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1. 发明专利

JP2014126416A Liquid chromatograph apparatus 审中-公开
标题翻译：液相色谱仪
公开(公告)号：JP2014126416A
公开(公告)日：2014-07-07
申请号：JP2012281940
申请日：2012-12-26
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： MINAMOTO NORIMASA , ITO MASATO , TAKI MAMORU , YAMADA HIDETOMO
IPC分类号： G01N30/34 , G01N30/26 , G01N30/86
摘要： PROBLEM TO BE SOLVED: To provide a liquid chromatograph apparatus for reducing user's burden by automatizing the adjustment of an enclosed liquid capable of keeping a high separation performance for a long time.SOLUTION: After analysis processing of a sample, the mixture ratio of at least two kinds of eluant is determined so that pH in a solution filled into a separation column is 4.0-7.0 and the chloride ion concentration is 0.1-0.5 mol/L. A pump is controlled so that the eluant is fed on the basis of the determined mixture ratio.
摘要翻译：要解决的问题：提供一种通过自动化能够长时间保持高分离性能的封闭液体的调节来降低用户负担的液相色谱仪装置。解决方案：对样品进行分析处理后，至少混合比确定两种洗脱剂，使得填充到分离塔中的溶液中的pH为4.0-7.0，氯离子浓度为0.1-0.5mol / L。控制泵，使得洗脱液基于所确定的混合比进料。

2. 发明专利

JP2014106213A Liquid chromatograph auto-sampler 审中-公开
标题翻译：液相色谱自动采样器
公开(公告)号：JP2014106213A
公开(公告)日：2014-06-09
申请号：JP2012261843
申请日：2012-11-30
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： HARADA YUJI , OTSUBO AYANO , ITO MASATO
IPC分类号： G01N30/16 , G01N30/20 , G01N30/26
摘要： PROBLEM TO BE SOLVED: To provide a method for providing a weighing bulb separate from a passage switch valve and weighing a sample in a passage provided in a seal to accurately inject the minute quantity of the sample.SOLUTION: A liquid sample introduction device for a liquid chromatograph comprises: a weighing bulb having a plurality of passages capable of storing the predetermined quantity of sample; a liquid sample introduction part for weighing and sucking the sample to introduce the sample into the passages provided in the weighing bulb; and a passage switch valve for switching the passages so as to introduce the sample introduced into the passages provided in the weighing bulb into a mobile phase passage.
摘要翻译：要解决的问题：提供一种用于提供与通道切换阀分开的称重灯泡并在设置在密封件中的通道中称量样品以精确地注入微量样品的方法。解决方案：一种液体样品引入装置，液相色谱仪包括：具有能够存储预定量样品的多个通道的称重灯泡; 用于称量和吸取样品以将样品引入设置在称重灯泡中的通道中的液体样品引入部分; 以及通道切换阀，用于切换通道，以将引入到设置在称重灯泡中的通道的样品引入流动相通道。

3. 发明专利

JP2014102096A Liquid spill detector for column thermostatic tank, method, and program 审中-公开
标题翻译：用于柱温箱的液体泄漏检测器，方法和程序
公开(公告)号：JP2014102096A
公开(公告)日：2014-06-05
申请号：JP2012252576
申请日：2012-11-16
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： KUBO SHINTARO , ITO MASATO , NARIMATSU IKUKO
IPC分类号： G01N30/54 , G01N30/86
摘要： PROBLEM TO BE SOLVED: To accurately detect liquid spill in a column thermostatic tank with a gas detection sensor.SOLUTION: The liquid spill detector for a column thermostatic tank comprises: a column thermostatic tank for keeping the temperature of a column for separating a specimen to be constant; a gas detection sensor for detecting the gas concentration in the column thermostatic tank; and a determination section for determining the presence/absence of the occurrence of liquid spill in the column thermostatic tank on the basis of the transition of the detection value in a certain period after the detection value of the gas detection sensor establishes a predetermined condition.
摘要翻译：要解决的问题：准确检测带有气体检测传感器的色谱柱恒温槽中的液体泄漏。解决方案：用于柱式恒温槽的液体溢出检测器包括：用于保持用于将样品分离的色谱柱的温度的色谱柱恒温槽不变; 气体检测传感器，用于检测列恒温槽中的气体浓度; 以及确定部，其基于在气体检测传感器的检测值建立了预定条件之后的一定时间段内的检测值的转变来确定列恒温槽中的液体溢出的存在/不存在。

4. 发明专利

JP2012145595A Liquid chromatograph device 有权
标题翻译：液相色谱仪
公开(公告)号：JP2012145595A
公开(公告)日：2012-08-02
申请号：JP2012105591
申请日：2012-05-07
申请人： Ajinomoto Co Inc , Hitachi High-Technologies Corp , 味の素株式会社 , 株式会社日立ハイテクノロジーズ
发明人： MARUOKA KANTARO , FUKUDA MASATO , TOMITA KOJI , OKUZAWA KAZUHIKO , MINAMOTO NORIMASA , KUBO SHINTARO , TSUTSUDA KOUJI , YOSHIDA MASAAKI , ITO MASATO , OZAWA SHINICHI
IPC分类号： G01N30/02
摘要： PROBLEM TO BE SOLVED: To provide an automated liquid chromatograph device, which can respond to such needs by recent users that they want to relatively easily operate liquid chromatography devices without participating in special educational training on liquid chromatography.SOLUTION: Automation in purging and bubbling can be achieved by controlling a high pressure change-over valve and an electromagnetic valve, respectively, by a time program. However, when these operations are always controlled by a given time program, an intelligent automated device is no longer obtained because of excessive purging or excessive bubbling. Thereby, it is required to scheme a process flow that takes knowledge of experts for achieving intelligent control. In the case of purging, it is preferable to control purging depending on a time period that a pump is stopped, such that a purging period is decreased with a shorter stop time, and the purging period is increased with a longer stop time.
摘要翻译：要解决的问题：提供一种自动化液相色谱装置，其可以响应最近用户的这种需要，以便他们想要相对容易地操作液相色谱装置，而不参加液相色谱的特殊教育培训。解决方案：通过时间程序分别控制高压转换阀和电磁阀可以实现吹扫和起泡中的自动化。然而，当这些操作总是由给定的时间程序控制时，由于过量的吹扫或过多的起泡，不再获得智能自动化设备。因此，需要制定一个掌握专家知识以实现智能控制的流程。在清洗的情况下，优选根据泵的停止时间来控制清洗，使得清洗期间以较短的停止时间减少，并且清洗期间以更长的停止时间增加。版权所有（C）2012，JPO＆INPIT

5. 发明专利

JP2012008061A Separation column for liquid chromatography and liquid chromatography 审中-公开
标题翻译：液相色谱和液相色谱分离柱
公开(公告)号：JP2012008061A
公开(公告)日：2012-01-12
申请号：JP2010145772
申请日：2010-06-28
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： SHIMIZU KATSUTOSHI , ITO MASATO
IPC分类号： G01N30/88
摘要： PROBLEM TO BE SOLVED: To provide a separation column for liquid chromatography achieving a high-speed separation and analysis without lowering a column performance even if enhancing a linear velocity, and to provide liquid chromatography.SOLUTION: A monolith type separation column incorporates a monolith rod formed into a columnar shape in the separation column, a specimen and a moving phase flow into the monolith rod, and the monolith rod is alternately provided with portions having pores and portions without pores. The monolith rod is configured such that porous bodies having pores and portions without pores are alternately disposed in the specimen flowing direction. Alternatively, the portions having pores are porous bodies and the portions without pores are non-porous beads.
摘要翻译：要解决的问题：提供用于液相色谱的分离柱，即使提高线速度也能实现高速分离和分析，而不降低色谱柱性能，并提供液相色谱。解决方案：整体式分离塔包括在分离柱中形成为柱状的整料，样品和移动相流入整料，并且整料棒交替地设置有具有孔和部分的部分，没有毛孔。整料杆构造成使得具有孔和不带孔的部分的多孔体在试样流动方向上交替地设置。或者，具有孔的部分是多孔体，没有孔的部分是无孔珠粒。版权所有（C）2012，JPO＆INPIT

6. 发明专利

JP2010112960A Liquid chromatography apparatus and analysis program 有权
标题翻译：液相色谱仪和分析程序
公开(公告)号：JP2010112960A
公开(公告)日：2010-05-20
申请号：JP2010007678
申请日：2010-01-18
申请人： Ajinomoto Co Inc , Hitachi High-Technologies Corp , 味の素株式会社 , 株式会社日立ハイテクノロジーズ
发明人： MINAMOTO NORIMASA , MARUOKA KANTARO , KUBO SHINTARO , YOSHIDA MASAAKI , ITO MASATO , OZAWA SHINICHI
IPC分类号： G01N30/34 , G01N30/84 , G01N30/86 , G01N30/88
摘要： PROBLEM TO BE SOLVED: To reduce an analysis cycle time.
SOLUTION: In a liquid chromatograph analysis, the cycle time from current sample injection to next sample injection is fixed. A sample is injected, before a column is equilibrated by an eluting solution. Since the timing, when the eluting solution is switched in each injection/analysis cycle and the timing, when the sample is injected are synchronized, the properties for comparatively and reproducibly solving the hold time of each component peak is applied, even though the column does not necessarily become equilibriated.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：减少分析周期时间。
解决方案：在液相色谱分析中，从当前样品注入到下次样品注入的循环时间是固定的。在将柱用洗脱液平衡之前，注入样品。由于在每次注入/分析循环中洗脱溶液切换时间和定时时间的同时，因此，在使样品注入时的时序同步化的情况下，即使使用色谱柱不一定变得平衡。版权所有（C）2010，JPO＆INPIT

7. 发明专利

JP2009204521A Separation column and liquid chromatograph 有权
标题翻译：分离柱和液相色谱
公开(公告)号：JP2009204521A
公开(公告)日：2009-09-10
申请号：JP2008048350
申请日：2008-02-28
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： MORI KIYOTOSHI , KACHI HIRONORI , ITO MASATO , ISHII KIMIHIKO , SHOJI TOMOHIRO , TOYOSAKI KOSAKU
IPC分类号： G01N30/88 , G01N30/32 , G01N30/46
CPC分类号： B01D15/22 , B01J20/28004 , B01J20/28042 , B01J2220/58 , B01J2220/82 , B01J2220/825 , G01N30/6065 , G01N2030/528
摘要： PROBLEM TO BE SOLVED: To provide a separation column with the monolith rod which breaks a monolith rod and achieves a transmission of a liquid at a high pressure without use of a resin coating material. SOLUTION: A liquid is transmitted at the high pressure by building the monolith rod (a monolithic silica rod) 1 formed into a tapered-columnar shape, onto a clad whose inner shape is machined into the tapered-columnar shape. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供具有破碎整料杆的整料杆的分离柱，并且在不使用树脂涂料的情况下实现高压下的液体的透过。解决方案：通过将形成为锥形的整料（整体式石英棒）1构造成内部形状被加工成锥形的包层，使液体在高压下传递。版权所有（C）2009，JPO＆INPIT

8. 发明专利

JP2008261880A Mixer and liquid analyzer 有权
标题翻译：混合器和液体分析仪
公开(公告)号：JP2008261880A
公开(公告)日：2008-10-30
申请号：JP2008176432
申请日：2008-07-07
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： OOHASHI TOMOKI , SASAKI YASUHIKO , ITO MASATO , KACHI HIRONORI
IPC分类号： G01N30/34 , B01F3/08 , B01F5/02 , B01F5/06 , B01F13/00 , B01F15/02
CPC分类号： B01F5/0256 , B01F13/0059
摘要： PROBLEM TO BE SOLVED: To provide a mixer capable of mixing two kinds of liquids with each other while varying a mixing ratio in a wide range of the flow rates thereof by causing the two liquids in trace amounts to come into contact with each other, or a mixer capable of mixing them in short time. SOLUTION: This mixer is composed of a very thin mixing chamber for effecting mixing reaction, and micro-nozzles, provided at a high density on the upper and lower faces thereof. The mixer is structured such that the micro-nozzles are arranged on the inner walls of the mixing chamber to oppose each other, and the two liquids are spurted from the micro-nozzles, thereby implementing mixing by taking advantage of a diffusion phenomenon. Since the two liquids in trace amounts are ejected from the micro-nozzles in such a way as to oppose each other, the two liquids in trace amounts come into contact with each other, thereby enabling diffusion mixing in short time. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种混合器，其能够通过使两种微量液体与每种液体接触而在宽的流速范围内改变混合比，从而将两种液体彼此混合或者混合器能够在短时间内混合它们。解决方案：该混合器由用于进行混合反应的非常薄的混合室和在其上表面和下表面上以高密度提供的微喷嘴组成。混合器被构造成使得微喷嘴布置在混合室的内壁上彼此相对，并且两个液体从微喷嘴喷出，从而通过利用扩散现象来实现混合。由于微量的这两种液体从微喷嘴以彼此相对的方式喷出，所以痕量的两种液体彼此接触，从而能够在短时间内进行扩散混合。版权所有（C）2009，JPO＆INPIT

9. 发明专利

JP2008256654A Liquid chromatography 有权
标题翻译：液相色谱
公开(公告)号：JP2008256654A
公开(公告)日：2008-10-23
申请号：JP2007101780
申请日：2007-04-09
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： KUBO SHINTARO , TONO HIROYUKI , ITO MASATO
IPC分类号： G01N30/24 , G01N30/20 , G01N30/26
摘要： PROBLEM TO BE SOLVED: To improve the analysis throughput without reducing the accuracy of analysis.
SOLUTION: The liquid chromatography includes an analysis column, a detector to detect components separated in the analysis column, a pump to transfer a mobile phase of liquid and an analysis sample to the analysis column, a needle to suck a sample and inject it into aninjection port and suck washing liquid and injecting it into a washing port, a measuring syringe to eject the sample and washing liquid, and two sample loops communicating the needle with the tip. The chromatography is equipped with a sample inlet flow channel selector valve and a measuring flow channel selector valve. The sample inlet flow channel selector valve has a function to change communications among the analysis column, pump, injection port, and two sample loops. The measuring flow channel selector valve has a function of alternatively communicating the measuring syringe to the washing liquid supply side, washing port, and the sample inlet flow channel selector valve.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提高分析吞吐量，而不降低分析的准确性。解决方案：液相色谱法包括分析柱，检测分析柱中分离成分的检测器，将液体流动相和分析样品转移到分析柱的泵，吸取样品的针头和注射将其注入入口并吸入洗涤液并将其注入清洗口，测量注射器以喷射样品和洗涤液体，以及将针与尖端连通的两个样品回路。色谱仪配有样品入口流道切换阀和测量流路切换阀。样品入口流道切换阀具有改变分析柱，泵，注射口和两个样品环之间的通讯功能。测量流路切换阀具有将测量注射器交替地连通到洗涤液供给侧，洗涤口和样品入口流路切换阀的功能。版权所有（C）2009，JPO＆INPIT

10. 发明专利

JP2008224559A Liquid chromatograph 有权
标题翻译：液相色谱
公开(公告)号：JP2008224559A
公开(公告)日：2008-09-25
申请号：JP2007065977
申请日：2007-03-15
申请人： Hitachi High-Technologies Corp , 株式会社日立ハイテクノロジーズ
发明人： SHIMIZU KATSUTOSHI , ITO MASATO
IPC分类号： G01N30/86 , G01N30/88
摘要： PROBLEM TO BE SOLVED: To overcome differences in results of analysis due to column-by-column variations of attribute parameters of separation columns such as a monolithic-type column.
SOLUTION: On the basis of the volume V
0 of a filler in a separation column and a non-retention time t
0 of an analysis sample, attribute parameters of separation columns such as a monolithic-type column, a pumping rate F of a liquid chromatograph is adjusted as an adjustment parameter in such a way that values of non-retention time t
0 of the analysis sample between separation columns, and between liquid chromatographs results in the same value. The liquid chromatograph performs measurement as above.
COPYRIGHT: (C)2008,JPO&INPIT

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