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1. 发明专利

JP2002102709A CRYSTALLINE MWW TYPE TITANOSILICATE CATALYST FOR PRODUCTION OF OXIDIZED COMPOUND, METHOD FOR PRODUCING THE SAME AND METHOD FOR PRODUCING OXIDIZED COMPOUND USING THE SAME 失效
公开(公告)号：JP2002102709A
公开(公告)日：2002-04-09
申请号：JP2000298133
申请日：2000-09-29
申请人： SHOWA DENKO KK
发明人： OGUCHI WATARU , TSUJI KATSUYUKI , TATSUMI TAKASHI , GO HO
IPC分类号： C30B29/22 , B01J29/70 , B01J29/89 , B82Y30/00 , C01B37/00 , C01B39/00 , C07B61/00 , C07C29/03 , C07C29/48 , C07C31/22 , C07D301/12 , C07D301/14 , C07D301/19 , C07D303/04 , C07D303/08 , C07D303/14 , C07D303/22 , H01L21/8246 , H01L27/105 , H01L41/08 , H01L41/083 , H01L41/18 , H01L41/187
摘要： PROBLEM TO BE SOLVED: To produce a crystalline titanosilicate catalyst usable as a catalyst for the oxidation reaction of a compound having a carbon-carbon double bond and one or more other functional groups, to provide a method for producing the catalyst and a method for producing an oxidized compound by the oxidation reaction using the catalyst. SOLUTION: The crystalline titanosilicate having the structure code MWW acts effectively as a catalyst for the oxidation reaction of the carbon-carbon double bond of a compound having one or more functional groups besides the double bond using a peroxide as an oxidizing agent and gives the objective oxidized compound with high selectivity.

2. 发明专利

JP2004256386A MODIFIED LAYERED METALLOSILICATE MATERIAL AND ITS PRODUCING METHOD 审中-公开
公开(公告)号：JP2004256386A
公开(公告)日：2004-09-16
申请号：JP2004026655
申请日：2004-02-03
申请人： SHOWA DENKO KK
发明人： TATSUMI TAKASHI , GO HO , TSUJI KATSUYUKI
IPC分类号： B01J29/89 , C01B33/00 , C01B33/36 , C01B37/00 , C01B39/04 , C01B39/48
摘要： PROBLEM TO BE SOLVED: To provide a convenient method for producing a modified layered material which has a high content of an element having a large ion radius and included in the skeletal structure. SOLUTION: The modified layered metallosilicate material is produced by the following five steps: the first step to obtain a boron-containing layered silicate precursor by heating a mixture containing a template compound, a boron compound, a silicon-containing compound and water; the second step to treat the precursor obtained by the first step with an acid; the third step to swell the layered precursor treated with an acid at the second step by heating the precursor in the presence of a swelling agent; the fourth step to modify the overlapping state of the layers of the swelled layered precursor obtained at the third step; and the fifth step to fire the precursor obtained at the fourth step, giving the modified layered metallosilicate material. COPYRIGHT: (C)2004,JPO&NCIPI

3. 发明专利

JP2008290942A Metallosilicate substance having mww type structure and precursor substance therefor 有权
标题翻译：具有MWW类型结构和前驱体物质的金属化物质
公开(公告)号：JP2008290942A
公开(公告)日：2008-12-04
申请号：JP2008200163
申请日：2008-08-01
申请人： Showa Denko Kk , 昭和電工株式会社
发明人： TATSUMI TAKASHI , GO HO , TSUJI KATSUYUKI
IPC分类号： C01B39/48 , C01B33/36 , C01B37/00 , C01B39/04 , C01B39/08
CPC分类号： C01B39/08 , C01B37/005 , C01B39/085 , C01B39/48
摘要： PROBLEM TO BE SOLVED: To provide a zeolite containing an element having a large ionic radius and being difficult to introduce by a common synthesis method in the framework at a high ratio. SOLUTION: The metallosilicate having the MWW type structure contains at least one type of an element selected from the elements of groups 3 to 14 in the fourth period or latter in the periodic table. This substance can be produced by the following steps 1 to 4: step 1 of heating a mixture containing a template compound, a compound containing an element of group 13 in the periodic table, a silicon-containing compound, and water to obtain a precursor, step 2 of acid-treating the precursor obtained in step 1, step 3 of heating the acid-treated precursor obtained in step 2 together with a mixture containing a template compound and water in the presence of a compound containing at least one type of an element selected from the elements of group 3 to 14 in the fourth period or latter in the periodic table to obtain a precursor again, and step 4 of calcining the precursor obtained in step 3 to obtain a crystalline zeolite substance. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：提供一种含有离子半径大的元素的沸石，并且难以通过通常的合成方法以高比例在骨架中引入沸石。解决方案：具有MWW型结构的金属硅酸盐在第四周期或后周期表中含有至少一种选自第3至14族元素的元素。该物质可以通过以下步骤1至4：步骤1，加热含有模板化合物，含有元素周期表中第13族元素的化合物，含硅化合物和水的混合物，得到前体，在步骤1，步骤3中获得的前体酸化处理步骤2，在含有至少一种类型元素的化合物的存在下，将在步骤2中获得的经酸处理的前体与含有模板化合物和水的混合物一起加热选自第四周期或第四周期中的组3至14的元素，以再次获得前体，以及煅烧步骤3中获得的前体以获得结晶沸石物质的步骤4。版权所有（C）2009，JPO＆INPIT

4. 发明专利

JP2004292171A Titanosilicate, its production method, and production method of oxidation compound using titanosilicate 有权
公开(公告)号：JP2004292171A
公开(公告)日：2004-10-21
申请号：JP2003036747
申请日：2003-02-14
申请人： Showa Denko Kk , 昭和電工株式会社
发明人： TATSUMI TAKASHI , GO HO , TSUJI KATSUYUKI
IPC分类号： C07D301/12 , B01J29/06 , B01J29/89 , B01J35/00 , C01B37/00 , C01B39/08 , C07B41/00 , C07B61/00 , C07C29/00 , C07C29/48 , C07D303/04 , C07D303/14
CPC分类号： B01J35/002 , B01J29/89 , B01J2229/37 , C01B37/005 , C01B39/085 , C07C29/48 , C07D301/12 , C07C31/225
摘要： PROBLEM TO BE SOLVED: To provide a titanosilicate which can be used as a catalyst for oxidation reaction of an organic compound. SOLUTION: The titanosilicate is represented by composition formula (1): xTiO 2 (1-x)SiO 2 (wherein x ia 0.0001-0.2). In its infrared spectrum measured in a dehydrated state, the maximum value of the absorption band is at 930±15cm -1 . COPYRIGHT: (C)2005,JPO&NCIPI

5. 发明专利

JP2003327425A Mww type zeolite substance, precursory substance thereof and their production method 有权
标题翻译： MWW型沸石物质及其生产方法
公开(公告)号：JP2003327425A
公开(公告)日：2003-11-19
申请号：JP2003026529
申请日：2003-02-03
申请人： Showa Denko Kk , 昭和電工株式会社
发明人： TATSUMI TAKASHI , GO HO , TSUJI KATSUYUKI
IPC分类号： C01B39/48 , C01B33/36 , C01B37/00 , C01B39/04 , C01B39/08
CPC分类号： C01B39/08 , C01B37/005 , C01B39/085 , C01B39/48
摘要： PROBLEM TO BE SOLVED: To provide a method of easily synthesizing zeolite containing elements having a large ionic radius of which introduction is hard by common synthesis methods in a skeleton at a high ratio. SOLUTION: The method of producing a zeolite substance having an MWW type structure comprises the step 1 wherein a mixture containing a template compound, a compound containing the group 13 elements in the Periodic Table, a silicon-containing compound and water is heated to obtain a precursor; the step 2 wherein the precursor obtained in the stage 1 is subjected to acid treatment; the step 3 wherein the acid-treated precursor obtained in the step 2 is heated together with a mixture containing a template compound and water to obtain the precursor once more; and the step 4 wherein the precursor obtained in the step 3 is fired to obtain the crystalline zeolite substance. COPYRIGHT: (C)2004,JPO
摘要翻译：要解决的问题：提供一种通过常规合成方法在骨架中以高比率容易地合成具有大的离子半径的含沸石元素的方法，其通过常规合成方法进行硬介导。解决方案：制备具有MWW型结构的沸石物质的方法包括步骤1，其中将含有模板化合物，含有元素周期表中第13族元素的化合物，含硅化合物和水的混合物加热以获得前体; 步骤2，其中在阶段1中获得的前体经受酸处理; 步骤3，其中将步骤2中获得的经酸处理的前体与含有模板化合物和水的混合物一起加热以再次获得前体; 和步骤4，其中烧成步骤3中得到的前体以得到结晶沸石物质。版权所有（C）2004，JPO

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