 1 wt.% or less at a temperature of 120°C or lower, and the obtained perfluoroalkyl carboxylic acid alkali metal salt is heated at a temperature of 120°C or higher to be subjected to vinylation.
摘要翻译：要解决的问题：提供以高产率获得全氟烷基乙烯基醚的方法，而不引起任何废溶剂处理的问题。解决方案：由通式Rf [OCF（CF 3 ） - COOM] n表示的全氟烷基羧酸碱金属盐的水溶液或醇溶液 n为1或2的整数，当n = 1时，Rf为2-12C具有直链或支链结构的全氟烷基，或当n = 2时具有2-12C的具有直链或支链结构的全氟亚烷基，M为碱金属）进行雾化干燥，直至在120℃以下的温度下，溶剂的残留量为1重量％以下，将得到的全氟烷基羧酸碱金属盐在 120℃以上进行乙烯化。版权所有（C）2013，JPO＆INPIT

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