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1. 发明专利

JP2008156525A Method for producing aliphatic polyester 审中-公开
标题翻译：生产聚酯聚酯的方法
公开(公告)号：JP2008156525A
公开(公告)日：2008-07-10
申请号：JP2006348181
申请日：2006-12-25
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TERADO YUJI , JINNAI TAKASHI , TAKAOKA MASAZUMI , WADA MASARU
IPC分类号： C08G63/90 , C08L101/16
摘要： PROBLEM TO BE SOLVED: To provide a method for producing an aliphatic polyester of improved yield compared with conventional method for polymerizing an aliphatic polyester. SOLUTION: An aliphatic polyester having a weight-average molecular weight of 100,000-600,000 and containing 0-2 wt.% aliphatic cyclic ester is produced by carrying out a ring-opening polymerization of an aliphatic cyclic ester (a) in molten state to obtain an aliphatic polyester (b) having a weight-average molecular weight of 100,000-600,000 and containing 20-70 wt.% aliphatic cyclic ester, granulating the product and bringing the granule into contact with an organic solvent in a state not to dissolve the aliphatic polyester. In the above method, the aliphatic cyclic ester present in the organic solvent after the contact with the aliphatic polyester is purified and the obtained aliphatic cyclic ester is used again as the polymerization raw material. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供与用于聚合脂族聚酯的常规方法相比，生产脂肪族聚酯的产率提高的方法。解决方案：重均分子量为100,000-600,000，含有0-2重量％脂族环酯的脂肪族聚酯通过在熔融状态下进行脂肪族环状酯（a）的开环聚合而制备以获得重均分子量为100,000-600,000并含有20-70重量％的脂族环酯的脂族聚酯（b），将产物造粒并使颗粒与有机溶剂接触，其状态不为溶解脂肪族聚酯。在上述方法中，与脂肪族聚酯接触后存在于有机溶剂中的脂肪族环酯被纯化，得到的脂肪族环酯再次用作聚合原料。版权所有（C）2008，JPO＆INPIT

2. 发明专利

JP2006143611A Method for preparing 1,5-diaminonaphthalene 有权
标题翻译：制备1,5-二氨基萘甲酸的方法
公开(公告)号：JP2006143611A
公开(公告)日：2006-06-08
申请号：JP2004332820
申请日：2004-11-17
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： KUMAMOTO YUKIHIRO , TAKAOKA MASAZUMI , WADA MASARU
IPC分类号： C07C209/14 , C07B61/00 , C07C201/12 , C07C205/06 , C07C205/26 , C07C211/57
摘要： PROBLEM TO BE SOLVED: To provide a new method for industrially advantageously preparing 1,5-diaminonaphthalene which does not by-produce a 1,8-diamino isomer and does not go through a relatively unstable nitroimine/nitroenamine as an intermediate. SOLUTION: 5-Nitro-1-tetralone is halogenated and dehydrohalogenated to be aromatized without using a large amount of a noble metal catalyst, and then reduced and aminated to industrially advantageously prepare 1,5-diaminonaphthalene. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供一种工业上有利地制备不产生1,8-二氨基异构体并不通过作为中间体的相对不稳定的硝基亚胺/硝基胺的1,5-二氨基萘的新方法。解决方案：将5-硝基-1-四氢萘酮卤化并脱卤化氢以在不使用大量贵金属催化剂的情况下芳构化，然后在工业上还原和胺化有利地制备1,5-二氨基萘。版权所有（C）2006，JPO＆NCIPI

3. 发明专利

JP2003277331A Method for producing 4,6-dinitroresorcin and new sulfonated substance of dihydroxybenzoic acids and salt thereof 审中-公开
标题翻译：二羟基苯甲酸及其盐的生产方法4,6-四氮杂环辛烷酮和新型磺化物质
公开(公告)号：JP2003277331A
公开(公告)日：2003-10-02
申请号：JP2002112275
申请日：2002-04-15
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： YOSHITOMI HIDETAKE , KUMAMOTO YUKIHIRO , TAKAOKA MASAZUMI , MIZUTA HIDEKI , MATSUZAKI YORIAKI
IPC分类号： C07C201/12 , C07C205/23 , C07C309/60
摘要： PROBLEM TO BE SOLVED: To provide a new method for industrially and advantageously producing 4,6-dinitroresorcin without passing through a nitrated substance of a halobenzene.
SOLUTION: The method for producing the 4,6-dinitroresorcin comprises treating a compound represented by general formula (1) (wherein, R denotes a hydrogen atom, a methyl group, an ethyl group or a propyl group) with a nitrating agent and then subjecting the resultant compound to a decarboxylation treatment. Furthermore, the compound represented by general formula (1) is treated with a sulfonating agent and the resultant new sulfonated substance is treated with the nitrating agent and then subjected to the carboxylation treatment. Thereby, the 4,6-dinitroresorcin can be produced.
COPYRIGHT: (C)2004,JPO
摘要翻译：要解决的问题：提供一种工业上有利地生产4,6-二硝基间苯二酚而不通过卤代苯的硝化物质的新方法。解决方案：制备4,6-二硝基间苯二酚的方法包括用硝化处理由通式（1）表示的化合物（其中R表示氢原子，甲基，乙基或丙基）然后使所得化合物进行脱羧处理。此外，用磺化剂处理由通式（1）表示的化合物，所得新的磺化物质用硝化剂处理，然后进行羧化处理。由此，可以制造4,6-二硝基间苯二酚。版权所有（C）2004，JPO

4. 发明专利

JP2008174517A Method for purifying cyclic ester 审中-公开
标题翻译：净化环孢菌素的方法
公开(公告)号：JP2008174517A
公开(公告)日：2008-07-31
申请号：JP2007011308
申请日：2007-01-22
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TAKAOKA MASAZUMI , WADA MASARU , MAEKAWA HIROKI
IPC分类号： C07D319/12
摘要： PROBLEM TO BE SOLVED: To provide a simple method of purification, obtaining a high purity cyclic ester used as a raw material of a high molecular weight polyester, at a high yield.
SOLUTION: This new method for purifying the cyclic ester expressed by formula (1) [wherein, R
1 to R
6 are each the same or different H, or a 1-4C linear or branched alkyl: and (n) is an integer of 1 to 3] is characterized by mixing the cyclic ester expressed by the formula (1) with an isocyanate compound, heating and then distilling.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供简单的纯化方法，以高产率获得用作高分子量聚酯的原料的高纯度环酯。解决方案：用于纯化由式（1）表示的环状酯的新方法[其中R 1和R 6各自相同或不同H，或 1-4烷基直链或支链烷基，（n）为1〜3的整数]的特征在于将由式（1）表示的环状酯与异氰酸酯化合物混合，加热然后蒸馏。版权所有（C）2008，JPO＆INPIT

5. 发明专利

JP2004196704A Method for manufacturing 5-nitro-1-tetralone 审中-公开
公开(公告)号：JP2004196704A
公开(公告)日：2004-07-15
申请号：JP2002366805
申请日：2002-12-18
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： KUMAMOTO YUKIHIRO , TAKAOKA MASAZUMI , MIZUTA HIDEKI , MATSUZAKI YORIAKI
IPC分类号： C07C201/12 , C07B61/00 , C07C205/45 , C07C205/56
摘要： PROBLEM TO BE SOLVED: To provide a method for safely manufacturing 5-nitro-1-tetralone, useful as a precursor of 1,5-diaminonaphthalene, selectively in a high yield without causing the formation of an isomer and without using chromic anhydride which exerts a great influence on the environment or a superacid which is difficult to handle.
SOLUTION: 5-Nitro-1-tetralone is industrially advantageously manufactured by the cyclization, using an acid catalyst, of 4-(2-nitrophenyl)butanoic acid halide obtained by halogenating 4-(2-nitrophenyl)butanoic acid obtained by hydrolyzing 4-(2-nitrophenyl)butanoate.
COPYRIGHT: (C)2004,JPO&NCIPI

6. 发明专利

JP2007009157A Method for producing aliphatic polyester 审中-公开
标题翻译：生产聚酯聚酯的方法
公开(公告)号：JP2007009157A
公开(公告)日：2007-01-18
申请号：JP2005195401
申请日：2005-07-04
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： WADA MASARU , UEDA NAOHIRO , TAKAOKA MASAZUMI , JINNAI TAKASHI
IPC分类号： C08G63/90 , C08G63/06
摘要： PROBLEM TO BE SOLVED: To provide a method for polymerizing an aliphatic polyester by polymerizing an alicyclic ester by solving a problem of requiring a very long polymerization time.
SOLUTION: This new method for producing the aliphatic polyester by polymerizing the aliphatic ester expressed by formula (1) [wherein, R
1 to R
3 are each the same or different and H, -CH
3 , -CH
2 -CH
3 , -(CH
2 )
2 -CH
3 or -CH(CH
3 )-CH
3 ; X is O or S; and (n) is an integer] is provided by performing melt ring-opening polymerization, then bringing the obtained polymer in contact with a solvent to remove the remaining aliphatic ester in the polymer.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供通过解决需要非常长的聚合时间的问题来聚合脂环族酯的聚合脂肪族聚酯的方法。解决方案：通过将由式（1）表示的脂肪族酯（其中R SB 1至SB 3与R SB 3）共聚制备脂肪族聚酯的新方法各自相同或不同的，H，-CH 3 SB 3， - CH 2， - CH 3， - （CH 2 SB 2） SB> 2 3 或-CH（CH 3 SB 3）-CH 3 SB 3; X是O或S; 和（n）为整数]通过进行熔融开环聚合提供，然后将所得聚合物与溶剂接触以除去聚合物中剩余的脂族酯。版权所有（C）2007，JPO＆INPIT

7. 发明专利

JP2007056138A Aliphatic polyester production method 审中-公开
标题翻译：涤纶聚酯生产方法
公开(公告)号：JP2007056138A
公开(公告)日：2007-03-08
申请号：JP2005243083
申请日：2005-08-24
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TERADO YUJI , TAKAOKA MASAZUMI , JINNAI TAKASHI , WADA MASARU
IPC分类号： C08G63/66 , C08G63/688 , C08G63/78
摘要： PROBLEM TO BE SOLVED: To provide a new aliphatic polyester production method which has the same or larger mol. wt. and a largely more shortened polymerization time as or than those of known aliphatic polyester production methods.
SOLUTION: This aliphatic polyester production method comprising ring-opening polymerizing an aliphatic cyclic ester (a) represented by the general formula (1) [R1, R2 and R3 are identically or differently each -H, -CH
3 , -CH
2 -CH
3 , -(CH
2 )
2 -CH
3 , or -CH(CH
3 )-CH
3 ; X is O or S] in the presence of a polymerization initiator and a catalyst is characterized by having a process for additionally charging the aliphatic cyclic ester (a) once or more and then continuously ring-opening polymerizing the mixture.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供具有相同或更大摩尔的新的脂族聚酯制备方法。重量。并且与已知的脂肪族聚酯制备方法的聚合时间大大缩短。解决方案：包含由通式（1）表示的脂族环酯（a）的开环聚合的脂族聚酯制备方法[R1，R2和R3各自相同或不同，各自为-H，-CH 3 ，-CH 2 3 ， - （CH 2 > 3 或-CH（CH 3 SB 3）-CH 3 SB 3; X是O或S]，并且催化剂的特征在于具有一种或多种脂肪族环酯（a）另外加入然后使混合物连续开环聚合的方法。版权所有（C）2007，JPO＆INPIT

8. 发明专利

JP2004115403A Method for producing 4,6-dinitroresorcinol 审中-公开
标题翻译：生产4,6-DINCORCORCINOL的方法
公开(公告)号：JP2004115403A
公开(公告)日：2004-04-15
申请号：JP2002278554
申请日：2002-09-25
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TAKAOKA MASAZUMI , YOSHITOMI HIDETAKE , KUMAMOTO YUKIHIRO , MIZUTA HIDEKI , MATSUZAKI YORIAKI
IPC分类号： C07C201/12 , C07C201/08 , C07C205/23
摘要： PROBLEM TO BE SOLVED: To provide a method for profitably producing 4,6-dinitroresorcinol.
SOLUTION: This method for producing the 4,6-dinitroresorcinol is characterized by treating a compound represented by general formula (1) (X is Cl or Br) with a nitrating agent and then hydrolyzing the product.
COPYRIGHT: (C)2004,JPO
摘要翻译：要解决的问题：提供一种有利地生产4,6-二硝基间苯二酚的方法。解决方案：该制造4,6-二硝基间苯二酚的方法的特征在于用硝化剂处理通式（1）表示的化合物（X为Cl或Br），然后水解产物。版权所有（C）2004，JPO

9. 发明专利

JP2004115402A Method for producing n,n'-dialkyl cyclic urea compound 审中-公开
公开(公告)号：JP2004115402A
公开(公告)日：2004-04-15
申请号：JP2002278553
申请日：2002-09-25
申请人： Mitsui Chemicals Inc , 三井化学株式会社
发明人： TAKAOKA MASAZUMI , MIZUTA HIDEKI , MATSUZAKI YORIAKI
IPC分类号： C07D233/34
摘要： PROBLEM TO BE SOLVED: To provide a method for profitably producing an N,N'-dialkyl cyclic urea compound.
SOLUTION: This method for producing an N,N'-dialkyl cyclic urea compound represented by general formula (3) [R
1 is a 1 to 4C straight chain or branched alkyl; (n) is an integer of 2 or 3] is characterized by reacting an N,N'-dialkylalkylenediamine compound represented by general formula (1) with a carbonic diester compound represented by general formula (2) (R
2 and R
3 are each identically or differently a 1 to 4C straight chain or branched alkyl or phenyl, provided that R
2 and R
3 may be bound to each other to form a ring).
COPYRIGHT: (C)2004,JPO

10. 发明专利

JP2003206267A METHOD FOR PRODUCING 4,6-DIAMINORESORCIN DIHYDROCHLORIDE 审中-公开
公开(公告)号：JP2003206267A
公开(公告)日：2003-07-22
申请号：JP2002003254
申请日：2002-01-10
申请人： MITSUI CHEMICALS INC
发明人： KUMAMOTO YUKIHIRO , YOSHITOMI HIDETAKE , TAKAOKA MASAZUMI , MIZUTA HIDEKI , MATSUZAKI YORIAKI
IPC分类号： C07C213/08 , C07C213/10 , C07C215/80
摘要： PROBLEM TO BE SOLVED: To provide a method for producing 4,6-diaminoresorcin dihydrochloride, capable of effectively producing the 4,6-diaminoresorcin dihydrochloride from a solution containing the 4,6-diaminoresorcin dihydrochlorde by reducing the amount of a discharged waste fluid to the least possible extent. SOLUTION: This method for producing the 4,6-diaminoresorcin dihydrochloride includes (1) a first process for mixing the aqueous solution containing the 4,6-diaminoresorcin dihydrochloride with hydrochloric acid to form a hydrochloric acid aqueous solution containing the 4,6-diaminoresorcin dihydrochloride, (2) a second process for concentrating the hydrochloric acid aqueous solution containing the 4,6-diaminoresorcin dihydrochloride to form a concentrate in which the 4,6-diaminoresorcin dihydrochloride is deposited, subjecting the concentrate to solid-liquid separation, and recovering the deposited 4,6-diaminoresorcin dihydrochloride from the concentrate together with a filtrate, and (3) a third process for reusing the filtrate which is recovered in the second process, or the hydrochloric acid which is recovered from the filtrate, as the hydrochloric acid which is mixed with a new aqueous solution containing the 4,6-diaminoresorcin dihydrochloride in the first process. COPYRIGHT: (C)2003,JPO

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