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1. 发明专利

JPS57117551A Powdering of acrylate polymer 失效
标题翻译：丙烯酸酯聚合物的粉末
公开(公告)号：JPS57117551A
公开(公告)日：1982-07-22
申请号：JP246981
申请日：1981-01-10
申请人： Seitetsu Kagaku Co Ltd
发明人： TAKAGI SHIYUUJI , NANBA HIROYUKI , ARAKI HIDEKAZU
IPC分类号： C08L33/00 , C08J3/12 , C08L33/02
摘要： PURPOSE: To obtain an inexpensive powdery resin having improved water absorption free from decomposition, by putting a predried powdery acrylate polymer in a dryer, preparing the titled polymer from a solution comprising an acrylate polymer without requiring grinding process.
CONSTITUTION: An acrylate polymer, preferably a polymer obtained by reversed phase emulsion polymerization, etc. from a monomer having a partial neutralization degree of 50W90mol% is blended with powdery acrylate polymer which is predried in a dryer in such a way that a ratio of the polymer to water in the system becomes ≥3/2, and the blend is dried in a dryer at drying temperature ≤150°C preferably in an inert gas atmosphere with stirring. No pretreatment is required at all, nor processes such as cutting, grinding, classification, etc. are needed. When the ratio of the polymer before the start of drying to water is
摘要翻译：目的：为了获得具有改善的吸水性分解的廉价的粉末状树脂，通过将预干燥的丙烯酸甲酯聚合物置于干燥器中，从包含丙烯酸酯聚合物的溶液中制备标题聚合物，而不需要研磨过程。构成：将丙烯酸酯聚合物，优选通过反相乳液聚合等获得的部分中和度为50-90mol％的单体的聚合物与在干燥器中预干燥的粉末状丙烯酸酯聚合物共混，的体系中的聚合物与水的比例变为> = 3/2，并且在干燥温度<= 150℃的干燥器中，优选在惰性气体气氛中搅拌下将共混物干燥。根本不需要预处理，也不需要切割，研磨，分级等处理。当开始干燥之前的聚合物与水的比例<3/2时，不能获得粉末聚合物，并且聚合物变成颗粒状或体积大的。

2. 发明专利

JPS54103873A PREPARATION OF 22BROMOOPYRIDINE OR ITS DERIVATIVE 失效
公开(公告)号：JPS54103873A
公开(公告)日：1979-08-15
申请号：JP791578
申请日：1978-01-26
申请人： SEITETSU KAGAKU CO LTD
发明人： KAWAMURA MASAO , AKUTSU SEIICHI , TAKAGI SHIYUUJI , SAWADA KIYOSHI
IPC分类号： C07D213/61
摘要： PURPOSE:To obtain the title compound useful as a raw material for pesticides, in high yield economically, by reacting a specific relatively inexpensive compound, e.g. 2-chloropyridine, with hydrogen bromide at a relatively low temperature with easy separation. CONSTITUTION:2-chloropyridine or its derivative of formula I: (R1, R2, R3 and R4 are H or CH3), e.g. 2-chloro-, 2-chloro-3-methyl- or 2-chloro-4-methylpyridine, is reacted with hydrogen bromide gas in an anhydrous organic medium, preferably glacial acetic acid, at 70 deg.C or above but not higher than the boiling point of the solvent to form a 2-bromopyridine or its derivative of formula II. Preferably, the weight ratio of the organic medium to the raw material (R) is 10-20:1, and the molar ratio of the hydrogen bromide gas to R is 1-10:1.

3. 发明专利

JPS5368769A PURIFICATION OF 22THIOPHENEACETIC ACID 失效
公开(公告)号：JPS5368769A
公开(公告)日：1978-06-19
申请号：JP14240476
申请日：1976-11-27
申请人： SEITETSU KAGAKU CO LTD
发明人： KAWAMURA MASAO , TSUCHIYA HIROO , TAKAGI SHIYUUJI
IPC分类号： C07D333/24 , C07D333/10
摘要： PURPOSE:To prepare highly pure 2-thiopheneacetic acid easily, useful as antibiotic chemical modifiers and raw materials for pharmaceuticals, in high yield by distillation of crude 2-thiopheneacetic acid with thin film evaporator. by low-temp. rapid distillation.

4. 发明专利

JPS60212430A Pulverization of polyolefin 失效
标题翻译：聚烯烃的粉化
公开(公告)号：JPS60212430A
公开(公告)日：1985-10-24
申请号：JP6963584
申请日：1984-04-06
申请人： Seitetsu Kagaku Co Ltd
发明人： TAKAGI SHIYUUJI , ARAKI HIDEKAZU , YAMAMOTO TAKUSHI , NAKAMURA MORIO
IPC分类号： C08J3/16 , C08J3/03
摘要： PURPOSE: Polyolefin is emulsified in an aqueous medium in the presence of ethylene oxide-propylene oxide copolymer and ethylene-acrylate copolymer, then cooled down to give a fine powder of uniform and true sphere.
CONSTITUTION: Polyolefin is heated under pressure in an aqueous medium in the presence of ethylene-propylene oxide copolymer and ethylene-acrylic acid copolymer and emulsified by melting and stirring, then cooled down lower than the softening point of the polyolefin. The polyolefin used is polyethylene or polypropylene with 20 or more, preferably 50 or more melt index at the emulsification temperature. The amount of the ethylene-acrylate copolymer is 0.5W20%, preferably 1W10% based on the polyolefin. The powder has a shape of true sphere of less than 5μ particle size.
COPYRIGHT: (C)1985,JPO&Japio
摘要翻译：目的：在环氧乙烷 - 环氧丙烷共聚物和乙烯 - 丙烯酸酯共聚物存在下，将聚烯烃在水性介质中乳化，然后冷却，得到均匀真实球体的细粉末。构成：在乙烯 - 环氧丙烷共聚物和乙烯 - 丙烯酸共聚物的存在下，在含水介质中加压聚烯烃，并通过熔融和搅拌乳化，然后冷却至低于聚烯烃的软化点。使用的聚烯烃是在乳化温度下具有20以上，优选为50以上的熔融指数的聚乙烯或聚丙烯。基于聚烯烃，乙烯 - 丙烯酸酯共聚物的量为0.5-20％，优选1-10％。粉末具有小于5mu粒径的真实球体的形状。

5. 发明专利

JPS6099184A COMPOSITION FOR BONDING AND METHOD FOR BONDING USING THE SAME 失效
公开(公告)号：JPS6099184A
公开(公告)日：1985-06-03
申请号：JP20804883
申请日：1983-11-04
申请人： SEITETSU KAGAKU CO LTD , SUMITOMO CHEMICAL CO
发明人： TAKAGI SHIYUUJI , AOSHIMA MASASHI , ARAKI HIDEKAZU , KOYAMA TAKASHI
IPC分类号： C08L61/12 , B29B15/14 , B29D30/40 , B29K21/00 , C08J5/04 , C08J5/12 , C08L23/00 , C08L23/34 , C08L61/00 , C08L61/04 , C08L101/00 , C09J123/28 , C09J161/06
摘要： PURPOSE:To provide a composition composed of an aqueous solution of a resorcinol.formaldehyde resin, a vulcanization controller for rubber and a sulfochlorinated polyolefin, and suitable for the firm bonding of a fiber material with rubber. CONSTITUTION:The objective composition is composed of (A) an aqueous solution of a resorcinol-formaldehyde resin, (B) a vulcanization controller for rubber (preferably tetramethylthiuram disulfide, mercaptobenzothiazole, nickel dibutyldithiocarbamate, etc.) and (C) a sulfochlorinated polyolefin (preferably sulfochlorinated polyethylene, etc.). The amount of the component B is preferably 0.3-30pts.wt. per 100pts.wt. of the component C.

6. 发明专利

JPS5953780A Surface treatment of fiber 失效
公开(公告)号：JPS5953780A
公开(公告)日：1984-03-28
申请号：JP16288682
申请日：1982-09-17
申请人： Sumitomo Chemical Co , Seitetsu Kagaku Co Ltd
发明人： OKITA TAISUKE , AOSHIMA MASASHI , NAKAMURA MORIO , TAKAGI SHIYUUJI
IPC分类号： D06M11/00 , B32B7/04 , B32B25/10 , C08J5/06 , D06M11/44 , D06M11/76 , D06M13/184 , D06M15/244 , D06M15/41 , D06M101/00 , D06M101/02 , D06M101/16

7. 发明专利

JPS60237091A PREPARATION OF DIALKYL ZINC 失效
公开(公告)号：JPS60237091A
公开(公告)日：1985-11-25
申请号：JP9160784
申请日：1984-05-07
申请人： SEITETSU KAGAKU CO LTD
发明人： TAKAGI SHIYUUJI , INOUE YOSHIO , NII SHINJI
IPC分类号： C07F3/06
摘要： PURPOSE:To obtain the titled compound useful as a polymerization catalyst for polymers, dopant for semiconductors, etc., economically in an industrial scale, by carrying out the reaction of alkyl halide with zinc and the thermal decomposition of the product in an organic solvent inert to dialkyl zinc. CONSTITUTION:At least one kind of alkyl halide (preferably an alkyl bromide or a mixture of alkyl bromide and alkyl iodide) is made to react with zinc, and the reaction product is thermally decomposed preferably at 150-300 deg.C in an organic solvent inert to dialkyl zince (preferably kerosene). The mixed vapor of dialkyl zinc and the organic solvent is separated from the reaction mixture by distillation.

8. 发明专利

JPS5843718A SEEDLING GROWING METHOD 失效
公开(公告)号：JPS5843718A
公开(公告)日：1983-03-14
申请号：JP14280581
申请日：1981-09-09
申请人： SEITETSU KAGAKU CO LTD
发明人： OOHAYASHI SHIGEJI , KATOU TAKESHI , NAKAMURA MORIO , TAKAGI SHIYUUJI , TAKEMORI SHINICHI
IPC分类号： A01G9/00

9. 发明专利

JPS5513244A PURIFICATION OF 22AMINOTHIAZOLE 失效
公开(公告)号：JPS5513244A
公开(公告)日：1980-01-30
申请号：JP8636478
申请日：1978-07-14
申请人： SEITETSU KAGAKU CO LTD
发明人： KAWAMURA MASAO , AKUTSU SEIICHI , TAKAGI SHIYUUJI
IPC分类号： C07D277/20 , C07D277/40
摘要： PURPOSE:To improve the yield and purity of the title compound useful as an intermediate for the synthesis of medicines and dyes, by concentrating and neutralizing the acid reaction mixture obtained from chloroacetaldehyde and thiourea to separate and purify the compound. CONSTITUTION:Chloroacetaldehyde obtained from vinyl acetate, paraldehyde, and acetal, is reacted with thiourea to give an acid reaction mixture, which is preferably concentrated in vacuo to distill away at least 1/4 of the mixture volume, preferably to dryness. The concentrate is neutralized with an aqueous alkali to deposit 2- aminothiazole.

10. 发明专利

JPS5346962A PREPARATION OF THIOPHENEACETIC ACIDS 失效
公开(公告)号：JPS5346962A
公开(公告)日：1978-04-27
申请号：JP12058476
申请日：1976-10-06
申请人： SEITETSU KAGAKU CO LTD
发明人： KAWAMURA MASAO , TSUCHIYA HIROO , TAKAGI SHIYUUJI , TAKAHASHI MASAHIDE , SOMETA HITOSHI
IPC分类号： C07D333/24 , C07D333/06
摘要： PURPOSE:To prepare thiopheneacetic acids easily, useful as chemical modifier for synthetic antibiotics and raw materials for pharmaceuticals, by the photochemical reaction of thiophene with monohaloacetic acid or its ester under ultraviolet irradiation.

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